姜渣-玉米淀粉膜的制备及研究

目的 制备一种纯天然的、具有抑菌性的可食用淀粉膜。方法 以玉米淀粉为原料,通过添加适量的姜渣、甘油、羧甲基纤维素钠,采用流延法制备姜渣-玉米淀粉膜。结果 当淀粉的质量分数为3%,甘油的质量分数为1%,姜渣的质量分数为0.4%时,膜的透光性、透油性、水蒸气透过性、溶解度、溶胀度等各项指标的综合测定结果较好。生姜中含有姜辣素、姜油等活性成分,添加姜渣可作为天然的抑菌剂,微生物试验结果证实,姜渣-玉米淀粉膜对霉菌和酵母菌具有一定抑菌作用,且抑菌效果与姜渣的含量成正比关系。结论 所制备姜渣-玉米淀粉的结构紧密、光滑平整,并具有一定的抑菌性。     

Synthesis and electrochemical characteristics of LiCrxNi0.5−xMn1.5O4 spinel as 5 V cathode materials for lithium secondary batteries

A series of electrochemical spinel compounds, LiCr_xNi_0.5−xMn_1.5O₄ (x=0, 0.1, 0.3), are synthesized by a sol–gel method and their electrochemical properties are characterized in the voltage range of 3.5–5.2 V. Electrochemical data for LiCr_xNi_0.5−xMn_1.5O₄ electrodes show two reversible plateaus at 4.9 and 4.7 V. The 4.9 V plateau is related to the oxidation of chromium while the 4.7 V plateau is ascribed to the oxidation of nickel. The LiCr_0.1Ni_0.4Mn_1.5O₄ electrode delivers a high initial capacity of 152 mAh g⁻¹ with excellent cycleability. The excellent capacity retention of the LiCr_0.1Ni_0.4Mn_1.5O₄ electrode is largely attributed to structural stabilization which results from co-doping (chromium and nickel) and increased theoretical capacity due to substitution of chromium.     

Strengthening effect of unshearable particles of finite size: a computer experimental study

Equilibrium configurations of a dislocation interacting with randomly distributed unshearable obstacles of finite size under an applied stress are analyzed. Ashby's critical dipole spacing Q′ argument for the self-stress effect of dislocations is utilized but analysis suggests that the spacing Q′ varies with the local obstacle distribution as well as with the obstacle shape. Computer simulations of a dislocation slip process through circular or linear obstacles, that are extensions of earlier work by Forman et al., were conducted. The dependence of the strengthening stress on the obstacle size was found to be less than that predicted by equations currently in use, particularly for linear obstacles. New, modified Orowan equations are suggested for the strengthening effects due to spherical, rod-like, and plate-like obstacles. The effect of the orientation distribution of the linear obstacles demonstrated in the simulation is in agreement with recent experimental observations.     

Bilinear precision of rational Bézier surfaces

This short note proves the bilinear precision property of rational Bézier surfaces and gives a simple algorithm to compute the weights. Linear precision of rational Bézier surfaces is also discussed.     

Characterization of Hot Deformation Behavior of a Novel Al–Cu–Li Alloy Using Processing Maps

The isothermally compression deformation behavior of an elevated Cu/Li weight ratio Al–Cu–Li alloy was investigated under various deformation conditions.The isothermal compression tests were carried out in a temperature range from 300 to 500 °C and at a strain rate range from 0.001 to 10 s-1.The results show that the peak stress level decreases with temperature increasing and strain rate decreasing,which is represented by the Zener–Hollomon parameter Z in the hyperbolic sine equation with the hot deformation activation energy of 218.5 k J/mol.At low Z value,the dynamic recrystallized grain is well formed with clean high-angle boundaries.At high Z value,a high dislocation density with poorly developed cellularity and considerable fine dynamic precipitates are observed.Based on the experimental data and dynamic material model,the processing maps at strain of 0.3,0.5 and 0.7 were developed to demonstrate the hot workability of the alloy.The results show that the main softening mechanism at high Z value is precipitate coarsening and dynamic recovery;the dynamic recrystallization of the alloy can be easily observed as ln Z B 29.44,with peak efficiency of power dissipation of around 70%.At strains of 0.3,0.5 and 0.7,the flow instability domains are found at higher strain rates,which mainly locate at the upper part of processing maps.In addition,when the strain rate is 0.001 or 0.02 s-1,there is a particular instability domain at 300–350 °C.     

基于小波的信号分析

简介小波概念之后,对一组模拟信号进行分析,采用小波变换,选出合适的小波函数,处理后再重构。对采用Mexican hat小波、Shannon小波、Meyer小波这三种不同小波得到的去噪结果进行比较,验证信号的滤波效果与选取的小波类型有较大的关系。     

一种带负载电流前馈的双闭环逆变控制的在线式UPS(英文)

提出了一种带负载电流前馈的双闭环逆变控制的数字化在线式UPS。该控制方法提升了UPS系统性能,使得UPS输出的动态和稳态性能较优、可靠性较高;此外,主电路采用了单相半桥逆变器,与普通的全桥结构形式相比,有着它自身突出的优点。在建立了逆变器及其控制系统数学模型的基础上,分析了系统性能,并采用了M atlab/S imu link仿真工具对逆变控制系统进行了仿真,仿真结果表明UPS不仅可以实现稳压稳频的输出,且系统性能也得到了改善。     

超声辅助提取黑松松针多糖的工艺优化及其抑菌性研究

采用超声辅助水提法提取黑松松针多糖,苯酚-硫酸法测定提取的多糖含量。在单因素试验基础上,通过正交试验对黑松松针多糖的提取工艺进行优化。采用抑菌圈法考察了提取的松针多糖对大肠杆菌、枯草芽孢杆菌的抑菌效果。结果表明:松针多糖的最佳提取工艺条件为浸提时间2 h、液料比80∶1(m L/g)、浸提温度90℃、超声功率为130 W,在此条件下,黑松松针多糖得率为2.47%。提取的黑松松针多糖对大肠杆菌、枯草芽孢杆菌具有一定的抑制作用。     

基于余弦算子的红外热像仪自然伪彩色编码

介绍了传统的伪彩色编码算法,研究了余弦算子自然伪彩色编码算法,通过比较,得出了余弦算子优于传统编码算法的观点。     

Effects of alloying elements on the electrochemical behaviors of Al-Mg-Ga-In based anode alloys

In this study, in order to investigate the effects of alloying elements on the electrochemical behaviors of Al-based anodes, pure Al and Al-Mg-Ga-In alloys with different compositions (Al-0.25Mg-0.3Ga-0.3In, Al-1Mg-0.05Ga-0.15In and Al-2Mg-0.15Ga-0.05In (wt%)) were fabricated. The microstructure, corrosion behavior, electrochemical property, discharge performance and corroded morphology of the four experimental anodes were studied. Al-Mg-In-rich intermetallic compounds were observed in Al-Mg-Ga-In alloys. The results of the polarization curve and electrochemical impedance spectroscopy indicate that the addition of Mg acts as a critical component in improving the discharge activity of Al-based anode and contributes to a more negative electrode potential. According to the corrosion morphologies after discharge, it can be concluded that the addition of In element plays an essential part in forming corrosion pits on the surface of the anode while the addition of Ga element plays a vital role in destroying the surface passive layer to prevent passivation once corrosion starts.