Synthesis of barium mercaptides and application of antimony/barium mercaptides

1　ＩＮＴＲＯＤＵＣＴＩＯＮＡｎｔｉｍｏｎｙｍｅｒｃａｐｔｉｄｅｓ[1～ 4 ] ｕｓｅｄａｓｈｅａｔｓｔａｂｉｌｉｚ ｅｒｉｓａｔｔｒａｃｔｉｖｅｎｏｔｏｎｌｙｆｏｒｉｔｓｒｅｌａｔｉｖｅｌｙｌｏｗｃｏｓｔ ,ｂｕｔａｌｓｏｆｏｒｉｔｓｓｉｍｉｌａｒｓｔａｂｉｌｉｚｉｎｇｅｆｆｅｃｔｃｏｍｐａｒｅｄｗｉｔｈｔｈａｔｏｆｔｈｅｍｏｓｔｅｘｃｅｌｌｅｎｔｏｎｅ ｏｒｇａｎｏｔｉｎ .Ｂｙｍａｋｉｎｇｆｕｌｌｕｓｅｏｆｔｈｅｐｌｅｎｔｉｆｕｌａｎｔｉｍｏｎｙｒｅｓｏｕｒｃｅ ,ｄｅｖｅｌｏｐｉｎｇａｎｔｉｍｏｎｙｍ…     

水平式隧穿磁强计的反馈控制系统设计

分析了水平式隧穿磁强计控制系统的原理和特点;给出了反馈控制系统传递函数方框图;求出了水平式隧穿磁强计的表头、隧道效应及梳齿静电驱动等框图的传递函数.采用二阶有源带通滤波的方式来减弱外界的噪声影响,经实验验证,降低了隧道间隙的变动量,使得隧道间隙从0.4～1.6nm减少到0.9～1.1nm,满足设计要求.     

磁梯度法探测钻孔桩钢筋笼长度的应用

建设工程基础桩的施工中,若少放钢筋笼将会造成工程桩的质量隐患,采用地球物理磁梯度法可以有效地检测桩中钢筋笼的节数和长度,并能取得满意的效果.     

Effect of various additives to marinating baths on some properties of cattle meat

Longissimus dorsi (LD) muscles obtained from young bull carcasses (Holstein Friesian) were marinated, using solutions containing 0.5% sodium tripolyphosphate (STP), 0.5% dicalciumhydrogen phosphate (CHP) and 0.5% citric acid (CA). All solutions, including a blank, contained 2% NaCl. Expressible moisture, cooking loss, marinade uptake, area gain (increase in slice size), colour coordinate values (L*, a*, b*), marinade and meat pH, and the textural properties of samples were evaluated. Marinating with STP and CHP solutions resulted lower cooking losses. Marinade uptake and area gain were lower for control steaks and steaks marinated with the CA solution. The highest lightness was found in steaks marinated with the CA solution. Steaks marinated with STP and CHP solutions were darker. The CA solution resulted in yellowness of steaks. All treatments significantly affected hardness, chewiness and resilience values of steaks. The lowest hardness value was found in steaks marinated with CA. STP and CHP treatments also improved tenderness.     

The effect of replacing fat with oat bran on fatty acid composition and physicochemical properties of meatballs

Oat bran was used as a fat substitute in the production of meatballs. The effect of oat bran addition on the fatty acid composition, trans fatty acids, total fat, some physicochemical and sensory properties of the samples was studied. Meatballs were produced with four different formulations; the addition of 5, 10, 15 and 20% oat bran. Control samples were formulated with 25% fat addition as in commercial production. The major fatty acids were cis-oleic, palmitic and stearic acid in all the meatball samples, those with oat bran added as well as the control. Meatballs containing oat bran had lower concentrations of total fat and total trans fatty acids than the control samples. Meatballs made with 20% oat bran had the highest protein, salt and ash contents, L value (lightness), b value (yellowness), and the lowest moisture content and a value (redness). There was no significant difference among the meatball samples with respect to sensory properties, and all samples had high acceptability.     

