Methylaluminoxane/haloalkane as initiator system for styrene polymerization

Summary Styrene polymerization was initiated by methylaluminoxane in the presence of haloalkane. The propagating species are shown by trapping experiments and electron paramagnetic resonance to be both radicals and cations.     

Rugorous analysis of planar waveguides with two-dimensionally periodic layer

Rigorous analysis of planar waveguides with two-dimensionally periodic (2DP) layer is presented. Characteristic solutions in periodic layer are exactly represented by a double Fourier series known as the Floquet solutions. The vector amplitudes of space harmonics are proved to be governed by five-term recurrence relation in the operator-vector form for sinusoidal modulation. A general transmission-line network representation of two-dimensionally periodic medium and multiport network representation of uniform-periodic-medium interface are introduced. Any layered structures cascading with periodic ones can be analyzed. Numerical results based on the established theory are also presented to illustrate characteristics of 2DP medium and structure.     

空间三重奏

设计的确是一项非常有趣的工作，就如同一位导演运用出色的技巧掌控有限的预算，为观众呈现令人回味的剧情，逼真的音效和异彩纷呈的视觉映像，这无疑是三个紧密相扣的环。     

An observer-based robust adaptive controller for permanent magnet synchronous motor drive with initial rotor angle uncertainty

An observer-based robust adaptive nonlinear position and speed tracking controller is developed for a permanent magnet synchronous motor with initial rotor angle uncertainty. The unknown initial rotor position is treated as a constant motor parameter in the development of the controller. An incremental encoder, which provides relative position variation of the rotor, is used along with stator current signals to achieve stable control. However, the controller does not require the knowledge of motor parameters and it only assumes friction, external disturbances, and model uncertainties are bounded. By using state observers, the measurement of acceleration and load torque, which is required usually in the nonlinear controller design with high tracking performance, is avoided. The stability of the control system and tracking convergence are guaranteed using Lyapunov theory. Finally, the stability and efficacy of the proposed drive system are verified by experimental results.     

Growth and morphology of nanometer LiMn2O4 powder

The growth of Li_1+xMn₂O₄ via detonation reaction was investigated with respect to the presence of an energetic precursor, such as the metallic nitrate and the degree of confinement of the explosive charge. The detonation products were characterized by scanning electron microscopy. Powder X-ray diffraction and transmission electron microscopy were used to characterize the products. Li_1+xMn₂O₄ with 1-2 μm spherical morphology and more uniform secondary particles, but with smaller primary particles of diameters from 20 to 60 nm and a variety of morphologies were found. The oxides produced by this cheap method affirmed the validity of detonation synthesis of nano-size powders.     

Shear mode coupling and tilted grain growth of A1N thin films in BAW resonators.

Polycrystalline A1N thin films were deposited by RF reactive magnetron sputtering on Pt(111)/Ti electrode films. The substrates were tilted by an angle ranging from 40 degrees to 70 degrees with respect to the target normal. A low deposition temperature and a high sputter gas pressure were found ideal for tilted growth. The resulting grain tilt angle amounts to about half the substrate tilt angle. For coupling evaluation, 5 GHz solidly mounted resonator structures have been realized. The tilted grain A1N films exhibited a permittivity in the 9.5-10.5 range and loss tangent of 0.3%. Two shear modes as well as the longitudinal mode could be clearly identified. The coupling coefficient k2(eff) of the fundamental thickness shear mode (TS0) was found to be about 0.5%, which is compatible with a c-axis tilt of about 6 degrees.     

利用计算机进行油气资源评价和勘探决策

本文着重介绍了构成《现代勘探决策理论系统》的5个主要计算机模块,即:生油岩热演化处理、求任意曲边形面积、数学模拟预测资源量、勘探经济评价分析及决策、辅助处理等模块。该系统曾在塔里木盆地和准噶尔盆地的油气资源评价和勘探决策中发挥了作用,受到了专家和用户的好评。     

Experimental Study on Energy Consumption of Combined Conventional and Dehumidification Drying

Conventional drying, dehumidification drying, and combined conventional-dehumidification drying of wood were experimentally studied in this article. The results showed that the energy consumption in the dehumidification drying is the least but its drying time is the longest. The energy consumption in the combined drying is more than that in the dehumidification drying but less than that in the conventional drying, and the drying time is half of that in the dehumidification drying. The advantages of the combined conventional and dehumidification drying are discussed from the experiments results.     

Electron microscopic observations and DNA chain fragmentation studies on apoptosis in bone tumor cells induced by ~(153)Sm-EDTMP

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I．O．T．旧梦成真

该文较详细地介绍了Ｉ．Ｏ．Ｔ管的发展历程，其特点及工作方式。