SOFC单电池局部性能的评价与测试

为了制备高性能大面积固体氧化物燃料电池(SOFC)单电池,解决由于面积过大而导致的单电池上气体分配不均匀及各部分温度差异,通过实验设计测试了单电池的各个区域的性能,包括局部电性能和局部温度.实验在1片10cm×10cm(有效反应面积9cm×9cm)的阳极支撑SOFC单电池上进行,电池的阴极以及空气气体分配板和集流器都被...     

γ射线辐照对Cu/LDPE纳米复合材料的影响

采用不同剂量的γ射线对Cu/LDPE进行辐照,并对复合材料的铜离子释放速度、力学性能、浸润性、自由体积等进行了分析。结果表明,辐照剂量不同,铜离子的释放性能发生较大改变;随辐照剂量的增加,拉伸强度先增大后减小,而材料的断裂伸长率和接触角持续减小,并初步探讨了实验结果。     

一种光固化3DP实体材料树脂

为研究紫外光固化三维打印(3DP)的成形技术及成形材料,制备了一种实体材料光敏树脂。使用实时傅立叶红外光固化实验研究了这种实体材料中主要成分在室温和55℃时的光固化速度;考察了黏度、表面张力及工作温度对实体材料可打印性的影响;在喷头为XAAR500的三维打印实验机上,测试了实体材料的打印稳定性和成形精度。结果表明,这种实体材料在55℃时可持续稳定地从喷头喷出,光固化速率和精度符合要求。     

橡胶辅助增压在非热压罐成型工艺中的应用研究

目的 针对蒙皮带筋典型构件,在容易产生孔隙的加强筋底部放入橡胶增压,以优化应力场、减小孔隙缺陷。方法 针对CFRP固化成型制度,进行红/蓝2种橡胶模量、热膨胀系数测试及双马树脂流变测试。基于材料测试数据及预浸料固化特征建立了固化前中后3类数值仿真模型,以对比不同橡胶在不同固化时期的增压效果。结果 在固化前期,红、蓝橡胶均有增压作用,可使加强筋底部应力提高约5倍;在固化中期,红橡胶有显著增压作用,可使加强筋底部应力提高约9倍并改善应力梯度;在固化后期,橡胶难以发挥增压作用。结论 红橡胶可显著发挥增压作用,有效解决加强筋固化成型前中期底部应力不足的问题;在CFRP固化前期,热膨胀系数是影响热应力的主要因素,在固化后期,模量为主要因素。通过对比多组仿真数据,明确了最优增压材料及最主要的材料属性,为解决OOA成型局部压力不足的问题提供了指导方向。     

铝基非晶合金的制备、性能与应用研究进展

铝基非晶合金因其独特的物理和化学性能在诸多领域具有广泛的应用前景,综述了铝基非晶合金的成分体系、制备方法、性能特点及应用研究进展。首先,介绍了铝基非晶合金的发展历史和成分体系,目前铝基非晶主要分为3大体系：二元、三元和多元体系,以及综合性能和形成能力2大方面,多元体系表现更佳,并逐渐向更多元化发展;其次,系统介绍了铝基非晶合金的制备方法,包括粉末状、薄带状、块体样品的制备,相较于非晶薄带的制备,块体和粉状的制备方法较为丰富,而粉状非晶通常作为铝基非晶涂层的预制材料;随后,详细介绍了铝基非晶合金的性能特点、应用现状及发展趋势,从性能上来看,铝基非晶在强度和硬度以及耐腐蚀性能上表现良好,目前主要以涂层的形式参与应用,除此之外,研究者们也开始对磁性和热塑性展开研究,由于玻璃形成能力的限制,作为结构材料的应用较少;最后,对其未来应用前景进行了展望,认为涂层是目前铝基非晶合金最具应用前景的工程化方式。     

适于中小型冲床的经济型自动送料机械手研制

在分析目前中小企业冲压产业现状的基础上,对现有国内外冲床送料机构进行了分类汇总并予以比较评估,介绍了与某企业合作研制的一种适合中国中小型冲压生产企业的新经济型自动送料机械手,并对机械手结构进行说明.通过对机械手运动过程及运动原理的分析,得出计划性能指标,通过在企业中的应用,得出实际应用指标及性价比.最后,对由该机械手组...     

Effect of microstructural parameters on the properties of W-Ni-Fe alloys

The aim of this research was to examine the effect of microstructural parameters on the tensile properties of dif- ferent compositions of tungsten heavy alloys. The microstructural parameters (grain size, connectivity, contiguity, and solid volume fraction) were measured and were found to have a significant effect on the tensile properties of tungsten-based heavy alloys. The microstructural parameters of W-Ni-Fe alloys are sufficiently different to present a range of me- chanical properties. It is concluded that the mechanical properties of tungsten heavy alloys largely depend on the micro- structural parameters and their ductility is particularly harmed when grains are contiguous.     

Electrodeposition and characterization of Bi2Se3 thin films by electrochemical atomic layer epitaxy (ECALE)

Bismuth selenide thin films were grown on Pt substrate via the route of electrochemical atomic layer epitaxy (ECALE) in this work for the first time. The electrochemical behaviors of Bi and Se on bare Pt, Se on Bi-covered Pt, and Bi on Se-covered Pt were studied by cyclic voltammetry and coulometry. A steady deposition of Bi₂Se₃ could be attained after negatively stepped adjusting of underpotential deposition (UPD) potentials of Bi and Se on Pt in the first 40 deposition cycles. X-ray diffraction (XRD) analysis indicated that the films were single phase Bi₂Se₃ compound with orthorhombic structure, and the 2:3 stoichiometric ratio of Bi to Se was verified by EDX quantitative analysis. The optical band gap of the as-deposited Bi₂Se₃ film was determined as 0.35 eV by Fourier transform infrared spectroscopy (FTIR), which is consistent with that of bulk Bi₂Se₃ compound.     

Preparation of PZT suspensions for direct ink jet printing

The present paper contains an experimental study of two different kinds of PZT suspensions for direct ink jet printing at 25 and 120 °C, respectively. The effect of processing parameters such as mixing time, the amount of dispersant, solid loading and milling method was investigated for the optimisation of viscosity for feasible jetting. The viscosity of PZT suspensions was within 5–15 mPa·s range for room temperature suspensions with MEK/EtOH medium and 10–20 mPa·s for high temperature suspensions with wax medium. FTIR analysis is also presented to explain the rheological behaviour of PZT suspensions. Finally, a demonstration of room temperature jetting of PZT suspension is shown.