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《Journal of the European Ceramic Society》2005,25(2-3):123-127
Ceramic fibers with compositions in the system Si–C have a great potential for high-temperature applications. In recent years, our efforts have been dedicated to the development of polymers consisting of polysilanes suitable to spin fibers and build up matrices for CMC as well. The polysilanes are synthesized via disproportionation of the so-called disilane fraction [Richter, R., Roewer, G., Böhme, U., Busch, K., Babonneau, F., Martin, H.-P. et al., Appl. Organomet. Chem., 1997, 11, 71 (and references cited therein)]. A further thermal treatment yields materials which are soluble in organic solvents, and these solutions can be dry-spun to give fibers which are subsequently pyrolyzed. Solubility and high ceramic yield make this precursor a promising candidate for matrix infiltrations, too. The chemistry and the adjustment of viscosity and solubility to the requirements of the fiber processing as well as the conversion of the dried fibers to pure SiC fibers by thermal treatment will be reported. 相似文献
23.
《Journal of the European Ceramic Society》2005,25(2-3):129-135
A poly(aminoborazine), precursor for hexagonal boron nitride (h-BN) obtained by reaction of borazine B3N3H6 with ammonia, and its pyrolysis derivatives have been extensively characterised by 15N and 11B MAS NMR. The various B and N sites have been identified according to their first neighbouring atoms, as well as to the second ones in the case of 15N, and have also been quantified. This study demonstrates that a suitable choice of NMR techniques together with the use of isotopic enrichment can lead to a large improvement in spectral resolution, which allows a better understanding of such complex BN preceramic polymer structures and permits to follow the polymer-to-ceramic transformation. 相似文献
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Dong Zhang 《Korean Journal of Chemical Engineering》2008,25(5):1205-1207
Ceria-zirconia solid particles have been recognized as a key material of the automotive exhaust catalysts since they can release
and uptake oxygen owing to the rapid reversible oxidation states of cerium between Ce3+ and Ce4+. Several methods have recently been described to prepare the CeO2-ZrO2 solid particles used in the catalysts. In this paper, a new coprecipitation method is used to prepare the CeO2-ZrO2 solid particles. The Ce-Zr alcogel is dried and calcined in flowing N2 not in flowing air under atmospheric pressure. The results show that the ceria-zirconia sample calcined at 650 °C has high
surface area over 90 m2g−1, which drops to 40 m2g−1 following treatment at 900°C. 相似文献
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《Journal of the European Ceramic Society》2005,25(6):857-862
Compressive creep tests in air were carried out on 1 cat.% Fe-doped alumina at a temperature T=1400 °C. Iron doping affected the plastic deformation by different ways in relation with Fe2+ cations population. Fe2+ cations sped up the deformation rates. FeAl2O4 spinel precipitates were identified and they were found (i) to interact with alumina grain boundaries (ii) to limit the grain growth within a range of strain. The Fe2+ cations underwent oxidation and this resulted in the dissolution of the some precipitates and in the decrease of deformation rates. It was suggested that deformation sped up this evolution through mass transport and that time was not a dominating parameter. 相似文献
28.
《Journal of Systems Architecture》2007,53(5-6):263-271
Configurable processors have emerged as a promising solution for high performance embedded systems. Many of these processors extend a RISC core with configurable functional units that execute dual-input, single-output (DISO) custom functions. Although studies have shown that supporting multiple-input, multiple-output (MIMO) custom functions can lead to significant speedups, mechanisms to efficiently achieve this have not been adequately addressed. The underlying reason is that a custom function is normally invoked by a single instruction, which usually transfers only two inputs and one output. Attempts to transfer more inputs and outputs in one instruction are impeded by the instruction length and the register file’s R/W ports. This paper proposes a simple extension to transfer multiple inputs and outputs of the custom functions using repeated instructions. While transferring the inputs and outputs may take a few extra cycles, our experiments show that the MIMO extension can still achieve an average 51% increase in speedup compared to a DISO extension and an average 27% increase in speedup compared to a multiple-input, single-output (MISO) extension. 相似文献
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《钢铁研究学报(英文版)》2006
Being a new permanent magnets(PMs) arrangement, the Halbach array could approve the magnetic flux density effectively, through weakening the magnetic flux density in one side of the PMs array, meanwhile strengthening the magnetic flux density in the other side. In the disk coreless PM synchronous motor (PMSM), the magnetic flux density is required to be sine wave and the peak value should be as high as possible. The paper deals with the application of the 90° Halbach array in the disk coreless PMSM, adopting NdFeB PMs. For the thickness of PMs influences the magnetic flux density in the air gap, the thickness variation technology is adopted. Through altering the adjacent PMs thickness, nine different PMs thickness combination is analyzed by FEM methods. And the conclusion is that when the thickness of tangential magnetization PMs is great than that of the radial magnetization PMs, the magnetic flux density wave is closer to sine wave than when the thickness of the tangential magnetization PMs is smaller than that of the radial magnetization PMs. Furthermore, when the thickness of the tangential magnetization PMs is great than that of the radial magnetization PMs, keeping the thickness of the tangential magnetization PMs being 0.006 m and the thickness of the radial magnetization PMs variation from 0.0048 m to 0.006 m, the magnetic flux density in the air gap will become closer to sine wave gradually, and then it becomes nonsinusoidal again. And when the thickness of radial magnetization PMs is 0.0054 m and 0.0055 m, the waves of magnetic flux density in the air gap are better than others. 相似文献