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《Journal of the European Ceramic Society》2005,25(2-3):129-135
A poly(aminoborazine), precursor for hexagonal boron nitride (h-BN) obtained by reaction of borazine B3N3H6 with ammonia, and its pyrolysis derivatives have been extensively characterised by 15N and 11B MAS NMR. The various B and N sites have been identified according to their first neighbouring atoms, as well as to the second ones in the case of 15N, and have also been quantified. This study demonstrates that a suitable choice of NMR techniques together with the use of isotopic enrichment can lead to a large improvement in spectral resolution, which allows a better understanding of such complex BN preceramic polymer structures and permits to follow the polymer-to-ceramic transformation. 相似文献
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《Applied Catalysis A: General》2005,278(2):213-221
Highly loaded supported (Ni)Mo sulfide catalysts prepared using different methods have been studied. Two zirconia supports of high specific surface area were used, including amorphous or tetragonal ZrO2 solids. The order of active components introduction as well as thermal treatment conditions were varied. The best performance in the reactions of hydrodesulfurisation of thiophene and hydrogenation of tetralin was shown by the coimpregnated systems sulfidized without calcination of the oxide precursor. Crystallized ZrO2 support always provides higher activities in both reactions, than amorphous zirconia, despite very high specific surface area of the last. The differences between variously treated systems were explained using the results of characterizations including laser Raman spectroscopy, XPS spectroscopy and temperature programmed reduction. 相似文献
246.
《Materials Letters》2007,61(11-12):2259-2261
We report the formation of silver nanoclusters of average size ∼ 1.1 nm in a single step ion-exchanged silica glass. Silver clusters are formed in a glass during ion-exchange by fine-tuning the ion-exchange parameters such as salt composition, temperature and time. Such nanocluster formation during ion-exchange preserves the waveguiding properties of the ion-exchanged surface of the glass making them suitable for nonlinear waveguide device fabrication. 相似文献
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Shuichi Yamamoto Teruaki Morihiro Koichi Ariyoshi Turkan Aktas 《Drying Technology》2005,23(6):1319-1330
As the surface properties of the drying materials are very important not only for the drying rate but also for the quality change during drying, the effects of surface concentration on the drying behavior of liquid foods (sugar solutions) were investigated by isothermal drying experiments and by numerical calculation experiments. The isothermal drying experiments with gelled sugar solution systems (sucrose and maltodextrin) were carried out at various relative humidity (RH) values (RH = 0 to 84%). Separate experiments were carried out for determination of the desorption isotherms.
The isothermal drying curves of sugar solutions at RH = 0 to 51% were very similar. Numerical simulations also showed that the drying curves of these sugars at the surface concentration = 0 and 0.1 are almost the same, although the concentration distributions are different.
When a small amount of gelatin was added to sugar solutions, the drying rate decreased remarkably as the gelatin might form a thin film (skin) near the surface, and consequently the retention of ethanol increased. 相似文献
The isothermal drying curves of sugar solutions at RH = 0 to 51% were very similar. Numerical simulations also showed that the drying curves of these sugars at the surface concentration = 0 and 0.1 are almost the same, although the concentration distributions are different.
When a small amount of gelatin was added to sugar solutions, the drying rate decreased remarkably as the gelatin might form a thin film (skin) near the surface, and consequently the retention of ethanol increased. 相似文献
250.
《Diamond and Related Materials》2005,14(1):113-120
This paper reports on the behavior of electron field emission from diamond thin films at elevated temperatures. The study is motivated by the possibility of using these structures in high temperature electronics or direct energy conversion processes. Three diamond samples were tested: nanocrystalline diamond, crowned diamond tips, and peaked diamond tips. All samples displayed moderately efficient field emission characteristics. For each of the samples, the onset of field emission decreased as the sample temperature increased. Temperature effects, interpreted through advanced parameter estimation techniques, were shown to have a small influence on the estimated work function between 300 and 700 K, except for the peaked tip sample, whose estimated work function became very large at the highest temperature. Emission areas were also estimated and revealed similar trends to that of work function. 相似文献