水性木器装修清漆的研制

以水性聚氨酯分散体与丙烯酸乳液及其混合液为成膜物 ,选用几种合适的助剂 ,研制出性能价格比良好的水性木器装修清漆。     

核壳结构纳米Ni／Al复合粉末的制备

在含氟离子的水溶液中，采用Al粉直接置换还原Ni盐的方法，实现了纳米Ni在Al粉表面上的快速化学沉积，制备出核壳结构的Ni／Al复合粉末。探讨了反应的过程，利用SEM、XRD、BET等测试手段对复合粉末进行了微观测试和表征。结果表明：Al粉表面连续、均匀包覆了由晶粒大小约20．6nm的Ni纳米颗粒组成的壳层。     

Electrical properties of BaTiO3-based NTC thermistors doped by BaBiO3 and La2O3

In our research it has been firstly found that BaTiO₃ materials doped with BaBiO₃ only show negative temperature coefficient effect over a wide temperature range. Major phases present in the sintered bodies are BaTiO₃ compounds with a perovskite structure and BaBiO₃ compounds with a monoclinic structure. Also, at a given BaTiO₃ and BaBiO₃ content, the influence of La₂O₃ content on the microstructure and electrical properties has been investigated. The mean grain size of samples decreases with an increase in La₂O₃ content. However the mean grain size remains unchanged with a further increase in La₂O₃ content when the La₂O₃ content in material is more than 0.20. As the amount of La₂O₃ in BaTiO₃-based ceramics thermistors increases, the resistivity decreases to a minimum value and then slowly increases again.     

电力系统稳定性研究的方法论思考

文章对电力系统稳定性研究内涵进行了评述，然后从认识论和方法论上加以分析，讨论了认识过程从功角稳定到电压稳定的转变、从线性向非线性的转变、从简单系统到复杂系统的转变、从重视解析方法到重视非解析方法的转变过程，为电力系统稳定性研究提供方法论指导。     

新型医用TLM钛合金管材加工工艺及性能研究

选择同样规格管坯进行了:①变形量ε分别为15%,28%,34%,40%的冷轧变形实验;②Q值为0.86,1.15,2.62的冷轧变形实验;③加热温度分别为680,715,730,820℃,均保温1 h的中间退火实验;④5种热处理工艺制度实验;⑤冷轧和拉拔2种不同加工方式实验.实验后用10%HF+30%HNO3+60%H2O酸洗液对管材表面进行处理,之后测试管材的力学性能.结果表明,该合金的变形量(ε)应选在30%～35%之间,Q值控制在2以下;中间退火温度应选在相变点以上,此时可获得最高的合金塑性,具有优良的冷加工性能;最终热处理应先在750℃固溶处理,然后再在510℃时效处理4 h可以得到塑性和强度匹配良好的管材.另外,采用轧制方法生产出的管材强度较高,塑性较低,表质量好,而采用拉拔方法生产出的管材塑性较高,强度略低,表面光洁度差.     

Preparation of a sensor substrate using functionalized mesoporous silica on a gold film for surface plasmon resonance (SPR) spectroscopy

The use of surface plasmon resonance (SPR) spectroscopy has been applied to a wide variety of fields such as biosensors and surface analysis instruments. In general, a SPR substrate is prepared using self-assembled monolayer (SAM) method of organic molecules as receptor for the target on a layer of gold or silver. However, mesoporous inorganic materials such as SBA-15 have benefits as sensor substrate for SPR. Mesoporous silica has a large surface area which receptor molecule can be attached and has a rigid body which has an excellent stability in the extreme condition compared to organic sensing layer. We prepared an organic modified mesoporous silica and successfully immobilized it on a gold surface, in an attempt to use as a substrate for SPR spectroscopy. For the comparison of sensitivity of prepared substrate, Pt²⁺ detection was selected as a model system. Substrate prepared in this study exhibited the capability of selective sensing for Pt²⁺ ions.     

Energy transfer mechanism of GdPO4: RE3+ (RE = Tb, Tm) under VUV-UV excitation

Polycrystal of GdPO₄:RE³⁺ (RE=Tb, Tm) phosphors were prepared by solid-state method. Vacuum ultraviolet excitation and emission spectrum and the energy transfer mechanism between the host and dopants of Tb³⁺ and Tm³⁺ were investigated respectively. The emission of Gd³⁺ at 313 nm was enhanced by the strong absorption of CTS of Tm³⁺ at 180 nm in GdPO₄: Tm. It has also been concluded that the excitation of Gd³⁺ is transferred to Tb³⁺ and then emission peaks of ⁵D_J→⁷F_J of Tb³⁺ were observed.     

现代工业设计中的新技术应用

科学技术的迅速发展支撑了现代工业设计的进步,针对现代工业设计的核心内容-产品设计的流程,讨论了各种新技术在产品设计各阶段中的应用,重点分析了计算机辅助工业设计(CAID)技术的应用现状及未来发展趋势.     

基于SPCE061A单片机的髋作用力测试仪设计

介绍了基于SPCE061A单片机的髋作用力测试仪的系统结构及部分软件编写流程,着重分析了测试仪的测力方法以及使用光电编码器进行测速和鉴相的原理.测试仪以SPCE061A单片机为控制核心,配有串行通信口,具备上位机实时监控、数据保存和复现、测试数据离线分析等功能.实验证明,该测试仪具有测量准确、稳定性高及操控界面友好等优点.     

基于混合PN／肖特基结构的新一代600V SiC肖特基二极管

第二代碳化硅(SiC)肖特基二极管——thinQ!2G是由一个肖特基结构和一个与它平行的独特的低电阻PN结组成,因此具备更加强大的浪涌电流处理能力,同时又继承了第一代碳化硅肖特基二极管所实现的良好的动态性能。