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81.
In close-coupled gas atomization(CCGA), the influences of melt superheat on breakup process are fundamental to obtain desired or finer powder. Based on a series of Cu atomization experiment under different superheating conditions, the influences of melt superheat on breakup process were studied. Experimental results indicate that as the melt superheat is increased to 150, 200, 250 and 300 K, the mean particle size (D50) decreases consequently to 34.9, 32.3, 30.9 and 19.7 μm. Theoretical analysis reveals that the primary breakup and secondary breakup processes are close coupled, and the melt superheat radically influences the melt properties, and plays a crucial role on governing the filming process of primary breakup and the atomization modes of secondary breakup. There exists a strong nonlinear decrease of contact angle of melt to nozzle orifice wall when the superheat is increased fi'om 250 K to 300 K, leading to a marked fall of the film thickness formed in primary breakup, and D50 of copper powders is therefore sharply reduced. However, the log-normal distribution feature of particle size has not been substantially improved. 相似文献
82.
Y. Yang B. F. Wang J. Xiong Y. Zeng Z. P. Chen X. Y. Yang 《Metallurgical and Materials Transactions A》2006,37(10):3131-3137
The microstructure and microtexture in adiabatic shear bands (ASBs) on the titanium side in the titanium/mild steel explosive
cladding interface are investigated by means of optical microscopy, scanning electron microscopy/electron backscattered diffraction
(SEM/EBSD), and transmission electron microscopy (TEM). Highly elongated subgrains and fine equiaxed grains with low dislocation
density are observed in the ASBs. Microtextures (25 deg, 75 deg, 0 deg), (70 deg, 45 deg, 0 deg), and (0 deg, 15 deg, 30 deg)
formed within the ASBs suggest the occurrence of the recrystallization. The grain boundaries within ASBs are geometrically
necessary boundaries (GNBs) with high angles. Finite element computations are performed to obtain the effective strain and
temperature distributions within the ASBs under the measured boundary conditions. The rotation dynamic recrystallization (RDR)
mechanism is employed to describe the kinetics of the nanograins’ formation and the recrystallized process within ASBs. During
the deformation time (about 5 to 10 μs), the following processes take place: dislocations accumulate to form elongated cell
structures, cell structures break up to form subgrains, and subgrains rotate and finally form recrystallized grains. The small
grains within ASBs are formed during the deformation and do not undergo significant growth by grain boundary migration after
deformation. 相似文献
83.
84.
《Journal of power sources》2006,160(1):657-661
The cathode-active materials, layered Li[Ni0.333Co0.333Mn0.293Al0.04]O2−zFz (0 ≤ z ≤ 0.1), were synthesized from a sol–gel precursor at 900 °C in air. The influence of Al–F co-substitution on the structural and electrochemical properties of the as-prepared samples was characterized by X-ray diffraction (XRD), scanning electron microscope (SEM) and electrochemical experiments. The results showed that Li[Ni0.333Co0.333Mn0.293Al0.04]O2−zFz has a typical hexagonal structure with a single phase, the particle sizes of the samples tended to increase with increasing fluorine content. It has been found that Li[Ni0.333Co0.333Mn0.293Al0.04]O1.95F0.05 showed an improved cathodic behavior and discharge capacity retention compared to the undoped samples in the voltage range of 3.0–4.3 V. The electrodes prepared from Li[Ni0.333Co0.333Mn0.293Al0.04]O1.95F0.05 delivered an initial discharge capacity of 158 mAh−1 g and an initial coulombic efficiency is 91.3%, and the capacity retention at the 20th cycle was 94.9%. Though the F-doped samples had lower initial capacities, they showed better cycle performances compared with F-free samples. Therefore, this is a promising material for a lithium-ion battery. 相似文献
85.
