B2O3/TiO2-ZrO2催化剂上环己酮肟的气相Beckmann重排反应

用共沉淀法制备了TiO2-ZrO2复合氧化物载体，BET，DTA，XRD表征结果表明，该复合载体具有较大的比表面和较好的热稳定性，对于环己酮肟气相Beckmann重排反应制己内酰胺，用复合载体制备的B2O3／TiO2-ZrO2催化剂，比分别以TiO2,ZrO2为载体所制备的B2O3/TiO2和B2O3／ZrO2催化剂具有更高的活性和选择性，实验表明，催化剂表面中等强度的酸位是环己酮肟气相Beckmann重排反应的有效活性中心。     

Finite-difference analysis of dielectric-loaded cavities using thesimultaneous iteration of the power method with the Chebyshevacceleration technique

A numerical procedure using the finite-difference technique, simultaneous iteration based on the power method, and the Chebyshev-polynomial preconditioning is proposed to analyze dielectric-loaded cavities. The merit of this method is that no matrix inversions are invoked and the convergence rate of the power method is greatly accelerated by the preconditioning. The TE, TM, and hybrid modes in axisymmetrical cavities loaded with a rod or ring dielectric resonator are analyzed. For the hybrid modes, an H_r-H_z formulation is proposed. Accurate numerical results are obtained efficiently and no spurious solutions are found by the present method     

Fuzzy estimation of feed-cutting force from current measurement-a case study on intelligent tool wear condition monitoring

It is very important to use a reliable and inexpensive sensor to obtain useful information about manufacturing processing, such as cutting force for monitoring automated machining. In this paper, the feed-cutting force is estimated using inexpensive current sensors installed on the ac servomotor of a computerized numerical control (CNC) turning center, with the results applied to the intelligent tool wear monitoring system. The mathematical model is used to disclose the implicit dependency of feed-cutting force on feed-motor current and feed speed. Afterwards, a neuro-fuzzy network is used to identify the cutting force with current measurement only. This hybrid math-fuzzy approach will reduce the modeling uncertainty and measurement cost. Finally, the estimated cutting force is applied in the tool-wear monitoring process. Successful experiments demonstrate robustness and effectiveness of the suggested method in the wide range of tool-wear monitoring applications.     

A new loss recovery architecture for wireless TCP

The loss recovery architecture of TCP under wireless environment is considered. We propose sent-time ordered two lists architecture as an alternative to sequence number ordered single list architecture. By keeping the sent-time order, the recovery mechanism can be more efficient and-simpler and transmission decision is decoupled from loss recovery using the second list. Simulation results show the superiority of our mechanism.     

加氢裂化工艺辅助操作与管理专家系统的开发与应用

近来，专家系统技术的利用已成火炼油与石油化工专家们感兴趣的问题。本文评述了国外这些领域中专家系统应用的进展概况。同时，对我们开发的专家系统工具ＦＥＸＳ的性能作了简介。详述了工业加氢裂化装置辅助操作与管理专家系统的研制过程和系统配置，讨论了系统开发的经验。最后，评价了该技术在炼油与石油化工业中的应用前景。     

用有限带宽反射波波形分析法进行储层横向预测

以正演地震模拟为基础的有限带宽反射波渡形分析法是一种新的储层横向预测方法。首先利用波形分解确定地震反射层的地质属性,找出能反映岩性变化的反射波波形特征参数;然后,采用多元数据聚类分析和灰色系统理论完成储层横向的预测。文中以预测江苏 J 凹陷 F 构造上阜二段生物灰岩分布及厚度横向变化为例,简述了反射波波形分析的全过程。预测结果已为钻探证实。     

胃动力信息采集与分析系统设计

本文设计了一套提取胃电和胃阻抗信号的胃动力信息采集与分析系统，该系统由采集系统和分析系统两部分构成。前者以单片机（ADuC834）为核心部件，实现了胃电和生物阻抗信号的同步采集和数据传输。后者对提取的阻抗信号和胃电信号运用小波多分辨分析处理，利用小波变换将胃阻抗信号从呼吸和血流信号中分离。系统可以应用于分析功能性消化不良患者胃动力的电过程和机械过程。     

Electrospinning of collagen-chitosan complex

The collagen-chitosan complex nanofibers have been prepared for the first time by electrospinning. The mixed HFP/TFA (the volume ratio of 90/10) was found to be the appropriate solvent for electrospinning. The concentration of the spinning solution and the ratio of chitosan/collagen were varied and adjusted to get smooth nanofibers. It was found that the diameter of the spun fibers became thick with the concentration of the solution increasing and became fine with the ratio of the chitosan/collagen increasing. We have characterised the molecular interactions in collagen-chitosan complex by Fourier transform infrared spectroscopy. The spun fibers are designed to mimic the native extracellular matrix for tissue engineering and to develop functional biomaterials.     

Analysis for the double staggered ladder circuit

A new type of mm-wave slow wave system, double staggered ladder circuit is analyzed in this paper, by means of “average cavity field method” and three-dimensional finite element method. The influence of the electron beam channel on the dispersion characteristics is discussed. An experimental research is made, the experimental results agree well with the theoretical one.     

冷却速度对激光相变组织分布的影响

提出通过改变边界换热条件，从而改变冷却速度，达到控制激光相变硬化。实验和计算结果的比较表明，这种控制相变及其组织分布的方法能够处理激光淬火难以解决的问题。