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711.
712.
干燥温度对醇提余甘子多酚含量及其抗氧化活性的影响 总被引:1,自引:0,他引:1
为探究干燥方式(冷冻真空干燥、热风干燥)和干燥温度(冻干、40、60、80、100℃)对余甘子多酚活性成分的影响,利用高效液相色谱(HPLC)检测不同干燥处理后余甘子醇提液中没食子酸、柯里拉京、鞣花酸、诃子鞣酸的含量,并测定其总多酚含量和抗氧化活性(ABTS+自由基清除能力和DPPH自由基清除能力)。结果表明,随着干燥温度的升高,余甘子中没食子酸、柯里拉京、鞣花酸、诃子鞣酸含量均增加,100℃热风干燥时达最高(分别为12.83、6.04、16.89、13.48 mg/g)。总多酚含量与抗氧化活性(ABTS+·清除能力和DPPH·清除能力)也随干燥温度升高而增加,80℃热风干燥时达最高(分别为200.92、695.76、725.05 mg/g)。此外,试验结果表明柯里拉京、诃子鞣酸和总多酚的含量与余甘子醇提样品ABTS+自由基清除能力呈显著或极显著正相关(P<0.05或P<0.01)。本次试验中,与热风干燥相比,冷冻干燥的样品中4种多酚单体和总多酚含量以及抗氧化活性无明显优势,综合考虑,80℃热风干燥为余甘子的最佳干燥方式。 相似文献
713.
714.
Ultra-wideband (UWB) technology has been considered to offer an innovative solution for future short-range high-speed wireless
communications. These systems use very low transmission power, spread over a bandwidth of several gigahertz. The very low
transmission power and the large bandwidth used, enable UWB radio systems to co-exist with other narrowband systems over the
same frequency band without interfering the narrowband systems. Nevertheless, these narrowband systems may cause interference
which may jam the UWB receiver completely. Since standard narrowband interference suppression techniques are not applicable,
techniques for interference suppression have to be developed. In this paper, the method of the local polynomial estimator
in time-hopping impulse radio (TH-IR) for UWB communication is considered, which should not estimate any parameter of channel.
And the narrowband interference (NBI) is modeled as a stationary process. Theoretical analysis of this algorithm reveals that
it can eliminate the narrowband interference almost completely and can be computed by simple expression. Moreover, the sampling
rate is very low. 相似文献
715.
《Information Sciences》2007,177(22):5134-5140
In this note, we show by examples that Propositions 2.4 and 2.5 in [N. Kuroki, P.P. Wang, The lower and upper approximations in a fuzzy group, Information Sciences 90 (1996) 203] and Theorem 2.5 in [N. Kuroki, Rough ideals in semigroups, Information Sciences 100 (1997) 139] are incorrect and offer their modified versions. 相似文献
716.
717.
Meng Jiang Qin Lin Dunmin Lin Qiaoji Zheng Ximing Fan Xiaochun Wu Hailing Sun Yang Wan Lang Wu 《Journal of Materials Science》2013,48(3):1035-1041
Ba0.85Ca0.15Ti0.90Zr0.10O3 + xmol% MnO2 lead-free ceramics have been prepared by a conventional sintering method and the effects of MnO2 and sintering temperature on microstructure, ferroelectric, and piezoelectric properties of Ba0.85Ca0.15Ti0.90Zr0.10O3 lead-free ceramics have been studied. The addition of 0.25 mol% MnO2 promotes grain growth, improves the ferroelectricity of the ceramics and strengthens ferroelectric tetragonal–ferroelectric orthorhombic phase transition near 40 °C. Because of the coexistence of tetragonal and orthorhombic phases and the combinatory effects of soft and hard doping of Mn ions, the ceramic with x = 0.25 exhibits the optimum piezoelectric properties (d 33 = 306 pC/N and k p = 42.2 %, respectively). Excess MnO2 inhibits the grain growth and degrades the ferroelectric and piezoelectric properties of the ceramics. Sintering temperature has an important influence on the microstructure, tetragonal–orthorhombic phase transition near 40 °C, ferroelectric and piezoelectric properties of the ceramics. The increase in sintering temperature leads to large grains and more noticeable tetragonal–orthorhombic phase transition near 40 °C, enhances ferroelectricity and thus improves effectively the piezoelectricity of the ceramics. The Ba0.85Ca0.15Ti0.90Zr0.10O3 ceramic sintered at 1350 °C possesses the optimum piezoelectric constant d 33 value of 373 pC/N. 相似文献
718.
Microstructure and corrosion behaviour of a binary Al–29 at%Co alloy have been studied. The alloy was prepared by arc-melting of Al and Co in high purity Ar and rapidly solidified on a water-cooled Cu mould. The alloy chemical composition and microstructure were characterized by scanning electron microscopy, energy dispersive X-ray spectroscopy and X-ray diffraction. Furthermore, the corrosion behaviour was studied by potentiodynamic polarization in aqueous NaCl (0.6 mol dm−3) at room temperature. The alloy was found to consist of three phases: hexagonal Al5Co2, Z-phase and AlCo (β). The corrosion resistance of different intermetallic phases is characterized. The results are compared to previously published results of Al–TM (TM = transition metal) alloys. 相似文献
719.
720.
Daojiang Gao Yanhong Li Xin Lai Jian BiDunmin Lin 《Journal of Alloys and Compounds》2011,509(3):697-703
LiCoO2 thin films have been directly synthesized on cobalt substrate in LiOH solution at room temperature by electrochemical method. The obtained LiCoO2 thin films were characterized by X-ray diffraction (XRD), scanning electronic microscopy (SEM) and X-ray photoelectron spectroscopy (XPS). The influence of electrochemical reaction time, current density and concentration of LiOH solution on the crystal structure and morphology of the obtained LiCoO2 thin films was discussed emphatically. Our results show that the as-synthesized LiCoO2 films all are pure hexagonal structure. The crystallinity, densification and uniformity of the films increase with increasing electrochemical reaction time, current density as well as concentration of LiOH solution and then decrease. The preferable electrochemical reaction conditions were optimized as: electrochemical reaction time is 50 h, current density is 1 mA cm−2 and concentration of LiOH solution is 3 mol dm−3. 相似文献