Ionic transport studies of the glassy silver vanadomolybdate system

Ionic conductivity of the Ag₂O-MoO₃-V₂0₅ system has been studied over a wide range of frequency, temperature and composition. A narrower glass forming region has been found in comparison to the corresponding Ag₂O-MoO₃-P₂O₅ and Ag₂O-B₂O₃-P₂O₅ systems. The highest conductivity at room temperature, _rt, = 3.21 × 10^–6–1 cm^–1 (d.c.) with an activation energy,E _act, of 0.466 eV, was observed for the glass former's ratio of unity. Further, it reached a maximum value of 2.2 × 10^–2¨-1 cm^–1 withE _act = 0.153 eV when the oxide-base glass was dissolved with Agl. D.c. conductivity, hopping rate and relaxation time in the present system have been found to be characterized by the same activation energy.     

Facile synthesis of nitrogen and oxygen co-doped hierarchical porous carbon materials for high performance super capacitors

Journal of Porous Materials - Nitrogen and oxygen co-doped hierarchical porous carbons (NOPCs) is prepared by the pyrolysis of polyethylene glycol-200 (PEG) and triazine carbon forming agent (CFA)...     

Synthesis and characterization of aromatic polyisoimides derived from PMDA and para-diamines. An approach to in situ generated rigid-rod molecular composites

A new concept for the processing and fabrication of rigid-rod molecular composites aiming at the elimination or minimization of phase separation is proposed. This approach calls for a coil-like aromatic polyisoimide which is soluble and compatible with an amorphous matrix polymer or thermosettable oligomer and can undergo facile transformation to the corresponding rigid-rod polyimide in solid composite state, thus imparting the inherently high strength/high modulus properties to the final form. To this end, various synthetic routes were explored to obtain para-diamines which could afford high molecular weight and aprotic-solvent-soluble polyisoimides upon polymerization with pyromellitic dianhydride (PMDA). Four such polyisoimides were prepared, with their inherent viscosities ranging from 0.25 to 1.89 dl g⁻¹ in dimethylacetamide at 30°C. Facile thermally induced isoimide-imide conversion was demonstrated by solid-state (film) Fourier transform infrared spectroscopy. A preliminary evaluation of the compatibility of the polyisoimide/matrix resin was made. In one instance, a film prepared from the polyisoimide derived from PMDA and 3,3′,5,5′-tetramethylbenzidine (TMB) showed no visually detectable phase separation.     

无芯胶管的研制、工艺现状和发展建议

20世纪60年代初,我国胶管领域自主开发创新研制了无芯胶管制造技术,并且形成定型技术,一直沿用至今,笔者参与、见证了该产品从试验到投产的全过程。本文对该产品的工艺进行了新旧对比,提出了今后发展的建议。     

Optimum sweeps of simple polygons with two guards

A polygon P admits a sweep if two mobile guards can detect an unpredictable, moving target inside P  , no matter how fast the target moves. Two guards move on the polygon boundary and are required to always be mutually visible. The objective of this study is to find an optimum sweep such that the sum of the distances travelled by the two guards in the sweep is minimized. We present an O(n²)$O(n^2)$ time and O(n)$O(n)$ space algorithm for optimizing this metric, where n   is the number of vertices of the given polygon. Our result is obtained by reducing this problem to finding a shortest path between two nodes in a graph of size O(n)$O(n)$.     

Reciprocating flow ion exchange part II: Application to saline water softening

The “hardness” components in sea water can be considerably reduced by means of a new economical fixed bed technique called “Reciprocating Flow Ion Exchange”, when used in conjunction with a closed cycle exchanger-evaporator system. Removal of 87.9% of the calcium and 54.5% of the magnesium in sea water has been obtained with an overall flow rate of 5.0 U. S. g. p. m./sq. ft. Results from bench scale and a 5,000 g. p. d. pilot plant were identical. The virtually continuous cyclic steady-state process requires a small amount of exchanger (0.5 to 2% of the usual ion exchange methods, such as conventional fixed beds or fluidized beds). The effects of variation in operating parameters are discussed.     

