L、T形柱轴压比限值研究

对T、L形柱轴压比限值进行了深入的研究,指出T、L形柱轴压比限值与截面尺寸有关;并针对T、L形柱当腹板受压时轴压比限值很低,在实际工程设计中很难实现这一现象,提出了提高轴压比限值的方法,考虑增加腹板端部配筋和箍筋约束混凝土作用的有利影响,对T、L形柱轴压比限值进行了电算分析。得出了以下主要结论:T、L形柱肢长、厚比越大,轴压比限值越低;增加腹板端部配筋对T、L形柱轴压比限值有所改善;考虑箍筋约束混凝土作用对轴压比限值有明显提高。最后给出了考虑肢长、厚比不同的T、L形柱轴压比限值。     

Modeling of Solidification Microstructures Based on Fully Coupling of Macro-transport Phenomena with Cellular Automata

This paper has attempted to simulate the microstructure formation based on fully coupling of temperature field, concentration field and velocity field with micro-kinetics. The authors presented a new way, which is the combination of FDM and cellular automata (CAFD) to visualize the microstructure formation of the thin complex superalloy turbine blades cast by the vacuum investment process. The distribution, orientation and mechanism of the heterogeneous nucleation, the growth kinetics of dendrites and the columnar to equiaxed transition (CET) are considered. Capitalizing on these simulating schemes, the comprehensive influence of key process variables on the scale and uniformity of grains has been investigated quantitatively. The simulated grain size and morphology agree well with the experimental results.     

回转窑焙烧钼精矿技术及设备

叙述了采用内燃式回转窑焙烧钼精矿的技术特点以及系统技术参数选择与配套方式，对提高和改变目前国内钼精矿焙烧现状，提供了具有实际参考价值的数据和配套设备。     

Fe-Al和Fe-Cr-Al合金在高温下的初期氧化

研究了Fe-10Al、Fe-5Cr-10Al和Fe-10Cr-10Al分别在900℃和1 000℃的初期氧化行为.利用电子显微镜(SEM)和俄歇电子谱(AES)分析了合金表面形成氧化膜的形貌与组成.Fe-Cr-Al实现铝的选择性氧化所需的时间取决于合金中铝和铬的质量分数,同时也与氧化温度有关,较高的反应温度能促进铝的选择性氧化.Fe-10Cr-10Al比Fe-5Cr-10Al更快地实现铝的选择性氧化,而Fe-5Cr-10Al在1 000℃比在900℃更快实现铝的选择性氧化.     

A Study on Crystal Defects in Epitaxial GaN Film by High-Order Weak-Beam Electron Microscopy

Various crystal defects in epitaxial GaN film were studied by high-order bright-field and dark-field electron microscopy. The results revealed that the film is composed of small grains in nano-meter scale. Distinct shapes of the grain boundaries and a great number of threading dislocations were shown in the experimental g/3g weak-beam images. Diffraction contrast analysis verified that the majority of threading dislocations is 1/3<11 0> edge dislocation. A unique (11 0) planar defect was observed in the specimen. The defect was identified to have a similar structure to the incipient 1/3[11 0] edge dislocation.     

Environmental and internal hydrogen embrittlement of a directionally solidified Ni-rich Ni3AI intermetallics

The influence of tensile orientation, test environments and internal hydrogen contents on the room temperature tensile properties of a directionally solidified Ni₃Al alloy was investigated. The specimens parallel to the growth direction exhibited a good ductility and little susceptibility to test environment. The values of elongation in vacuum, air and H₂ are 39.7%, 39.2% and 29.7%, respectively. Also, a transgranular fracture mode was observed in the specimens. However, the specimens perpendicular to the growth direction exhibited lower ductility, much more sensitivity to test environment and intergranular fracture mode. The elongation values in vacuum, air and H₂ are 13.7%, 10.3% and 3.3%, respectively. The results indicate that the cohesive strength of grain boundaries in the alloy is low and they are more susceptible to test environment than are grain interiors. In addition, only a slight embrittlement of the internal hydrogen was found in the specimens parallel to the growth direction.     

Pure mechanical wear loss measurement in corrosive wear

The method for the measurement of the pure mechanical wear loss for 321 stainless steel, 1045 steel and pure iron in the study of the synergy between corrosion and wear was studied. The methods studied included the measurement in distilled water, by cathodic protection and by adding inhibitor KI, and all were compared with the wear loss in air. The experiment showed that the pure mechanical wear losses and friction coefficients obtained by the three methods were close to each other and can be used to calculate the various wear components in the study of the interaction of corrosion and wear, but the measurements in distilled water for pure iron and 1045 steel are not recommended due to their corrosion     

Temperature fluctuation/hot pressing synthesis of Ti3SiC2

A novel temperature fluctuation synthesis and simultaneous densification process for the preparation of Ti₃SiC₂ was developed. The advantages of this novel method include low synthesis temperature, short reaction time and simultaneous densification. The microstructure and room temperature mechanical properties of the Ti₃SiC₂ synthesized using this method were investigated. The result demonstrated that the Ti₃SiC₂ ceramic consisted of mainly laminated grains. It was found, with the aid of computer simulated crystallite shape, that the laminated Ti₃SiC₂ grains were composed of thin hexagonal plates. These laminated grains characterized the Ti₃SiC₂, and were responsible for the mechanical properties of the polycrystalline Ti₃SiC₂ ceramic. The measured flexural strength and the fracture toughness were 470 ± 26 MPa and 7.0 ± 0.2 MPa·m^1/2, respectively. The high toughness was attributed to the contribution of crack deflection, crack bridging, delaminating and grain pull-out of laminated Ti₃SiC₂.     

Solidification and interfacial structure of in situ Al-4.5Cu/TiB2 composite

In situ particle reinforced Al-4.5Cu/TiB₂ composite was fabricated with TiO₂, H₃BO₃, Na₃AlF₆ powders and Al-4.5Cu alloy by reaction in melt. The composite can be directly casted into moulds to make composite parts. TiB₂ particles distribute uniformly in the matrix. The average size of TiB₂ particles is 0.93 m. At the atomic scale, TiB₂ is hexagonal, and exhibits hexagon or quadrilateral shape. The orientation relationships exist in the interfaces between TiB₂ particle and -Al, and between the reinforced small Al₂Cu phase and -Al in the composite. They are . TiB₂ particle is nucleation site for -Al matrix growth in the composite. The interface between TiB₂ particles and the matrix is clean and well bonded. No reaction product has been found through HREM observation. This is beneficial to the strength of the composite. The as-cast Al-4.5Cu/TiB₂ composite exhibits mechanical excellent properties: the tensile strength is 416.7 MPa, the yield strength is 316.9 MPa, and the elongation is 3.3 pct.     

Properties of Reactive Magnetron Sputtered ITO Films without in-situ Substrate Heating and Post-deposition Annealing

1. Introductiontransparent conductive indium tin oxide (ITO)films have been extensively used in a variety of electronic and opto--electronic applications because oftheir high transmission in the visible range, high infrared (IR) reflection, and low electrical resistivity.A variety of deposition techniques have been appliedto fabricate ITO films such as CVD, spray pyrolysisand sputteringll'2]. However, sputtering is the mostextensively used technique especially in industry. Recelltly, targe…