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992.
Xue Zhang Jin Du Guosheng Su Peirong Zhang Yujing Sun Chongyan Zhang Xiangmin Kong 《International Journal of Applied Ceramic Technology》2022,19(3):1354-1366
Mo2NiB2 is a kind of cermet with excellent mechanical properties, stable chemical properties, and excellent corrosion resistance and is often used in wear-resistant application fields, such as injection molding machine parts, can making tools and hot copper extruding dies. The brittleness of Mo2NiB2-based cermets limits their wide application. Mo2NiB2-based cermets were prepared by the vacuum sintering method, the effect of SiC whiskers (SiCw) on the microstructure and mechanical properties of cermets was investigated, and the toughening mechanism of SiCw on cermets was further discussed. The results indicate that with increasing SiCw content, the indentation fracture toughness (KIC), transverse fracture strength (TRS), and Vickers hardness (HV) of the cermets first increase and then decrease. The HV, TRS, and indentation fracture toughness of Mo2NiB2-based cermets with 0.5 wt% SiCw are 1 113 HV, 1 620 MPa, and 27.97 MPa·m1/2, respectively, which are 16.8%, 22.7%, and 25% higher than those without SiCw. In the sliding friction tests, Mo2NiB2-based cermets with 0.5 wt% SiCw have the smallest friction coefficient, low wear rate, and high wear resistance. SEM observation and analysis of the crack path and fracture surface showed that the toughening mechanism is whisker bridging, crack deflection, microcrack toughening, and whisker pull-out. The results indicate that the addition of 0.5 wt% SiCw can effectively improve the mechanical properties of Mo2NiB2-based cermets and further expand the application space of Mo2NiB2-based cermets. 相似文献
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本文对金川集团东部贫矿锅炉房高效煤粉锅炉运行中负荷不能达产达标的问题进行了调查分析,探讨提出了负荷提升优化途径,并组织实施,取得了可观的经济效益和环保效果。 相似文献
995.
This article studies the effects of groove shape optimization on cavitation and lubricating characteristics of microgroove rotary seals (MGRS). A lubrication model considering cavitation effects for MGRS is established to obtain the variation in cavitation and lubricating characteristics with operating conditions. Furthermore, an optimization model of groove shape based on the lubrication cavitation model is developed and an optimal groove is obtained by co-designing the parameters of both groove shape structures and molded lines. The effects of optimal grooves and ordinary spiral grooves on cavitation and lubricating characteristics are compared and validation tests are carried out. Theoretical and experimental results indicate that the lubrication cavitation model based on the mass conservation boundary condition for MGRS could accurately predict the cavitation region of ordinary spiral grooves. Optimal grooves improve the pressure distribution of the groove area and restrain the generation of a cavitation region; therefore, the fluid bearing capacity and dynamic stiffness of optimal grooves are much larger than those of ordinary spiral grooves. 相似文献
996.
Wen Jin Liu Zhi Bin Xu Ke Jian Cui Min Xue Zi Hui Meng Xiao Chuan Huang Zhong Xue Ge Zhi Hui Lin Guang Ming Qin 《Propellants, Explosives, Pyrotechnics》2015,40(5):645-651
Two intermediates, 1,5‐dinitroso‐3,7‐dinitro‐1,3,5,7‐tetraazacyclooctane (DNDS) and 1‐nitroso‐3,5,7‐trinitro‐1,3,5,7‐tetraazacyclooctane (MNX), were isolated and characterized in the synthesis of 1,3,5,7‐tetranitro‐1,3,5,7‐tetraazacyclooctane (HMX) from the nitrolysis of 3,7‐dinitro‐1,3,5,7‐tetraazabicyclo[3,3,1]nonane (DPT) for the first time. When the nitrolysis of DPT was slowed down, two intermediates were detected with HPLC. It was proposed that electrophilic NO2+ and NO+ from HNO3 and N2O4 might attack nitrogen atoms at positions 3 and 7 of DPT to form the cations of the intermediates, then nucleophilic H2O attacked the bridge carbon atoms of DPT to produce the intermediates, which were oxidized to form HMX. 相似文献
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