Support vector regression methodology for prediction of input displacement of adaptive compliant robotic gripper

The prerequisite for new versatile grippers is the capability to locate and perceive protests in their surroundings. It is realized that automated controllers are profoundly nonlinear frameworks, and a faultless numerical model is hard to get, in this way making it troublesome to control utilizing tried and true procedure. Here, a design of an adaptive compliant gripper is presented. This design of the gripper has embedded sensors as part of its structure. The use of embedded sensors in a robot gripper gives the control system the ability to control input displacement of the gripper and to recognize specific shapes of the grasping objects. Since the conventional control strategy is a very challenging task, soft computing based controllers are considered as potential candidates for such an application. In this study, the polynomial and radial basis function (RBF) are applied as the kernel function of Support Vector Regression (SVR) to estimate and predict optimal inputs displacement of the gripper according to experimental tests and shapes of grasping objects. Instead of minimizing the observed training error, SVR _poly and SVR _rbf attempt to minimize the generalization error bound so as to achieve generalized performance. The experimental results show that an improvement in predictive accuracy and capability of generalization can be achieved by the SVR approach compared to other soft computing methodology.     

Multi-scale patch-based sparse appearance model for robust object tracking

When objects undergo large pose change, illumination variation or partial occlusion, most existing visual tracking algorithms tend to drift away from targets and even fail to track them. To address the issue, in this paper we propose a multi-scale patch-based appearance model with sparse representation and provide an efficient scheme involving the collaboration between multi-scale patches encoded by sparse coefficients. The key idea of our method is to model the appearance of an object by different scale patches, which are represented by sparse coefficients with different scale dictionaries. The model exploits both partial and spatial information of targets based on multi-scale patches. Afterwards, a similarity score of one candidate target is input into a particle filter framework to estimate the target state sequentially over time in visual tracking. Additionally, to decrease the visual drift caused by frequently updating model, we present a novel two-step object tracking method which exploits both the ground truth information of the target labeled in the first frame and the target obtained online with the multi-scale patch information. Experiments on some publicly available benchmarks of video sequences showed that the similarity involving complementary information can locate targets more accurately and the proposed tracker is more robust and effective than others.     

Two-dimensional bilinear preserving projections for image feature extraction and classification

Two-dimensional locality preserving projections (2DLPP) was recently proposed to extract features directly from image matrices based on locality preserving criterion. A significant drawback of 2DLPP is that it only works on one direction (left or right) to reduce the dimensionality of the image matrices and thus too many coefficients are needed for image representation in low-dimensional subspace. In this paper, we propose a novel method called two-dimensional bilinear preserving projections (2DBPP) for image feature extraction. We generalized the image-based (2D-based) feature extraction techniques into bilinear cases, in which 2DLPP is a special case of our proposed method. In order to obtain the bilinear projections, we proposed an iteration method by solving the corresponding generalized eigen-equations. Moreover, analyses show that 2DBPP has stronger locality preserving abilities than 2DLPP. By using the label information and defining different local neighborhood graphs, the proposed framework is further extended to supervised case. Experiments on three databases show that 2DBPP and its supervised extension are superior to some other image-based state-of-the-art techniques.     

Preparation of Titanium Nitride/Alumina Laminate Composites

A preparation route for TiN/Al₂O₃ laminate composites has been described. A water-based process using Al₂O₃ and TiN slurries with solids contents of 40 and 35 vol%, respectively, was used to make TiN and Al₂O₃ tapes. The removal of the binder was monitored by weight-loss measurements in a thermogravimetry unit. Bodies composed of Al₂O₃ and TiN tapes were densified at temperatures of 1400° and 1500°C using the Spark Plasma Sintering^® (SPS) technique. Densities of >98% of the theoretical densities were approached. Crack-free and almost fully densified TiN/Al₂O₃ compacts were prepared by heating the burned-out green bodies to the final sintering temperature (1500°C) at a rate of 100°C/min, and with a holding time of 5–10 min, under a pressure of 75 MPa. The microstructures of the obtained compacts were studied using scanning electron microscopy. Grain sizes in the sintered Al₂O₃ and TiN compacts were similar to those of the precursor powders. Hardness and indentation fracture toughness were measured at room temperature, and the monolithic compacts as well as the laminate composites exhibited anisotropic mechanical behavior; i.e., the cracks propagated much more easily in a direction parallel to the laminas than perpendicular to them.