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31.
Li Xi Zuoyan Peng Wei Fan Kui Guo Gu Jianmin Muyu Zhao Wu Guoqiang 《Materials Science and Engineering: B》1996,40(2-3):147-152
SrMgxTi1 - xO3 nanocrystals (x = 0.1–0.6) were synthesized by the stearic acid gel method. Powder samples were characterized by X-ray diffraction and X-ray photoelectron (XP) spectroscopy. The results showed that the lattice parameter a and the O 1s XP spectrum changed not only with the Mg content x but also with the grain size d of the samples. The conductivity of a thick film specimen fabricated on an aluminium oxide wafer was investigated in a nitrogen—oxygen atmosphere. 相似文献
32.
Thirty six patients of pulmonary or nasopharyngeal carcinoma were treated with Xilixin granule (XLXG) combined with radiotherapy and compared their efficacy with that of 31 patients treated by Zhenqi Fuzheng granule combined with radiotherapy for control. Results showed that the symptoms of Yin Deficiency syndrome in treated group were obviously improved, the leucocyte decreased by 5.6%, while in control group it reached 25.8%, the 3 year survival rate was significantly higher in treated group (75.0%) than that in control group (51.6%). Animal experiment revealed that XLXG had the effects of tumor inhibition, it could increase white blood cells, platelets and hemoglobin of patients, especially in using large dosage. These results suggested that XLXG have some protective effect against radiotherapeutic damage in patients with malignant tumor. 相似文献
33.
Porous silica glass was prepared by sol-gel process from tetraethoxysilane (TEOS). The effects of solvents (water, ethanol), drying condition, heat treatment temperature on specific surface area and pore size distribution of porous silica were investigated. Gelation process accelerates with an increase of H2O content, while retards with the increase of ethanol amount. Structure changes during heat treatment were studied by means of DTA, XRD. TEM micrographs show that the gel particles shrink after heated at 500°C, thus the average pore size decreases. 相似文献
34.
The Bi-system tapes and coils were prepared by the powder-in-tube method. The effect of processing and heat treatment on the properties of the tapes and coils was studied. It is found that the shearing stress produced by the rolling process may destroy the 2223 phase, and the destroyed 2223 phase cannot be recovered by heat treatment, whereas the pressing stress produced by the uniaxial pressing process only makes the 2223 phase grains break, and the broken 2223 phase can be closed by the heat treatment. TheJ
c values of the rolling samples, pressing sample, and the coil with a diameter of 35 mm are over 1.3×104, 2.5×104, and 4×103 A/cm2 (77 K, 0 T), respectively. 相似文献
35.
Digital periodic signal analysis often requires synchronized sampling with the signal being analyzed. In certain practical situations, however, this condition is difficult to satisfy. As a result, a number of undesirable effect such as the spectral leakage associated with the discrete Fourier transform (DFT), and the truncation errors in digital wattmeters arise and degrade system performance. This paper presents a new approach which attempts to remedy the underlying problem. The basic idea of the proposed method is to modify the actual sampled sequence such that it becomes an ideal sample sequence which is synchronized with the signal subjected to sampling. A simple algorithm for modifying the sampled sequence on-line is derived based on interpolation. The proposed approach requires quite modest additional computational burden which makes it suitable for real-time signal professing. To illustrate the practical applicability of the proposed algorithm, the paper considers two distinct but common cases. First, it shows how the proposed method can be used in the case of DFT analysis of harmonic signals, and secondly, it considers the digital wattmeter application area in electrical power-system measurement. Results show that the proposed algorithm is capable of reducing both the leakage effect in DFT analysis and truncation errors in digital wattmeters 相似文献
36.
分析恒载效应的有限元方法 总被引:2,自引:0,他引:2
本文在Takabatake关于恒载对梁静、动力影响的研究工作的基础上,导出了梁考虑恒载效应的动力分析有限元公式,提出了荷载影响刚度矩阵的概念。分析了分布和集中两种恒载型式对简支梁和悬臂梁自振特性的影响。计算结果表明,用本文方法与Takabatake应用Galerkin方法和近似闭合解方法的结果吻合良好。同时由于本文采用了矩阵形式,不仅便于编制计算机程序,且使方法有更广泛的适用性和灵活性,可更方便地用于各种不同的构造和边界条件下的实际结构。 相似文献
37.
38.
Humin Cheng Jiming Ma Zhenguo Zhao Di Qiang Yongxiang Li Xi Yao 《Journal of the American Ceramic Society》1992,75(5):1123-1128
A pure, acicular lead titanate (PbTiO3 ) fine powder with a white color has been prepared by hydrothermal synthesis. It is a new phase of PbTiO3 with I 4 symmetry, cell parameters of a = 12.358 Å and b = 14.541 Å, and a density of 6.80 g.cm−3 . The influences of pH (12.5 to 14.4), Pb/Ti ratio (1.0 to 1.6) in the feedstock, reaction temperature (130° to 230°C), time (0.25 to 4 h), starting materials, and additives on the formation of acicular PbTiO3 under hydrothermal conditions have been investigated. The acicular PbTiO3 with I 4 symmetry, referred to as the PX phase, can be converted to the perovskite-type (PE phase) of PbTiO3 at about 605°C while its acicular morphology is essentially unchanged. The preferable conditions for preparing pure acicular PX-phase PbTiO3 are that the pH is 13.0 to 14.0, Pb/Ti ratio is >1.3, reaction temperature is 170° to 200°C, time is 0.5 to 1.0 h, titanium butoxide (Ti[O(CH2 )3 CH3 ]4 ) is the starting material, and poly(vinyl alcohol) is an additive. The acicular grain of the PX phase is usually less than 100 nm in diameter and more than 1000 nm in length. 相似文献
39.
Fan Chu Hong-Tao Sun Liang-Ying Zhang Xi Yao 《Journal of the American Ceramic Society》1992,75(11):2939-2944
Based on a linear voltage ramp method, ultraslow dielectric relaxation of undoped BaTiO3 ceramic has been carefully measured over the temperature range between − 180° and +120°C. Temperature dependence of the dielectric constant in the frequency range from 10 −5 to 10−1 Hz can be obtained using Kramers–Kronig equations. Close to the Curie temperature, the dielectric constant increases so rapidly that the Curie peak is overwhelmed. Two kinds of relaxation processes were observed in this experiment. Ferroelectric domain and mobile charge are proposed to be responsible for the relaxation over the temperature range. With temperature increasing, Maxwell–Wagner relaxation associated with mobile charge gradually dominates. From relaxation time constants at various temperatures, relaxation activation energies about 0.06 and 0.09 eV are identified. 相似文献
40.
本文用不同的测试技术和方法测定了锗酸铋(BGO)单晶的比热(300~800K)热膨胀系数(100~1100K)和导温系数(140~700K),进而导出了 BGO 单晶不同温度下的导热系数、定容比热、德拜温度和格虑内森数。本文还对 BGO 单晶热物理性质的变化规律作了理论解释。 相似文献