不同栓塞剂治疗肝巨大海绵状血管瘤的疗效

【摘要】 目的 探讨不同栓塞剂治疗肝巨大海绵状血管瘤中的疗效。方法 2008—2010年经诊断明确的肝海绵状血管瘤30例,行介入栓塞治疗,根据栓塞剂不同分为两组,即平阳霉素碘油乳剂（PLE）联合海藻酸钠微球（KMG）组（A组,15例）及（PLE）组（B组,15例）,术后1、3、6、12 个月进行CT 检查以评价疗效。结果 两组术后成功率均达100%,A、B两组所用PLE剂量分别为（10.9 ± 5.2）ml、（11.4 ± 4.9）ml,两者差异无统计学意义（P > 0.05）,术后第1、3、6个月复查CT,A组瘤体缩小率在50%以上者为分别为9、11、14例,B组分别为0、3、5例（P < 0.05）。术后1周A组患者疼痛较B组明显,差异有统计学意义（P < 0.05）,术后两组部分患者有轻度肝功能异常,主要表现在转氨酶升高,对症处理后恢复正常,经问卷随访A组满意度较B组高。结论 经肝动脉注入PLE治疗肝巨大血管瘤安全、有效, PLE联合KMG组瘤体缩小主要集中在术后第1、3个月内,见效快,但疼痛较PLE组明显。     

Determination of industrial pollution effects on citrus honeys with chemometric approach

The aim of this study was to determine the levels of essential, trace and toxic elements, such as K, Ca, Fe, Cu, Al, Ni, Sn, Pb and Cd in citrus honeys from different regions (industrialized and nonindustrialized) of Hatay, Turkey. K, Ca, Na and Mg were the most abundant elements, with mean contents of 363.5, 256.6, 88.1 and 37.7 mg/kg, respectively. The trace element mean contents ranged between 0.032 and 15.58 mg/kg. Significant differences in Fe, Cu, Al, Ni, Sn, Pb, Cd, Co and Sr levels were observed between two different regions. The findings that Fe, Cu, Al, Ni, Sn, Pb, Cd, Co and Sr contents in citrus honeys from industrialized regions were higher than citrus honeys from non-industrialized regions indicate that the honeys were affected by industrial pollution. Chemometric methods were applied to classify honey according to mineral content. Cluster analysis showed three clusters corresponding to the three different regions.     

米曲霉菌今野菌株所产蛋白酶性质的研究

采用(m)2SO4盐析,再透析提纯得到今野菌株的蛋白酶,该酶热稳定性好,40℃保温5小时,剩余酶活为54%,采用正交试验,得其在反应过程中所受因素影响大小为pH＞酶液浓度＞底物浓度＞温度.酶反应的最适pH为7.0,最适温度为40℃.在以酪素为底物时,该蛋白酶的Km值为6.6‰,NaCl对其有抑制作用.抑制类型为非竞争性抑制.     

The effect of magnetic field on the impurity binding energy of shallow donor impurities in a Ga1?xInxNyAs1?y/GaAs quantum well

Using a variational approach, we have investigated the effects of the magnetic field, the impurity position, and the nitrogen and indium concentrations on impurity binding energy in a Ga_1−xIn_xN_yAs_1−y/GaAs quantum well. Our calculations have revealed the dependence of impurity binding on the applied magnetic field, the impurity position, and the nitrogen and indium concentrations.     

渤海湾盆地东营—惠民凹陷油气成藏模式和油气富集控制因素

东营凹陷和惠民凹陷作为济阳坳陷南部两个相邻的、构造格局相似的陆相箕状断陷,其石油地质特征有相似之处,但油气富集程度有明显差异。控制油气富集的主要因素有油源条件、构造特征、火山活动以及生储盖组合与构造的配置等。生储盖组合与构造特征的配置,是造成不同构造部位主要储油气层位和油气藏类型差异性的直接原因。结合油源特征、生储盖组合和输导系统特征,东营、惠民凹陷的油气成藏模式可归为5种类型:洼陷带自生自储-侧向运移成藏模式、洼陷区上生下储-垂向运移成藏模式、中央隆起带和北部陡坡带下生上储-垂向运移成藏模式、南部斜坡带下生上储-复合运移成藏模式和周边凸起区新生古储-复合成藏模式。