Poly(3‐chlorothiophene) films prepared by the direct electrochemical oxidation of 3‐chlorothiophene in mixed electrolytes of boron trifluoride diethyl etherate and sulfuric acid

3‐Chlorothiophene (CT) was electrochemically polymerized in mixed electrolytes of a boron trifluoride diethyl etherate solution containing 0–20% (by volume) sulfuric acid. The oxidation potentials of the monomer in these media were measured to be only 1.06–1.31 V (vs Ag/AgCl). These values were much lower than that of CT in acetonitrile and 0.1 mol/L (Bu)₄NBF₄ (1.92 V vs Ag/AgCl). Poly(3‐chlorothiophene) (PCT) films with conductivities of 0.1–2 S cm^?1 were obtained. The structure, morphology, and electrochemical behavior of the PCT films also were investigated. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 87: 502–509, 2003     

Collaborative representation with reduced residual for face recognition

Collaboration representation-based classification (CRC) was proposed as an alternative approach to the sparse representation method with similar efficiency. The CRC is essentially a competition scheme for the training samples to compete with each other in representing the test sample, and the training class with the minimum representation residual from the test sample wins the competition in the classification. However, the representation error is usually calculated based on the Euclidean distance between a test sample and the weighted sum of all the same-class samples. This paper exploits alternative methods of calculating the representation error in the CRC methods to reduce the representation residual in a more optimal way, so that the sample classes compete with each other in a closer range to represent the test sample. A large number of face recognition experiments on three face image databases show that the CRC methods with optimized presentation residual achieve better performance than the original CRC, and the maximum improvement in classification accuracy is up to 12 %.     

以松节油为原料合成对异丙基甲苯

从松节油中分离出α 蒎烯 ,在溶剂回流温度和SiO2 -Al2 O3 -FeSO4催化剂作用下合成松油烯和柠檬萜烯 ,其收率分别达 4 7%和 4 3%以上。松油烯和柠檬萜烯在Ni-Cu催化作用下 ,采用固定床积分反应器合成对异丙基甲苯 ,工艺条件为温度 30 0～ 35 0℃、压力 9～ 11kPa,对异丙基甲苯的收率达 5 6 %以上。两步反应的催化剂效果良好     

扬巴工程中承包商合同控制

阐述扬巴项目中合同控制的基本做法,比较国内工程与涉外工程项目中合同控制的差异,提出承包商在涉外工程项目中做好合同控制工作的建议。     

A survey of traffic-based routing metrics in family of expected transmission count for self-organizing networks

Self-Organizing Networks (SONs) are attractive for applications where flexibility, resilience, and a large network service area are required. In order to meet the requirements of those applications, the principal issue is to guarantee efficient routing in SONs. Hence, the design and selection of appropriate routing metrics is important. A mass of metrics have been proposed in the past several decades. Among all the metrics, Expected Transmission Count (ETX) has drawn the most attention. Since the proposal of ETX, many ETX-based or extended metrics have been proposed. ETX and its descendants compose the ETX family. This paper is an attempt to analyze, compare and summarize traffic-based routing metrics in the ETX family. Details of each routing metric are presented and analyzed. Some of our viewpoints on the principal for designing metrics in SONs are presented.     

国产核电厂蒸汽发生器下封头接管区模拟装置承受循环载荷能力的试验

国产核电厂蒸汽发生器下封头群孔接管区具有应力分布复杂、焊接施工条件差的特点。为考核其承受循环载荷的能力，设计制造了与实物相似的模拟试验装置，根据核电厂运行寿命期内的载荷特点，确定了模拟试验装置的试验载荷与试验循环数。循环加载试验的结果表明，蒸汽发生器下封头群孔接管区承受循环载荷的能力在寿命期内是符合要求的。     

两步法合成大粒径丁苯胶乳

研究了聚甲基丙烯酸甲酯（MMA）对丁苯（BS）胶乳的附聚作用以增大丁苯胶乳粒径；探讨了无机盐、体系pH值及体系中MMA胶乳与BS胶乳的固含量比（R值）对附聚后丁苯胶乳的粒径及稳定性的影响。结果表明：适当添加无机盐可以稳定胶乳体系，最佳用量（质量分数）为0．1％～0．2％；适当增大体系pH值，可增大胶乳粒径；在附聚过程中，当R值在两个附聚峰附近时，可增大丁苯胶乳的粒径。     

集成电路密封用高纯邻甲酚醛环氧树脂的制备

ECN树脂中的可水解氯含量是决定树脂质量的—个重要指标。本文研究了反应温度、ECH/OCN配比、反应时间和碱用量等因素的影响,取得了规律性的认识,并获得最佳配方,制备出高纯度的ECN树脂系列产品。     

十二烷基苯磺酸钠水溶液聚集性质的研究

用滴体积法测出十二烷基苯磺酸钠（ＳＤＢＳ）稀水溶液的表面张力；然后求出其临界胶束浓度（ＣＭＣ）。同时通过溶液的电导率、吸收光谱以及荧光光谱测定求出其ＣＭＣ。这样测出的ＣＭＣ值为１．２～１．６×１０－３ｍｏｌ／Ｌ，与文献值相符。也研究了部分水解的聚丙烯酰胺（ＰＨＰＡＭ）对ＳＤＢＳ聚集性质的影响；发现ＳＤＢＳ的ＣＭＣ值随ＰＨＰＡＭ的加人而减少并且ＰＨＰＡＭ水溶液的粘度随ＳＤＢＳ的存在而急剧降低（类似盐效应）。这些方法与性质对强化采油（ＥＯＲ）是重要的。     

高职院校软件教学体系研究

本文在概述软件教学体系及其理论的基础上,结合软件教学的特点,阐述了软件教学体系的结构、应用环境以及在教学中将遇到的问题和解决对策,并描述了＂软件教学资源网系统＂建立的目的、设计方案、功能及开发环境。