氮气氛下LTCC基板Cu共烧金属化研究

从PMMA型LTCC素坯膜的制备和PMMA的排胶机理两方面，研究了LTCC基板Cu共烧金属化。结果表明，采用PMMA作为粘结剂的流延浆料具有剪切变稀行为，所得的流延坯膜微观组织均匀，叠压后坯体内部无分层现象。热失重、差热和傅立叶红外光谱联用分析结果表明高纯N2气氛中PMMA以解聚机理热解，热解后释放的主要产物为丙烯酸甲酯。在高纯N2气氛中LTCC与Cu共烧后Cu金属化膜平整、致密，连通良好。经测试，基板表面Cu导体方阻小于5mΩ/□。     

Experimental investigation of the heat and mass transfer between air and liquid desiccant in a cross-flow regenerator

The regenerator is one of the essential components in a liquid desiccant air-conditioning system, whose efficiency directly influences the system performance. A performance test-bed for a cross-flow regenerator was established in the present analysis. Celdek structured packings were used in the regenerator and LiBr aqueous solution was used as the liquid desiccant. Moisture removal rate and regenerator effectiveness are adopted to describe the mass transfer performance of the regenerator. Effects of air and desiccant inlet parameters on the regenerator performance are experimentally investigated, and performance comparisons between present cross-flow regenerator and other counter-flow configurations available in the literature are also carried out. The comparison results show that the impacts of air and desiccant inlet parameters show similar tendency with those of counter-flow regenerators. A dimensionless mass transfer correlation is proposed, which gives results in good agreement with the experimental findings.     

Optimal determination of warranty region for 2D policy: A customers' perspective

Warranty is treated by the manufacturer as a marketing strategy that creates better customer satisfaction, which finally helps to get hold of a bigger market share. The cost incurred towards this service is termed as warranty cost, which is a function of warranty policy and region, product quality and reliability, and the customers' usage pattern. Under the 2D warranty policy, there exists numerous iso-cost regions for any specified value of warranty cost. In this article, we propose a methodology to determine the optimal region when customers' utility is measured by the length of warranty coverage time. It is believed that the results will help the manufacturer to provide improved customer service.     

VERIFICATION AND COMPARISON OF FORMULAS FOR BED LOAD TRANSPORT

1 .　ＩＮＴＲＯＤＵＣＴＩＯＮＴｈｅｂｅｄｌｏａｄｔｒａｎｓｐｏｒｔｈａｓｂｅｅｎｅｘｔｅｎｓｉｖｅｌｙｓｔｕｄｉｅｄｉｎｔｈｅｐａｓｔｆｅｗｄｅｃａｄｅｓａｎｄｍａｎｙｆｏｒｍｕｌａｓｆｏｒｐｒｅｄｉｃｔｉｎｇｂｅｄｌｏａｄｔｒａｎｓｐｏｒｔｒａｔｅｈａｖｅｂｅｅｎｐｒｅｓｅｎｔｅｄ(Ｅｉｎｓｔｅｉｎ 1950 ;Ｍｅｙｅｒ Ｐｅｔｅｒ 194 8;Ｂａｇｎｏｌｄ 1973;Ｅｎｇｅｌｕｎｄ 1976;Ｙａｌｉｎ 1972 ;Ｓａｍａｇａ 1986;ａｎｄＫａｒｉｍ 1998) .Ｗｈｅｎａｐｐｌｉｅｄｔｏｓｔｒｅａｍｓｗｉｔｈｐａｒｔｉａｌ…     

Formation mechanism of bainitic ferrite and carbide

Superledges on the broad faces of bainitic ferrite plates have been observed with transmission electron microscope (TEM). The observed superledges, ranging from less than 1 to 24 nm in height, are imaged in three dimension by way of tilt operation under TEM. Also, an array of smaller superledges are observed to pile up in front of a secondary phase. Pileup of superledges in front of a barrier is indicative of the mobility of an individual superledge. The precipitation of carbide associated with bainitic ferrite is also studied. It is observed that a carbide of a wedgelike shape may exist in front of a superledge with its tip(i.e., thinner end) penetrating the austenite and its root (the other end) originating at α:γ boundary. This condition indicates that the observed carbides may nucleate at the austenite side of α:γ phase boundary and grow toward austenite matrix. This article is based on a presentation made at the Pacific Rim Conference on the “Roles of Shear and Diffusion in the Formation of Plate-Shaped Transformation Products,” held December 18-22, 1992, in Kona, Hawaii, under the auspices of ASM INTERNATIONAL’S Phase Transformations Committee.     

Studies on the corrosion behavior of cerium-implanted zircaloy-4 with GAXRD

In order to study the influence of cerium ion implantation on the aqueous corrosion behavior of zircaloy-4, specimens were implanted by cerium ions with a fluence range from 1×10¹⁶ to 1×10¹⁷ ions/cm² at maximum 150°C, using MEVVA source at an extracted voltage of 40 kV. The valence and elements penetration distribution of the surface layer were analyzed by X-ray photoelectron spectroscopy (XPS) and auger electron spectroscopy (AES) respectively. Glancing angle X-ray diffraction (GAXRD) was employed to examine the phase transformation due to the cerium ion implantation in the oxide films. Three-sweep potentiodynamic polarization measurement was employed to value the aqueous corrosion resistance of zircaloy-4 in a 1 N H₂SO₄ solution. It was found that a significant improvement in the aqueous corrosion behavior of zircaloy-4 implanted with cerium ions compared with that of the as-received zircaloy-4. The improvement effect will declined with raising the implantation fluence. The bigger is the fluence, the less is the improvement. Finally, the mechanism of the corrosion behavior of the cerium-implanted zircaloy-4 is discussed.     

Co^3＋—modified Surface of LiMn2O4 Spinel for its Improvementof Electrochemical Properties

Cobalt was used to modify the surface of spinel LiMn2O4 by a solution technique to produce Co^3 -modified surface material (COMSM). Cobalt was only doped into the surface of LiMn2O4 spinel. XPS(X-ray photoelectron spectroscopy) analysis confirms the valence state of Co^3 . COMSM has stable spinel structure and can prevent active materials from the corrosion of electrolyte. The ICP(inductively coupled plasma) determination of the spinel dissolution in electrolyte showed the content of Mn dissolved from COMSM was smaller than that from the pure spinel. AC impedance patterns show that the charge-transfer resistance (Rct) for COMSM is smaller than that for pure spinel. The particles of COMSM are bigger in size than those of pure spinel according to the micrographs of SEM(scanning electron microscopy). The determinations of the electrochemical characterization show that COMSM has both good cycling performance and high initial capacity of 124.1 mA/h at an average capacity loss of 0.19 mAh/g per cycle.