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51.
References: 《中国炼油与石油化工》2007,(3):35-42
The proton nuclear magnetic resonance spectroscopy (1H-NMR), the synchronous fluorescence spectrometry (SFS) and the ruthenium ions catalyzed oxidation (RICO) method were used to determine the chemical structure of polyaromatic nucleus in Oman residue fractions. The results of 1H-NMR analyses showed that the average numbers of aromatic rings in the aromatics, resins and asphaltenes units were 3.2, 5.6 and 8.2, respectively. SFS was used to investigate the distribution of aromatic rings in residue fractions, the main distribution range of aromatic rings in aromatics, resins and asphaltenes were 3 4 rings, 3--5 rings and more than 5 rings, respectively. The aromatic network in residue fractions was oxidized to produce numerous carboxylic acids. The types and content of benzenepolycarboxylic acids, such as phthalic acid, benzenetricarboxylic acids, benzenetetracarboxylic acids, benzenepentacarboxylic acid and benzenehexacarboxylic acid disclosed the condensed types of aromatic nuclei in the core. The biphenyl fraction (BIPH), the cata-condensed fraction (CATA), the peri-condensed fraction (PERI) and the condensed index (BCI) were calculated based on the benzenepolycarboxylic acids formed. The results implied that there was less biphenyl type structures in all residue fractions. The aromatics fraction was almost composed of the cata-condensed type system, and the asphaltenes fraction was wholly composed of the peri-condensed type system, while in the resins fraction co-existed the two types, herein the peri-con- densed type was predominant over the cata-condensed type. Based on the analytical results obtained in the study, the components --aromatics, resins and asphaltenes -- were given the likely structural models. 相似文献
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Interpretation of scatterometer ocean surface wind vector EOFs over the Northwestern Pacific 总被引:1,自引:0,他引:1
Jiayi Pan Xiao-Hai Yan Quanan ZhengW.Timothy Liu Victor V Klemas 《Remote sensing of environment》2003,84(1):53-68
Satellite scatterometer winds over the northwestern Pacific were analyzed with the vector empirical orthogonal function (VEOF) method. The Hilbert-Huang transform (HHT), a newly developed non-linear and non-stationary time series data processing method, was also employed in the analysis. A combination of European Remote Sensing Satellite (ERS) −1/2 scatterometer, NASA Scatterometer (NSCAT) and NASA's Quick Scatterometer (QuikSCAT) winds covering the period from January 1992 to April 2000 and the area of 0-50°N, 100-148°E constitutes the baseline for this study. The results indicate that annual cycles dominate the two leading VEOF modes. The first VEOF shows the East Asian monsoon features and the second represents a spring-autumn oscillation. We removed the annual signal from the data set and calculated the interannual VEOFs. The first interannual VEOF represents the interannual variability existing in the spring-autumn oscillation. The temporal mode is correlated with the Southern Oscillation Index (SOI), but has a half-year lag with respect to the SOI. The spatial mode of the first interannual VEOF reflects the response of the tropical and extratropical winds to ENSO events. The second interannual VEOF is another ENSO related mode, and the temporal VEOF mode is correlated with the SOI with a correlation coefficient of 0.78, revealing the wind variability over mid-latitudes, which is associated with ENSO events. Further analysis indicated that the wind variability over the coast of East Asia represents anomalies of a Hadley cell. The quasi-biennial oscillation (QBO) was found in the temporal mode, indicating and verifying that the QBO in the wind fields is related to ENSO events. The third VEOF shows the interannaul variability in the winter-summer mode and displays the interannual variability of the East Asian monsoon. The three leading interannual VEOFs are statistically meaningful as confirmed by a significance test. 相似文献
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分析了百万吨级乙烯冷箱的设计难点和采取的对策,介绍杭氧设计、制造的乙烯冷箱的技术参数和设计方案,与国外公司设计方案的比较,说明杭氧乙烯冷箱的设计、制造技术与世界先进水平的差距大大缩小。 相似文献
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纳米技术在中药开发中的应用 总被引:7,自引:0,他引:7
本文综述了纳米科技与中药制剂相结合的发展,阐述了纳米中药的概念、特性,介绍了纳米中药的制备技术,另外探讨了收集纳米粒子的方法,最后,着重展望了纳米技术在中药制剂中广泛的应用前景。 相似文献
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