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11.
以丙烯腈和苯甲醇为原料,浓硫酸作催化剂,合成了N-苄基丙烯酰胺(N-BAA)。考察了反应温度、反应时间和催化剂用量等因素对产物收率的影响,得出了最佳反应条件:n(丙烯腈):n(苯甲醇):n(浓硫酸)=3:1:1.2,反应时间3h,反应温度60℃。在最佳条件下,N-BAA的收率可达92%。每100g粗产物用10%氢氧化钠溶液提纯,精制产物纯度可达99.80%,熔点为64~65℃。通过红外光谱对产物结构进行了表征。 相似文献
12.
低温脂肪酶产生菌的筛选、鉴定及其部分酶学性质 总被引:15,自引:1,他引:14
从南极乔治王岛冻土来源的76株低温细菌中筛选到13株低温脂肪酶产生菌,对其中的BTsl0022菌株进行鉴定。通过生理生化特征、16s rDNA基因序列的同源性和系统发育分析发现,菌株RTsl0022属于假单胞菌属(Pseudomonas),但与已定名的假单胞菌有一定的差异,与未定名的Pseudomonas sp.PsB的亲缘关系最接近,故将其暂定名为Pseudomonas sp.BTsl0022。对该菌脂肪酶的酶学性质初步研究表明,酶的最适作用温度为24℃,对热敏感,60℃处理30min仅残留25%酶活性,酶的适宜作用pH范围在7.0~9.0,最适pH为8.0。 相似文献
13.
14.
Liang Y.C. Wenjiang Zeng Pick Hong Ong Zhaoxia Gao Jun Cai Balasubramanian N. 《Electron Device Letters, IEEE》2002,23(12):700-703
In this letter, a concise process technology is proposed for the first time to enable the fabrication of good quality three-dimensional (3-D) suspended radio frequency (RF) micro-inductors on bulk silicon, without utilizing the lithography process on sidewall and trench-bottom patterning. Samples were fabricated to demonstrate the applicability of the proposed process technology. 相似文献
15.
Xiangfei Chen Jianping Yao Fei Zeng Zhichao Deng 《Photonics Technology Letters, IEEE》2005,17(7):1390-1392
A novel single-longitudinal-mode (SLM) fiber ring laser that incorporates an equivalent phase-shifted fiber Bragg grating acting as an ultra-narrow bandpass filter in the laser cavity is proposed. The equivalent phase-shifted fiber Bragg grating has an ultra-narrow transmission bandwidth which ensures an SLM lasing. Stable SLM operation without mode hopping is demonstrated. 相似文献
16.
Hong Wang Rong Zeng Xiuping Li 《Microwave Theory and Techniques》2005,53(2):564-570
In this paper, RF noise in 0.18-mum NMOSFETs concerning the contribution of carrier heating and hot carrier effect is characterized and analyzed in detail via a novel approach that modulates the channel carrier heating and number of hot carriers using body bias. We confirm qualitatively a negligible role of hot carrier effect on the channel noise in deep-submicrometer MOSFETs. For a device under reverse body bias (Vb), even though the increase in hot carrier population is clearly characterized by dc measurements, the device high-frequency noise is found to be irrelevant to the increase in the channel hot carriers. Experimental results show that the high-frequency noise is slightly reduced with the increase in |Vb|, and can be qualitatively explained by secondary effects such as the suppression of nonequilibrium channel noise and substrate induced noise. The reduction of NFmin and Rn with the increase in |Vb| may provide a possible methodology to finely adjust the device high-frequency noise performance for circuit design 相似文献
17.
Aimin Xiang Zhongjie Du Qinghua Zeng Chen Zhang Hangquan Li 《Polymer International》2005,54(10):1366-1370
This paper presents recent efforts on the preparation of flexible polyhedral particles via concentrated emulsion templating polymerization in which the hydrophilic monomer (acrylamide) and hydrophobic monomer (butyl acrylate) are polymerized simultaneously in the continuous and dispersed phase, respectively. Such templating polymerization has been enhanced in our systems owing to the introduction of acrylamide monomer and their higher polymerization rate in continuous phase as compared with butyl acrylate in dispersed phase. Diffusion between the different phases was also inhibited. Furthermore, the stability of the concentrated emulsion and the molecular weight of the produced poly(butyl acrylate) were found to be significantly affected by the amount of redox initiator. The morphology of the particles could be controlled by varying the volume fraction of the dispersed phase and the polyhedral particles were achieved at higher volume fraction. Copyright © 2005 Society of Chemical Industry 相似文献
18.
曾春志 《信息安全与通信保密》2005,(10):38-39
前言随着电信市场竞争越来越激烈,各种电信业务资费呈下降趋势,因此大客户原来主要采用低速专线来组织其内部通信网的方式也发生变化,逐渐采用高速的2M电路或者LAN专线、VPN等IP电路进行组网。目前大客户主要分布在金融、政府、行政、外企、交通等行业,其采用运营商电路来组织其内部通信网络以满足中心网点与各个分支网点、分支机构的语音、数 相似文献
19.
Jianxin Wei Mark R Pickering Michael R Frater John F Arnold John A Boman Wenjun Zeng 《IEEE transactions on image processing》2005,14(8):1033-1042
It is well known that tile-boundary artifacts occur in wavelet-based lossy image coding. However, until now, their cause has not been understood well. In this paper, we show that boundary artifacts are an inescapable consequence of the usual methods used to choose tile size and the type of symmetric extension employed in a wavelet-based image decomposition system. This paper presents a novel method for reducing these tile-boundary artifacts. The method employs odd tile sizes (2N + 1 samples) rather than the conventional even tile sizes (2N samples). It is shown that, for the same bit rate, an image compressed using an odd tile length low-pass first (OTLPF) convention has significantly less boundary artifacts than an image compressed using even tile sizes. The OTLPF convention can also be incorporated into the JPEG 2000 image compression algorithm using extensions defined in Part 2 of this standard. 相似文献
20.