In situ technique for synthesizing multiple ceramic particulates reinforced titanium matrix composites (TiB + TiC + Y2O3)/Ti

In situ synthesized titanium matrix composites reinforced with multiple ceramic particulates including TiB, TiC and Y₂O₃ were fabricated by non-consumable arc-melting technique utilizing the chemical reaction among Ti, B₂O₃, B₄C and Y. The thermodynamic feasibility of the in situ reactions has been considered. X-ray diffraction (XRD) was used to identify the phases in the composites. Microstructures of the composites were observed by means of optical microscope (OM), scanning electron microscope (SEM) and electron probe. It is concluded that multiple reinforcements are synthesized and they show different shapes: TiB grows in needle shape; TiC grows in near-equiaxed and rod-like shapes; Y₂O₃ grows in near-equiaxed shapes when the content of Y is 0.6 wt.% and grows in dendritic shapes when the content of Y increases to 1.8 wt.%. Reinforcements TiB, TiC and Y₂O₃ are distributed uniformly in the titanium matrix.     

EXPERIMENTAL TESTING OF DRAW—BEAD RESTRAINING FORCE IN SHEET METAL FORMING

Due to complexities of draw-bead restraining force calculated according to theory and depending on sheet metal forming properties experiment testing system, a simplified method to calculate draw-bead restraining force is put forward by experimental method in cup-shaped drawing process. The experimental results were compared with numerical results and proved agreement. It shows the method is effective.     

NANO-MULTILAYERS WITH HIGH PERPENDICULAR ANISOTROPY FOR MAGNETIC RECORDING

(FePt/Ag)n nano-multilayers were deposited on MgO (100) single crystal with laser ablation and then subjected to annealing. FePt L1o grains with (001) texture and thus a large perpendicular magnetic anisotropy constant Ku of the order of 106 J/m3 were formed. A thick Ag layer is found to be favorable for decreasing the dispersion of the easy axis for magnetization. The measurement of time decay of magnetization gave rise to a small activation volume of the order of 10-25m3, showing the promising of being the recording medium for future high density perpendicular recording.     

MICROSTRUCTURE AND PROPERTIES OF C-Cu NANOSTRUCTURE THIN FILM

Nanostructured C-Cu thin films were deposited by reactive sputtering method and co-sputtering method. The relationships between microstructures, properties, and depo-sition parameters were studied and the results obtained from TEM, AFM, and XPS.indicate that the thin films are nanostructural, and have good in-depth uniformity. Theselected area electron diffraction (SAED) found that the nanosize Cu particles havethe fcc structure and the others are amorphous carbon or nanocrystallized graphiticcarbon. The peak positions of the Cu and C in XPS indicate them to be at the ele-mental state. In the IR transmission spectrum, diamond two-phonon absorption andgraphite Raman peaks were observed, which suggests microcrystal diamond particlesand graphite components exist in the C-Cu film. The higher electrical resistivity wasobtained.     

THERMAL DEMAGNETIZATION AND RANDOMNESS OF DOMAIN NUCLEATION OF SINGLE PHASE Nd_2 Fe_(14) B

Based on the observation of temperature variation of both domain structure and magnetic con-trast.the thermal demagnetization and randomness of domain nucleation was discussed.     

FORMING CONDITIONS AND GEOMETRICAL VARIETY OF ETCH FIGURES

本文以立方晶系中{100}型蚀坑为例,详细讨论了三种典型晶面(h00),(hk0)和(hkl)上出现的各类蚀坑的形成条件。给出了同类蚀坑几何多样性的判据,从而揭示了实际观察到的蚀坑几何多样性的根源。文中并提出了(hkl)面上蚀坑的复原及推演图解法。     

ROLE OF NITROGEN IN GRAIN ORIENTED SILICON STEEL CONTAINING Al

本文旨在确定Al,N含量在人们感兴趣的范围内与硅钢磁性的相关性。用热氢抽取法测定固溶氮和AlN中的氮,以阐明氮在含Al硅钢中的行为,并对以AlN为主要抑制剂的晶粒取向硅钢的工艺特性进行初步探讨。     

DECOMPOSITION AND PRECIPITATION OF CARBIDES IN HOT-ROLLED Si-Fe SHEETS

在高温金相显微镜下,直接观察碳化物在热轧硅钢中的分解与析出过程。指出冷却速度对碳化物析出形态有很大影响。用差热分析确定了碳化物的分解与析出温度。所得结果为改进热轧硅钢生产工艺提供了重要的依据。     

陶瓷喷砂嘴的冲蚀磨损特性及其损坏机理

采用热压烧结工艺制备了Al2O3/TiC、Al2O3/(W,Ti)C和B4C陶瓷喷砂嘴.以SiC和Al2O3为冲蚀磨料进行了喷砂冲蚀试验.结果表明纯B4C陶瓷材料的烧结温度高、保温时间长、致密度低、晶粒粗,抗弯强度和断裂韧性低,但硬度最高;而Al2O3/TiC和Al2O3/(W,Ti)C陶瓷材料的烧结温度和保温时间比纯B4C陶瓷大大减小,致密度高,抗弯强度和断裂韧性比纯B4C陶瓷高1倍以上,但硬度相对低.对陶瓷喷砂嘴在磨料冲蚀下的应力状态进行了有限元分析,结果表明陶瓷喷嘴入口处所受的应力最大,出口次之,中间区域最小.B4C陶瓷喷砂嘴的最佳入口锥角为11°,而Al2O3/(W,Ti)C陶瓷喷砂嘴的最佳入口锥角为16°.陶瓷喷嘴入口和出口处的磨损机理主要表现脆性断裂;而中间区域的磨损机理主要表现为磨料颗粒对喷嘴内壁表面的研磨、抛光和微切削作用.     

压铸模与铝合金金属间化合物的形成与分解

为了研究压铸模与铝合金金属间化合物的形成与分解过程,进行了热浸铝试验.试验结果表明金属间化合物的形成与分解是一个连续不断的循环过程,两者之间的相互关系导致了钢基的失重以及体积的减少.