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91.
水热法合成SnO2微球的酒敏特性研究 总被引:1,自引:0,他引:1
采用分析纯的SnCl4 ·5H2O和NaOH为起始原料,在160 ℃温度条件下水热法反应12 h得到SnO2微球.利用X射线衍射仪(XRD)、扫描电镜( SEM)对合成材料的结构、尺寸和形态进行了表征;采用静态配气法测试了材料的气敏性能.研究结果表明:在160 ℃水热条件下一步合成了均分散的SnO2微球,粒径大约为200 nm.用其制作的旁热式气敏元件在5 V工作电压下对0.005%的C2H5OH的灵敏度为8.7,达到了口腔酒精气体浓度检测限度0.008%的要求,并且响应-恢复特性良好. 相似文献
92.
《Chemical engineering science》1986,41(8):2193-2195
Exact relationships are given for the enhancement of gas absorption rate as a function of particle size in a three-phase slurry reactor. The solid-liquid mass transfer in the liquid film at the gas-liquid interface is considered as a transfer through spherical surface. The solid phase is the catalyst or reactant. The enhancement of the gas absorption rate calculated by the given equations are in very good agreement with the experimental data as a function of particle size and solid phase concentration. 相似文献
93.
《Combustion and Flame》1986,65(2):127-135
The IR spectra of the monomers and homopolymers of glycidyl azide (GAP), 3-azidomethyl-3-methyloxetane (AMMO), 3,3-bis(azidomethyl)oxetane (BAMO), 3-azidooxetane (AZOX), and 3-(2,3-diazidopropoxymethyl)-3-methyloxetane (DAPMMO) were assigned. Rapid-scanning Fourier transform infrared spectroscopy (10 scans s−1) was used to characterize the slow (5K min−1) and rapid thermolysis (50–255K s−1) of these compounds. The azide group decomposes before the polymer backbone does. However, once decomposed the products are essentially a mixture of those expected of low-membered cyclic ethers and methyl azide. The gaseous decomposition product concentrations are strikingly insensitive to the applied pressure (1–1000 psi Ar) and to the heating rate (50–255K s−1). HCN is the dominant IR active product in all cases except for AMMO monomer, where CO is more abundant. AMMO polymer is the most thermally stable of the polymers. 相似文献
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Birnessite-type MnO2 nanoparticles are synthesized by mixing KMnO4 solution directly with ethylene glycol under ambient conditions. When cobalt exists in the solution, the micro-morphology of the products transforms from conglomeration to dispersive state. The result of transmission electron microscopy (TEM) and field emission scanning electron microscopy (FE-SEM) shows that the product is constructed with nanosphere in sizes of ca. 40 nm. These nanospheres are twisted by nanorods clusters. X-ray diffraction (XRD) pattern shows that the products are birnessite-type. The electrochemical properties of the prepared materials are studied using cyclic voltammetry (CV) and galvanostatic charge–discharge test in aqueous electrolyte. The product shows a very high specific capacity of 326.4 F g−1. These results indicate that cobalt has great effects on the micro-morphology and electrochemical properties of manganese dioxide. 相似文献
97.
《Combustion and Flame》1986,64(1):65-81
In this paper we describe our measurements of the soot particle inception (“nucleation”) rate in an atmospheric pressure premixed flat flame. After demonstrating that interfering optical signals from molecules in the flame could be eliminated or accounted for, we were able to use laser light scattering and extinction to detect the soot particles. An aerosol dynamics model was developed to allow interpretation of the optical data, and an efficient technique was found to solve the differential equations. From their solutions we determined that the soot particle inception rate in our flame peaked near 1016 cm−3 s−1. Net surface growth during the particle inception process was close to zero, possibly because the soot was also being oxidized. The particle inception process lasted for about 2.5 ms. We carried out a sensitivity analysis to evaluate the effects of uncertainty in the properties of incipient particles. 相似文献
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Haiyuan Ren Jinrui Li Ai Peng Ting Liu Mengjun Chen Hongguang Li Xiaojing Wang 《International journal of molecular sciences》2022,23(10)
As carbon-based nanomaterials, water-soluble C60 derivatives have potential applications in various fields of biomedicine. In this study, a water-soluble fullerene C60 derivative bearing alanine residues (Ala-C60) was synthesized. The effects of Ala-C60 on neural stem cells (NSCs) as seed cells were explored. Ala-C60 can promote the proliferation of NSCs, induce NSCs to differentiate into neurons, and inhibit the migration of NSCs. Most importantly, the Ala-C60 can significantly increase the cell viability of NSCs treated with hydrogen peroxide (H2O2). The glutathioneperoxidase (GSH-Px) and superoxide dismutase (SOD) activities and glutathione (GSH) content increased significantly in NSCs treated even by 20 μM Ala-C60. These findings strongly indicate that Ala-C60 has high potential to be applied as a scaffold with NSCs for regeneration in nerve tissue engineering for diseases related to the nervous system. 相似文献