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201.
(反应)模晶生长法制备NBT-6BT织构陶瓷的研究 总被引:1,自引:0,他引:1
以熔盐法合成的片状SrTiO3,Bi4Ti3O12为种晶,分别采用模晶生长法(TGG)和反应模晶生长发(RTGG)制备了具有〈001〉取向的0.94(Na1/2Bi1/2)TiO3-0.06BaTiO3(NBT-6BT)织构陶瓷。研究了不同种晶选择、流延和热处理工艺参数对陶瓷织构化程度、显微结构和压电性能的影响。结果表明,RTGG制备的织构陶瓷比TGG的在结构和性能等方面都具有优势,且用该方法以Bi4Ti3O12为种晶,制备出了高密度(f≥96%)、高织构度(F≈95%)、高性能(d33≈241pC/N)的NBT-6BT无铅压电陶瓷。 相似文献
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观察了Bi—2223带村内部组织结构的变化。测定了带材内导电性能不均匀和轧制及冷压过程变形不均匀的关系 相似文献
205.
本文通过重氮化反应设计、合成了鲁米诺偶联的氨基锌酞菁,对其电子吸收光谱和荧光光谱性质进行了研究,结果表明该分子激发单重态可能以振动驰豫的方式使大部分能量耗散,鲁米诺偶联前后,氨基取代锌酞菁的荧光光谱有明显差别,为进一步开发酞菁类荧光光存储材料提供了理论依据. 相似文献
206.
Xiangming He Weihua Pu Li Wang Jianguo Ren Changyin Jiang Chunrong Wan 《Electrochimica acta》2007,52(11):3651-3653
A novel process was proposed to synthesize nano Sb-encapsulated pyrolytic polyacrylonitrile composite for anode material in lithium secondary batteries. The preparation started with the dissolution of SbCl3 and polyacrylonitrile (PAN) in dimethylformamide (DMF) solution, followed by the addition of KBH4 to reduce Sb3+ in the solution. The Sb composite was obtained by pyrolysis of the Sb/PAN mixture that precipitated out when the DMF solution was added by plentiful water. The TEM analysis showed that about 100-200 nm Sb particles were embedded by the pyrolyzed PAN, which provided a conductive matrix to relieve the morphological change of Sb during electrochemical cycling. As-prepared composite presented good cycleability for lithium storage. The proposed process paves an effective way to prepare high performance alloy based composite anode materials for high performance lithium-ion batteries. 相似文献
207.
Electron Emission from Barium Strontium Titanate Ceramics 总被引:1,自引:0,他引:1
Shutao Chen Xianlin Dong Shuxin Zheng Ziqiu Zhu Chuanxiang Tang 《Journal of the American Ceramic Society》2006,89(7):2118-2122
This paper focuses on understanding the influence of materials' properties on the ferroelectric electron emission. Ferroelectric ( x =1.0 and 0.8) and paraelectric ( x =0.67 and 0.5) compositions of barium strontium titanate (Ba x Sr(1− x ) TiO3 ) system were chosen for study based on their different ferroelectric and dielectric properties. Similar emission current waveforms were obtained from four compositions with negative triggering voltage applied to the rear electrode of the samples. It was difficult to explain the experimental results using the spontaneous polarization-switching model. The mechanism of electron emission from Ba x Sr(1− x ) TiO3 ceramics was ascertained to surface plasma emission. 相似文献
208.
209.
Xingzhong Zhao Jiajun Liu Baoliang Zhu Hezhou Miao Zhenbi Luo 《Ceramics International》1997,23(6):483-488
Si3N4-based ceramic cutting tools are used nowadays for machining cast iron, nickel-based alloys, etc. Austenitic stainless steel AISI 321 is one of the most difficult to cut materials. In order to investigate the wear behaviour of Si3N4 ceramic when cutting the stainless steel, wear tests are carried out on a pin-on-disc tribometer, which can simulate a realistic cutting process. The selected load range is from 58.8 N to 235.2 N, the speed range is from 0.8 m/s to 3.2 m/s. The test results show that the wear of Si3N4 ceramic increases with both load and speed and the wear of the ceramic is mainly caused by adhesion between the rubbing surfaces. Scanning electron microscope (SEM), electron probe microanalyser (EPMA) and energy dispersive X-ray analyser (EDXS) were used for examinations of the worn surfaces. The wear mechanisms of Si3N4 ceramic sliding against the stainless steel were discussed in detail. 相似文献
210.
Electroporation creates aqueous pathways by short high-voltage pulses resulting in a transient perme- abilization of stratum corneum and an increase in the transdermal delivery rate.However the aqueous pathways will reseal after pulsing,which leads to the rapid drop of transdermal flux.In the present study,the surfactants were added to the donor solution to hinder the shrinkage and resealing of the electropore,and to prolong the lifetime of the aqueous pathways with the consideration that the surfactants could reduce the surface energy of the electropore. These effects of surfactants were demonstrated by the dynamic electrical resistance of the skin and the fluorescent imaging of the local transport regions.Piroxicam(PIX)was transported percutaneously in the presence of surfactants in vitro.Owing to the longer lifetime of aqueous pathways,together with the promotion of PIX availability at the barrier exterior and the improvement in the partition of PIX into the aqueous pathways,the presence of surfactants led to a remarkable increase in the transdermal delivery rate during electroporation and a significant growth of the accumulative transdermal amount of PIX. 相似文献