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131.
In order to study the influence of cerium ion implantation on the aqueous corrosion behavior of zircaloy-4, specimens were implanted by cerium ions with a fluence range from 1×1016 to 1×1017 ions/cm2 at maximum 150°C, using MEVVA source at an extracted voltage of 40 kV. The valence and elements penetration distribution of the surface layer were analyzed by X-ray photoelectron spectroscopy (XPS) and auger electron spectroscopy (AES) respectively. Glancing angle X-ray diffraction (GAXRD) was employed to examine the phase transformation due to the cerium ion implantation in the oxide films. Three-sweep potentiodynamic polarization measurement was employed to value the aqueous corrosion resistance of zircaloy-4 in a 1 N H2SO4 solution. It was found that a significant improvement in the aqueous corrosion behavior of zircaloy-4 implanted with cerium ions compared with that of the as-received zircaloy-4. The improvement effect will declined with raising the implantation fluence. The bigger is the fluence, the less is the improvement. Finally, the mechanism of the corrosion behavior of the cerium-implanted zircaloy-4 is discussed. 相似文献
132.
Co^3+—modified Surface of LiMn2O4 Spinel for its Improvementof Electrochemical Properties 总被引:3,自引:0,他引:3
ZishanZHENG ZilongTANG ZhongtaiZHANG JunbiaoLU WanciSHEN 《材料科学技术学报》2003,19(4):359-362
Cobalt was used to modify the surface of spinel LiMn2O4 by a solution technique to produce Co^3 -modified surface material (COMSM). Cobalt was only doped into the surface of LiMn2O4 spinel. XPS(X-ray photoelectron spectroscopy) analysis confirms the valence state of Co^3 . COMSM has stable spinel structure and can prevent active materials from the corrosion of electrolyte. The ICP(inductively coupled plasma) determination of the spinel dissolution in electrolyte showed the content of Mn dissolved from COMSM was smaller than that from the pure spinel. AC impedance patterns show that the charge-transfer resistance (Rct) for COMSM is smaller than that for pure spinel. The particles of COMSM are bigger in size than those of pure spinel according to the micrographs of SEM(scanning electron microscopy). The determinations of the electrochemical characterization show that COMSM has both good cycling performance and high initial capacity of 124.1 mA/h at an average capacity loss of 0.19 mAh/g per cycle. 相似文献
133.
工作流是近年来网络领域里研究的一个热点,对工作流模型的性能分析是工作流研究的一个重要内容.实际的模型往往规模大而复杂,这为分析其性能带来了很大的困难.但有一类模型可由工作流的四种基本模型(顺序、并行、选择、循环)嵌套组成,对于这类模型,本文给出了计算其性能乘积解的数学公式.文中给出了如何由这四种基本模型嵌套组成实际模型的方法,推导出了计算这四种基本模型的性能等价公式,并按建立实际模型相反的顺序,用由里到外逐层的分析方法,给出了计算实际模型的性能乘积解. 相似文献
134.
随着网络规模越来越大,选择一个完善的网络管理框架并有效降低标签需求量对于MPLS网络而言显得十分重要。为此,探讨了基于策略的MPLS管理以及Trainet等近年来出现的大规模MPLS网络新兴技术,并与现有相关技术进行了比较。 相似文献
135.
Mesopore nickel-based mixed rare-earth oxide (NMRO) and activated carbon (AC) with rich oxygen-contained groups were prepared as electrode materials in a supercapacitor using room temperature ionic liquid (RTIL) electrolyte. These electrode materials were characterized by XPS, XRD, N2 adsorption, SEM as well as various electrochemical techniques, and showed good properties and operated well with RTIL electrolyte. A 3 V asymmetrical supercapacitor was fabricated, which delivered a real power density of 458 W kg−1 as well as a real energy density of 50 Wh kg−1, and during a 500-cycle galvanostatic charge/discharge measurement, no capacity decay was visible. Such promising energy-storage performance was to a large extent ascribed to nonvolatile RTIL electrolyte with wide electrochemical windows and high stable abilities worked with both electrode materials. 相似文献
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138.
The effect of tetramethylammonium cations (TMA+) on TiO2 crystal morphology in hydrothermal conditions has been studied. The as-synthesized samples were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM) and scanning electron microscopy (SEM) methods. The morphologies including besom-like particle, nanosheet and nanotube have been observed. The different ways TMA+ cations in the hydrothermal bases affect the crystal growth manner are suggested to be responsible for the different morphologies of the as-synthesized samples. 相似文献
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