Objective To study on the role of thymus transplantation for heart allograft in rats. Methods Vascularized heart-thymus combined transplantation was performed with microsurgical technique. Graft survival, histopathology,
level of IL-2, IL-4 and its mRNA expression in serum and cardiac grafts were investigated. Results Heart-thymus combined transplantation achieved effect in the prolongation of cardiac graft survival with short-term administration
of cyclosporine. Conclusions Vascularized thymus transplantation induced immune tolerance in thymectomized rats. 相似文献
86.
《Fuel》2006,85(7-8):944-956
The oxidation of kerosene Jet-A1 and that of n-decane have been studied experimentally in a jet-stirred reactor at atmospheric pressure and constant residence time, over the high temperature range 900–1300 K, and for variable equivalence ratio (0.5≤ϕ≤2). Concentration profiles of the reactants, stable intermediates, and final products have been obtained by probe sampling followed by on-line and off-line GC analyses. The oxidation of neat n-decane and of kerosene in these conditions was modeled using a detailed kinetic reaction mechanism (209 species and 1673 reactions, most of them reversible). The present model was successfully used to simulate the structure of a fuel-rich premixed n-decane–oxygen–nitrogen flame. In the modelling, kerosene was represented by four surrogate model fuels: 100% n-decane, n-decane-n-propylbenzene (74%/26% mol), n-decane-n-propylcyclohexane (74%/26% mol), and n-decane-n-propylbenzene-n-propylcyclohexane (74%/15%/11% mol). The 3-component model fuel was the most appropriate for simulating the JSR experiments. It was also successfully used to simulate the structure of a fuel-rich premixed kerosene–oxygen–nitrogen flame. 相似文献
87.
Lutein and lutein esters in marigold flowers was quantitatively determined by high performance chromatography (HPLC) with ODS-C18 column. A mixture of CH3CN-CH3OH-CH3COOCH2CH2 with volume ratio of 55:1:44 was used as mobile phase at a flow rate of 1.0mL/min and detection was carried out at 480 nm. The column temperature was about 20℃. The contents of lutein and lutein esters were determined by analytical curve of lutein since lutein and lutein esters have the same spectral characteristics. Determination results of hexane extracts and saponified samples of lutein show that the saponification transforms the esters into free lutein. The increase of the content of dipalmitate and palmitate stearate reveals that the reaction includes transesterifications. 相似文献
88.
《Materials Letters》2007,61(11-12):2208-2211
Multiwall carbon nanotubes (MWCNTs), synthesized by microwave plasma enhanced chemical vapor deposition, were used as the precursor to synthesize diamond in a pure hydrogen microwave discharge. Diamond-scratched silicon wafers, with and without precoated MWCNTs, were placed side by side on a substrate holder. Diamond was formed on both wafers with the consumption of MWCNTs. The present results suggest that the solid–gas–solid transformation mechanism is involved in this process. 相似文献
89.
《Journal of Systems Architecture》2007,53(9):629-643
In this work we present a self-reconfiguration control focused on multiprocessor core-based systems implemented on FPGA technology. An infrastructure of signals, protocols, interfaces and a controller is exposed to perform safe hardware/software reconfigurations. This infrastructure is part of the Tornado framework that includes other elements such as a multi-context assembler for a reconfigurable processor or a custom design flow developed for the Wishbone IP-Core interconnection specification. We present two applications where the presented control system has been applied, and it is compared with other available approaches. 相似文献
90.
《Materials Letters》2007,61(4-5):1154-1157
Lanthanum (La), a rare earth element with anticoagulative and antiphlogistic function, was added into the medical grade 316L stainless steel in order to improve its biocompatibility. The corrosion resistance of the La added 316L steel in two different simulated body fluids, simulated blood plasma and Hank's solution, was evaluated. The result showed that the addition of La in the steel could largely affect the corrosion behavior of the steel. The steel with 0.01% La showed the widest passive region and the best resistance to pitting attack, within the addition range of La from 0.01% to 0.08%. The corrosion resistance improvement of La added 316L stainless steel is probably due to the effect of La on the purification of the steel, the modification of inclusions, and the passive film formation in the simulated body fluids. 相似文献