无卷边单分子层WS2纳米片原子结构的高分辨电子显微术研究

本文利用高分辨电子显微术(HRTEM)确定了无卷边的单分子层WS2纳米片的原子结构像.通过对样品不同区域HRTEM像进行傅里叶变换(FFT)分析,得到了各个区域的WS2纳米片的晶体取向,确定了WS2纳米片分子层数分布.根据电子显微像强度与样品层数的线性关系以及WS2纳米片的单分子层数分布模型,确定不同区域WS2纳米片的分子层数.为了进一步定量分析结果的正确性,通过模拟电子显微像在不同碳膜厚度及不同成像条件下WS2纳米片的HRTEM像,也确定了在像衬度上与实验像很好的匹配.     

左截尾双参数指数分布的可靠性评估(Ⅰ)

对左截尾双参数指数分布,给出了其分布参数(位置参数μ,尺度参数θ)、可靠性测度(失效率A,平均失效前时间(MTTF)M,可靠寿命tR,可靠度R(t))的UMVUE、Bayes估计与经典精确限和Bayes精确可信限,还给出了MTIF高精度的经典近似限.最后用数值例说明了这些方法.     

动态特征选择算法对恶意行为检测的优化研究

针对互联网中存在的恶意行为,特别是社交网络应用中的在线恶意行为,通常使用基于用户多维特征的聚类分析算法进行检测。提出一种动态特征选择算法(DFSA),使用具有特征加权熵的模糊C均值目标函数,首先为参数构建一个学习模式,自动计算每个特征权重,并剔除权重小于阈值的特征,动态选择重要的特征,迭代地更新隶属函数、簇中心和特征权重直到最优化为止,最后识别出具有高精度的恶意用户行为簇。仿真结果表明,对比SDAFS算法、ELAFC算法和NADMB算法,DFSA算法在Rand指数、Jaccard指数和归一化互信息量3个主要性能指标上均有改善。     

大型体育场屋盖索膜结构的施工质量控制

大跨空间屋盖应用索膜结构,属于现代的新材料与新技术,国内尚未有相关的施工规范。通过佛山体育场屋盖索膜结构施工,介绍了屋盖支撑钢结构、拉索及膜的安装施工工艺要求,由于采取了可靠的施工质量控制方法,工程质量优良。     

一种快速直接的长码捕获方法

传统的PMF-FFT算法用于直接长码捕获时,每次只能搜索一个码片相位,FFT的运算次数较多,捕获时间长,大步进PMF-FFT算法每次可以搜索多个码片相位,减小FFT的运算次数,从而加快了捕获速度.实验结果表明,该算法在长码捕获过程中能取得良好的捕获性能,具有广阔的应用前景.     

Essential oil composition and antimicrobial activity of Sphallerocarpus gracilis seeds against selected food-related bacteria

Sphallerocarpus gracilis from China is a little-investigated edible and medicinal plant. In the present study, the essential oil composition from S. gracilis seeds was investigated by GC and GC–MS. A total of 34 compounds representing 94.69% of the essential oil were tentatively identified. The main constituents were p-cymene (17.42%), γ-terpinene (25.58%) and α-asarone (33.12%). The antimicrobial activity, minimum inhibitory concentration (MIC), and minimum bactericidal concentration (MBC) of the essential oil from S. gracilis seeds were evaluated against eight Gram-positive bacteria (Listeria monocytogenes, Staphylococcus aureus, Staphylococcus epidermidis, Micrococcus luteus, Bacillus megaterium, Bacillus cereus, Bacillus coagulans and Bacillus subtilis), four Gram-negative bacteria (Salmonella enteritidis, Salmonella typhimurium, Klebsiella pneumoniae and Escherichia coli) and one fungus (Aspergillus niger). Results revealed that the essential oil from S. gracilis seeds exhibited significant in vitro antimicrobial property. Among all the tested microorganisms, the essential oil showed the strongest inhibitory effect against K. pneumoniae, whereas no inhibitory effect was found against L. monocytogenes and A. niger. Additionally, scanning electron microscopy (SEM) was used to observe morphological changes of bacteria treated with the essential oil from S. gracilis seeds. SEM observations confirmed the physical damage and considerable morphological alteration to the tested microorganisms treated with the essential oil. The data of this study suggests that the essential oil from S. gracilis seeds has great potential for application as a natural antimicrobial agent to preserve food.     

Improve on/off ratio of organic heterojunction transistors by adopting single-sandwich configuration

Organic heterojunction transistors (OHJTs) based on 5,5′″-bis(naphtha-2-yl)-2,2′:5″,2′″-quaterthiophene (NaT₄)/copper-hexadecafluoro-phthalocyanine (F₁₆CuPc) heterojunction were fabricated in single-sandwich and sandwich configurations, respectively. All the devices operated in depletion-accumulation (normally-on) mode. High field-effect mobility of 0.35 cm²/Vs was obtained for all devices, which was higher than that, 0.20 cm²/Vs of the devices with NaT₄ as active layer. The on/off ratio of 1 × 10⁵ was obtained for OHJTs with single-sandwich configuration, which is three orders of magnitude higher than that of OHJTs with sandwich configuration. Compared with OHJTs with sandwich configuration, the higher on/off ratio was mainly determined by the lower off state current in OHJTs with single-sandwich configuration. In OHJTs with single-sandwich configuration, the well-type shield effect of the source and drain electrodes caused a very narrow empty region in F₁₆CuPc film, which is responsible for the lower off state current.     

Study on Thermal Deformation Behavior and Properties of Vacuum Hot-press Sintered W(50)/Cu-Al_2O_3 Composite

In this work, the tungsten particulate reinforced Al2O3 dispersion strengthened copper base composites were successfully fabricated by using a vacuum hot-press sintering method. With the test temperature varying from 650 to 950 ℃ and the strain rate varying from 0.01 to 5 s-1, the W(50)/Cu-Al2O3 composites were isothermally compressed on a Gleeble-1500D thermal simulator. The true stress-strain curves of the W(50)/Cu-Al2O3 under different test conditions were obtained. The dynamic recrystallization of the W...     

Reliability-based bond design for GFRP-reinforced concrete

Most of proposed models available so far associated with the evaluation of design embedded length of fiber reinforced polymer (FRP) rods in concrete are not reliability-based. This paper made an attempt, from the probabilistic standpoint, to determine the design embedded length of a glass fiber reinforced polymer (GFRP) rod in the case of splitting bond failure from concrete. The mathematical model put forward by Orangun et al. for evaluating the average bond strength of reinforcing bars in concrete for splitting failure has been adopted to develop the nonlinear limit state function corresponding to GFRP’s splitting bond failure in which five independent random variables, i.e. concrete strength, GFRP tensile strength, embedded length, GFRP diameter and computational uncertainty factor, are included. As the result of the probabilistic calibration procedures using the Rackwitz–Fiessler method, a non-dimensional factor K associated closely with the design embedded length of a GFRP rod in concrete is proposed to be 0.0306 with the suggested additional target reliability index of 1.10. The effects of some factors on GFRP’s design embedded length have been identified through the following parametric study. Although the calibration process is case-dependent to some extent, the proposed formula is thought to be acceptable for general bond design purposes of GFRP-reinforced concrete components.