ZnO微／纳米纤维的静电纺丝及其表征

以聚乙烯吡咯烷酮(PVP)为络合剂与醋酸锌[Zn(CH3COO)2]反应制得前驱体溶液,用静电纺丝法制备了PVP／Zn(CH3COO)2纤维,经煅烧得到具有微孔结构的氧化锌(ZnO)微／纳米纤维。对所制备纤维分别采用差热-热重分析、红外光谱分析、X射线衍射分析、扫描电镜等手段进行了表征。结果表明: PVP/Zn(CH3COO)纤维表面光滑,直径约300-700 nm,经700℃煅烧后,可得到ZnO微／纳米纤维。     

PET工程塑料概况

综述了PET工程塑料合金化方面的主要研究开发情况，就PET／PBT、PET／PC、PET／聚酯聚醚、PET／尼龙、PET／PE等合金的研究及应用情况作了简单介绍。     

Association-Based Active Access Control models with balanced scalability and flexibility

In existing Active Access Control (AAC) models, the scalability and flexibility of security policy specification should be well balanced, especially: (1) authorizations to plenty of tasks should be simplified; (2) team workflows should be enabled; (3) fine-grained constraints should be enforced. To address this issue, a family of Association-Based Active Access Control (ABAAC) models is proposed. In the minimal model ABAAC₀, users are assigned to roles while permissions are assigned to task-role associations. In a workflow case, to execute such an association some users assigned to its component role will be allocated. The association's assigned permissions can be performed by them during the task is running in the case. In ABAAC₁, a generalized association is employed to extract common authorizations from multiple associations. In ABAAC₂, a fine-grained separation of duty (SoD) is enforced among associations. In the maximal model ABAAC₃, all these features are integrated, and similar constraints can be specified more concisely. Using a software workflow, case validation is performed. Comparison with a representative association based AAC model and the most scalable AAC model so far indicates that: (1) enough scalability is achieved; (2) without decomposition of a task, different permissions can be authorized to multiple roles in it; (3) separation of more fine-grained duties than roles and tasks can be enforced.     

Preparation and Catalytic Performance of Mesostructured Aluminosilicate Nano-particles with Wormhole-Like Framework Structure

A facile two-step sol–gel method has been developed for the preparation of mesostructured aluminosilicate nano-particles (Si/Al = 7.5) with wormhole-like but uniform pore structures and highly catalytic activities towards bulky hydrocarbon cracking. It is desirable that, as this synthesis takes place in the absence of alkali cations, the mesoporous nano-particulate material is directly obtained in the acid form, making a subsequent ion-exchange and calcination treatment superfluous.     

管材超声波分层缺陷检测中盲区的构成探析

管材超声波分层检测作为控制产品质量的关键步骤,必须引起相关从业人员的重视,特别是要重点分析分层缺陷检测中盲区的构成原因和分布特征。只有这样,才能切实保证检测结果的准确性,更好地控制管材质量。通过对超声波分层缺陷检测的重要性进行阐释,分析了其中盲区的构成和分布等问题。     

聚丙烯催化剂进展及应用

介绍了聚丙烯（ＰＰ）催化剂、工艺技术的进展及近十几年世界新开发的金属茂催化剂的结构、特点及用于生产问规聚丙烯的实例。金属茂催化剂用于ＰＰ生产，为开发高性能ＰＰ产品，提高市场竞争能力提供了可能。     

一种应对APT攻击的安全架构:异常发现

威胁是一种对特定系统、组织及其资产造成破坏的潜在因素,反映的是攻击实施者依照其任务需求对被攻击对象长期持续地施以各种形式攻击的过程.面对高级可持续威胁(advanced persistent threat,APT),在其造成严重经济损失之前,现有的安全架构无法协助防御者及时发现威胁的存在.在深入剖析威胁的外延和内涵的基础上,详细探讨了威胁防御模型.提出了一种应对APT攻击的安全防御理论架构:异常发现,以立足解决威胁发现的难题.异常发现作为防御策略和防护部署工作的前提,通过实时多维地发现环境中存在的异常、解读未知威胁、分析攻击实施者的目的,为制定具有针对性的应对策略提供必要的信息.设计并提出了基于异常发现的安全体系技术架构:"慧眼",通过高、低位协同监测的技术,从APT攻击的源头、途径和终端3个层面监测和发现.     

带长矩形接管受压圆简体的有限元分析与强度计算

本文运用有限元软件FEPG,建立了带长矩形接管受压圆筒体的三维参数化有限元模型,研究了矩形接管部位的应力分布特点,按照分析设计规范对带长矩形接管受压圆筒体进行了强度评定,并针对应力分布的不合理性提出了结构改进措施。     

涂层转移法精密铸造技术在子午线轮胎模具制造中的应用

子午线轮胎模具计算机辅助快速制造系统是由ＣＡＤ技术、快速成型技术、涂层转移法精密铸造技术、材料技术等多项高新技术组合而成的一项独特的先进制造技术。该系统充分利用液态材料成型任意性和高再现性的特点，具有适应性强、重复性好、加工周期短、制造成本低的特点。     

一种低温高光泽艺术陶瓷装饰用大红釉的研制

使用低温含铅透明釉为基础釉，选用适宜的包裹红色料，研制成功一种艺术瓷用高光泽大红釉，并探讨了不同因素对大红釉呈色的影响。