自卸车驾驶室振动对标测试与分析

针对某厂商研制的无副梁自卸车,为验证其更换主梁后驾驶室舒适性是否有所改善,进行不同速度及路况下的驾驶室振动测试试验,并与有副梁原型自卸车进行对标,采用时域与频域数据处理方法对结果进行分析,结果显示扭曲路面下无副梁自卸车的驾驶室舒适性有所改善,但对于4Hz以下的振动,其车架的隔振效果较弱。在碎石路面与平坦路面下无副梁自卸车满载时,其车架的隔振效果要明显好于对标自卸车,但在碎石路面空载时,其隔振效果则较弱。     

用于较大水平位移测量的电阻应变式位移传感器

针对目前位移传感器很难直接测得木结构或木构件在转动中产生较大绝对水平位移的问题,研制了量程为±500 mm的电阻应变式位移传感器（WD位移传感器）,应用正交试验法分析WD位移传感器的影响因素,并对其进行设计与制作,拟合了传感器在不同量程下应变位移的分段函数关系,通过计算得出了WD位移传感器的6种静态参数指标。试验结果表明,WD位移传感器克服了传统电阻应变式位移传感器量程小的问题,解决了木结构或木构件发生非直线运动很难直接测得绝对水平位移的问题,且各静态参数指标良好。     

Refinement mechanism of in-situ Al4C3 particles on AZ91 magnesium alloys

The effects of SrCO3 on the microstructure of AZ91 magnesium alloy were investigated by OM, SEM, EDS, XRD and DTA analyses. The results show that AZ91 magnesium alloy with 1.0% SrCO3 addition has the best refining effect at 730 ℃ for 20 min, the average size of the α-Mg grain in AZ91 matrix alloy is reduced from about 91 μm to 58 μm, with reduction of about 36%. Based on the analysis results of EDS, binding energy, and Gibbs free energy, it is evident that the grain is refined because of the generation of A14 C3 particles which can be used as the crystal nucleus of the magnesium alloy when SrCO 3 is added. Owing to the generation of A14C3 in AZ91 magnesium alloy, the grain boundary is pined and the grain growth is inhibited. In the accession to the Al4C3, small subcooling temperature difference leads to the formation of fine grain microstructure in alloy melt. Fine grain microstructure in AZ91 alloy melt with the addition of SrCO3 can be obtained on the condition of lower undercooling temperature according to the DTA analysis results.     

MoO3/SO4^2- —TiO2 catalyst for transesterification of dimethyl cabonate with phenol

A new MoO3/SO4^2- -TiO2 catalyst was prepared by a conventional impregnation of SO42-/TiO2 as carrier with an aqueous solution of ammonium molybdate and used for the synthesis of transesterification of dimethyl carbonate （DMC） with phenol.A series of MoO3/SO42--TiO2 catalysts with different MoO3 loadings were investigated and characterized using X-ray diffraction （XRD）,Fourier transform infrared spectrometer （FTIR）,NH3-temperature programmed desorption （NH3-TPD） and X-ray photoelectron spectroscopy （XPS）.The results show that MoO3 loading is related to the activity of transesterification reaction.With the increase of MoO3 loading,the activity of transesterification reaction increases.The sulfur species in the catalyst have an influence on the molybdenum species,and lead to an increase in the electropositive of molybdenum,which promotes the catalytic activity of MoO3/SO42--TiO2.Among the series of catalysts prepared,MoO3/SO42--TiO2 with 10% MoO3 and 823 K calcinated is found to be the most active catalyst for transesterification reaction.Under the reaction conditions of 453 K and 12 h,the conversion of DMC is 30.5 %,and the yields of MPC and DPC reach 21.2 % and 8.7 %,respectively.     

Engineering oxygen vacancy-rich Co3O4 nanowire as high-efficiency and durable bifunctional electrocatalyst for overall alkaline water splitting

A novel kind of vacancy-rich nanowire arrays were prepared by reducing rough Co₃O₄ nanowires with NaBH₄ solution on 3D nickel foam at room temperature for overall water splitting. Co₃O₄/NF treated by NaBH₄ for 10 min was highly active for oxygen evolution reaction (OER) and simultaneously efficient for hydrogen evolution reaction (HER) with the need of the overpotentials of 240 and 132 mV to drive 10 mA·cm^-2 in alkaline media, respectively. Furthermore, the electrocatalysts as both cathode and anode in a two-electrode system presented excellent durability for over 60 h at 10 mA·cm^-2, maintaining the cell voltage of merely 1.63 V. This work provides new methods and ideas for the preparation of transition metal oxide bifunctional electrocatalysts rich in oxygen vacancies.     

真空熔炼AZ91镁合金过程中Mg元素的蒸发行为

在真空Ar气氛中熔炼AZ91镁合金，测定了不同精炼温度下Mg元素的蒸发速率。结果表明，随着精炼温度的升高，Mg元素的蒸发量增大。通过计算可知，Mg的蒸气压是Al的10^9倍，是Zn的46倍，因此主要是Mg的蒸发而导致合金其他元素含量升高。XRD分析表明，蒸发物是Mg元素。结合Mg元素的蒸发机制，在该试验条件下推导出Mg元素蒸发率的计算公式以及Mg元素的表观传质系数、蒸发率与精炼温度的关系，计算得出Mg元素蒸发率为0．86×10^-3-1．35×10^3g／cm^2·s，Mg元素的表观传质系数在2×10^-5-24×10^-5cm／s范围内。     

Effects of silicocalcium on microstructure and properties of Mg-6Al-0.5Mn alloy

1 Introduction Magnesium alloys are attractive for applications in the automobile, aerospace and electronic industries due to their light mass, high stiffness, high specific strength, good dimensional stability and damping capacity. It is the lightest sp…     

铝合金激光焊接的工艺特点及发展现状

概述了铝合金激光焊接的工艺特性及难点，提出改进措施，并指出了铝合金激光焊接技术的研究现状及未来的发展方向。     

热轧厚规格窄带钢厚度控制策略优化

针对某450 mm窄带钢生产线生产6.00 mm以上厚规格产品时带钢扭转导致测厚仪产生厚度测量偏差，严重影响厚度自动控制系统的正常投用，对产品厚度控制精度产生影响的问题，通过对轧件扭转前后轧件厚度的比较，实现了6.00 mm以上厚规格产品的厚度测量补偿，以此为基础实现了厚度的精确控制。现场实际生产应用表明，6.00 mm以上厚度规格96%以上达到了±50 μm的厚度控制精度，有效地保证了产品质量。     

晋东北金矿床石英流体包裹体与找矿

晋东北各种类型金矿中都广泛发育热液型石英脉，与矿化有关的石英流体包裹体的特征反映了不同的矿床类型。对该区石英脉型、蚀变岩型及磁铁石英岩型金矿床的研究表明，石英中流体包裹体的成分、温度和红外吸收光谱等特征可以作为划分矿床类型和作为金矿找矿评价的标志