Demineralization of a UK bituminous coal using HF and ferric ions

A UK bituminous coal has been used to study demineralization by two-stage chemical leaching. The first-stage uses hydrofluoric acid (HF) at 65 °C and reduces the ash content from 5.30 wt% to 1.37 wt% by mainly removing Al and Si containing minerals. Subsequent leaching by ferric ions decreases the ash content further to 990 ppm by removing most of the pyrite and fluorides formed during the HF leaching. Calorific value of the coal shows no change following leaching, which suggests no oxidation is occurring to the coal carbonaceous matrix. The mercury and sulfur contents after the two-stage leaching sequence decrease by 40% and 26%, respectively.     

Ozone-Based Advanced Oxidation Processes for the Decomposition of N-Methyl-2-Pyrolidone in Aqueous Medium

The present study investigates the decomposition of N-Methyl-2-Pyrolidone (NMP) using conventional ozonation (O₃), ozonation in the presence of UV light (UV/O₃), hydrogen peroxide (O₃/H₂O₂), and UV/H₂O₂ processes under various experimental conditions. The influence of solution pH, ozone gas flow dosage, and H₂O₂ dosage on the degradation of NMP was studied. All ozone-based advanced oxidation processes (AOPs) were efficient in alkaline medium, whereas the UV/H₂O₂ process was efficient in acidic medium. Increasing ozone gas flow dosage would accelerate the degradation of NMP up to certain level beyond which no positive effect was observed in ozonation as well as UV light enhanced ozonation processes. Hydrogen peroxide dosage strongly influenced the degradation of NMP and a hydrogen peroxide dosage of 0.75 g/L and 0.5 g/L was found to be the optimum dosage in UV/H₂O₂ and O₃/H₂O₂ processes, respectively. The UV/O₃ process was most efficient in TOC removal. Overall it can be concluded that ozonation and ozone-based AOPs are promising processes for an efficient removal of NMP in wastewater.     

Spherical NiO-C composite for anode material of lithium ion batteries

Spherical NiO-C composite was prepared by dispersing spherical NiO in glucose solution and subsequent carbonization under hydrothermal conditions at 180 °C. The microstructure and morphology of the NiO-C and NiO powders were characterized by means of X-ray diffraction (XRD) and scanning electron microscopy (SEM). The electrochemical properties of the electrodes were measured by galvanostatic charge-discharge tests, cyclic voltammetric analysis (CV), and electrochemical impedance spectroscopy (EIS). SEM images showed that the amorphous carbon not only coated on the surface but also filled the inner pores of the NiO spheres. Electrochemical tests showed that the NiO-C composite exhibited higher initial coulombic efficiency (66.6%) than NiO (56.4%), and better cycling performances. The improvement of these properties is attributed to the carbon, as it can reduce the specific surface area of porous sphere, and enhance the conductivity of porous NiO.     

Ultrasonic oscillations effect on rheological and processing properties of metallocene‐catalyzed linear low density polyethylene

The effects of ultrasonic oscillations and die materials on die pressure, productivity of extrusion, melt viscosity of metallocene‐catalyzed linear low density polyethylene (mLLDPE), as well as their mechanism were studied in a special ultrasonic oscillations extrusion system developed in our lab. Die materials used in our experiment included steel, brass, and polytetrafluoroethylene (PTFE)_. The experimental results showed that ultrasonic oscillations as well as die materials have great influence on the rheological and processing behavior of mLLDPE. Ultrasonic oscillations can greatly increase the productivity of mLLDPE melt extruded through different dies, and can decrease the die pressure and the melt viscosity of mLLDPE. Compared with steel or brass die, mLLDPE melt extruded through PTFE die is more sensitive to ultrasonic oscillations. A possible mechanism for the improved processability of mLLDPE is proposed in this article. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 90: 1873–1878, 2003     

基于蜜罐技术的主动防护网络入侵探究

随着信息技术的快速发展,网络安全问题日益突出,如何保护网络安全成为人们研究的重点.在实际工作过程中应用蜜罐技术来进行主动防护网络入侵是一种新方式.由蜜罐技术和分布式代理构成的防护体系,能够有效降低攻击检测误报率.网络安全形势日益复杂的背景下加强对蜜罐技术的研究具有重要意义.本文将重点探讨如何利用蜜罐技术来实现对网络入侵的主动防护.     

XRF法在聚乙烯微量金属分析中的应用

探讨了用Ｘ射线荧光光谱分析法（ＸＲＦ法）测定聚乙烯中所含的微量金属Ｆｅ、Ｔｉ、Ａｌ的方法，简 分析条件及实验方法。     

多媒体教学服务系统的设计

本文从实际使用出发,提出了多媒体教学系统的设计思路,主要介绍了多媒体教学系统的系统结构、主要系统功能等。     

网络安全评估方法分析

近年来,网络攻击事件时有发生,给社会和企业带来巨大威胁和损失,对于网络安全评估方法的研究成为了热点,文中介绍了网络安全评估方法的研究现状,分析了网络安全评估相关技术,进而探析了网络安全评估方法。     

UPnP基本原理以及在NAT中的应用

在互联网应用越来越丰富的情况下,设备之间如何通过UPn P方案实现互联互通显得日益重要,本文介绍了UPn P所定义的基本协议（如SSDP、GENA、SOAP等）,重点分析了UPn P实现的基本工作流程,并通过抓包工具捕获数据包,对各种流程传递的协议报文进行详尽分析,最后结合NAT技术,重点叙述UPn P在NAT技术中的应用。通过本文能够加深认识设备之间互联互通的一种方案。     

DES_RSA及其混合算法的加密速度研究

为了在保证安全性的前提下提高大量数据加密的加密速度,本文通过DES和RSA算法的分析,针对DES算法密钥安全性差和RSA算法加密速度慢的问题,提出DES和RSA混合算法.对比DES和RSA两种算法加密所需时间,就RSA算法耗时长的问题,通过几种可行的大素数判定算法分析,提出改进的大素数判定算法.在保证安全性的前提下,将改进的大素数判定算法应用于RSA算法中,提升了加密速度.由于改进算法加密速度仍远差于DES算法,不适合大量数据加密.因此在兼顾安全性与加密速度的基础上,提出DES和RSA混合加密算法.经分析该算法综合了前两种算法的优点,是一种理想的加密算法.