Preparation of phenolic resin derived 3-D ordered macroporous carbon

Three-dimensionally ordered long-range macroporous carbon structures were prepared using commercially available phenolic resin by utilizing sacrificial colloidal silica crystalline arrays as templates that were subsequently removed by HF etching after pyrolysis in an argon atmosphere. SEM, TEM, and BET were employed to characterize the morphology and the surface area of the porous carbon structures. The pore size (150–1000 nm) and BET surface area, which reflect pore volume (298.6 m²/g (1.32 cm³/g) ∼ 93.7 m²/g (0.12 cm³/g)), of the macroporous carbon structures produced were approximately proportional to the size (150–1000 nm) of the sacrificial silica sphere templates used (annealing temp. 550°C). The achieved 550 nm porous carbon structures were examined to function as potential catalyst carriers and were successfully impregnated with Ag or Pt-Ru on their inner walls after borohydride reduction at room temperature. In addition, porous carbon patterns were fabricated using the ‘micromolding in capillary’ technique, which has potential applications in the microreaction technology.     

Study of different effect on foaming process of biodegradable bionolle in supercritical carbon dioxide

Microcellular foaming of biodegradable Bionolle in supercritical CO₂ has been produced. The effects of a series of variable factors, such as saturation temperature, saturation pressure, and depressurization time and step on the foam structures and density, were studied through measurement of density and SEM observation. The experimental results show that higher saturation temperatures lead to an increase in bulk densities; and different depressurization time and step result in different product cell morphology. In addition, at some saturation temperature, the orientation of the cells can be found in the product morphology. XRD experimental results show that the foaming treatment with SC CO₂ increased the crystallinity of Bionolle. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 100: 2901–2906, 2006     

心理资本前因变量研究

采用心理资本问卷对分别属于医药、建筑、水利工程、电信、通讯运营和服务行业的6家企业的员工进行了调查.根据对回收的283份有效问卷的统计分析,认为员工的性别、受教育程度和所在企业的性质对员工心理资本不会产生显著性影响,而员工年龄的影响显著,50岁以上员工的总体心理资本水平高于其他年龄段员工.     

Fabrication and characterization of nano silver powder prepared by spray pyrolysis

Silver powder was fabricated by spray pyrolysis, using 2%–20% AgNO₃ solution, 336–500 mL/h flux of AgNO₃ solution, 0.28–0.32 MPa flux of carrier gas and in the 620–820 °C temperature range. The effects of furnace set temperature, concentration of AgNO₃ aqueous solution, flux of AgNO₃ aqueous solution as well as carrier gas on the morphology and particle size distribution of silver powder, were investigated. The experimental results showed that with the high concentration of AgNO₃ aqueous solution, the average grain size of silver decreased with the increasing of furnace set temperature. But the gain size distribution was not homogenous, the discontinuous grain growth occurred. With the low concentration of AgNO₃ aqueous solution, the higher furnace set temperature made the nano sliver grains sintered together to grow. Nano silver powder about 100 nm was fabricated by spray pyrolysis, using 2wt% AgNO₃ solutions, 336 mL/h flux of AgNO₃ aqueous solution, 0.32 MPa flux of carrier gas at 720 °C furnace set temperature.     

Zonal disintegration phenomenon in enclosing rock mass surrounding deep tunnels -- Elasto-plastic analysis of stress field of enclosing rock mass

The zonal disintegration phenomenon (ZDP) is a typical phenomenon in deep block rock masses. In order to investigate the mechanism of ZDP, an improved non-linear Hock-Brown strength criterion and a bi-linear constitutive model of rock mass were used to analyze the elasto-plastic stress field of the enclosing rock mass around a deep round tunnel. The radius of the plastic region and stress of the enclosing rock mass were obtained by introducing dimensionless parameters of radial distance. The results show that tunneling in deep rock mass causes a maximum stress zone to appear in the vicinity of the boundary of the elastic and the plas-tic zone in the surrounding rock mass. Under the compression of a large tangential force and a small radial force, the rock mass in the maximum stress zone was in an approximate uniaxial loading state, which could lead to a split failure in the rock mass.     

Study on early warning index of spatial deformation for high concrete dam

Owing to the deficiency in early warning for high concrete dam,a formula was established to characterize the deformation behavior of high concrete dam as a whole.The early warning index of spatial deformation was calculated by low probability principle on the basis of the deformation entropy formula proposed.The steps were as follows.Firstly,the probability method was utilized to define the degree of order and degree of chaos for each survey point.Secondly,the weight distribution among the survey points was...     

基于单片机的病房无线呼叫系统设计

为解决传统病房有线呼叫系统存在的布线复杂、易出故障、维修不便、不能在现有床位基础上及时增加新床位信息等问题,提出了无线呼叫系统设计。采用STC89C52系列单片机作为主控芯片,nRF905作为无线收发的核心芯片,并配以相应的LCD显示屏和声光报警器,设计出了无线病房呼叫系统。结果表明,该系统可靠传输距离达90 m以上,具有一定的抗干扰性,且可以临时方便增加床位显示信息,能够满足医院的临时实际需求。该系统性能稳定,操作简便,可以有效代替传统有线呼叫系统。     

Research on technology of desktop virtualization based on SPICE protocol and its improvement solutions

Increasingly mature cloud computing technology promotes virtual desktop technology, which can solve many problems existing in traditional computing models. However, virtual desktop solutions introduce the thorny problem of how to deliver a real desktop experience to users, as if they are using it locally, especially when playing video. The SPICE （simple protocol for independent computing environments） virtual desktop solution provides several image compression algorithms to address this problem with the purpose of making virtual desktops as real as possible. Although different compression algorithms can contribute their own abilities to different images to a large extent, switching between them is a big problem that consumes a large amount of resources to detect the different type of image and also causes jitter of the virtual desktop. This paper proposes a new solution, called SPICEx, using the JPEG2000 compression algorithm with dynamic compression ratios to solve the problem and finally validates that the performance is better than that of SPICE. With better quality of user experience and also reducing bandwidth consumption, SPICEx solution is meaningful in virtual desktop fields and can be widely used.     

An SVD-based adaptive robust speech steganography using MDCT coefficient

Multimedia Tools and Applications - Speech is one of the essential ways of communication. The study of speech steganography provides great value in information security. To improve imperceptibility...     

Full-scaled deep metric learning for pedestrian re-identification

Multimedia Tools and Applications - The pedestrian re-identification problem (i.e., re-id) is essential and pre-requisite in multi-camera video surveillance studies, provided the fact that...