分析化学网络智能组卷系统的开发

为了进一步推动教学改革,促进教学质量的提高,我们开发了分析化学智能组卷系统,介绍了智能组卷系统开发的意义、开发过程、主要特色及使用效果,并对开发前景进行了展望。结果表明:该网络智能组卷系统具有客观性强、时间快、易于控制试卷难度等特点,深受师生和专家好评。     

壳聚糖及其衍生物在食品工农业中的应用研究进展

壳聚糖作为一种天然碱性多糖,具有高附加值、可再生资源、抑菌、无毒、易成膜、可生物降解、螯合重金属等优点。文章综述了壳聚糖在食品工农业方面的应用研究进展情况,详细介绍了壳聚糖、改性壳聚糖和复合壳聚糖在果蔬保鲜、植物诱导、防止微生物生长、果汁澄清、添加剂和食品工业废水方面的应用性能,并对壳聚糖在食品中应用的未来发展进行展望。     

Investigation on the morphology of hierarchical mesoporous ZSM-5 zeolite prepared by the CO2-in-water microemulsion method

A series of hierarchical mesoporous ZSM-5 zeolites with different morphology were successfully synthesized by the CO₂-in-water microemulsion method, and mesoporosity was formed without organotemplate. The different synthesis conditions, including silica alumina molar ratio, stirring time and compressed CO₂ pressure, were systematically investigated to discuss the influence of these conditions on the morphology of ZSM-5 zeolite. The resulting samples were characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), inductively coupled plasma (ICP) and nitrogen adsorption-desorption measurement. XRD results indicated that compressed CO₂ route for the synthesis of MFI zeolites had a fast crystallization rate and good crystallinity. SEM images showed that the ZSM-5 hierarchical mesoporous ZSM-5 zeolite had a uniform chain-like crystal morphology, whereas silicalite-1 displayed a monodisperse crystal morphology. In addition, the nitrogen adsorption-desorption measurement provided sufficient evidence for the presence of hierarchical mesopores in ZSM-5 zeolite.     

Pore formation during the breakdown process in anodic Ta2O5 films

The breakdown damage during the anodic oxidation of tantalum has been studied through reanodization experiments. The results have been interpreted assuming the formation of non-shorting pores produced as a consequence of the breakdown process. On the basis of this model, the extent of the damaged area and the pore depth has been assessed.     

Enhanced hydrodesulphurization of cokes deposited on iron ore by air gasification

The influence on air-gasification of cokes deposited on iron ores were studied in under successive desulphurization at 750 °C under atmospheric hydrogen. Gasification promoted by steam (water: 40 μl min⁻¹) at 350 °C for 125 min gasified 21% of the coke and allowed 25% oxidative desulphurization (based on sulphur in the coke) during the gasification and enhanced the successive hydrodesulphurization level up to 63% giving a total desulphurization of 88%. This level is comparable with that achieved after grinding. Gasification at higher temperatures, which burned more coke, was less effective in enhancing hydrosedulphurization. Gasification increases the access of hydrogen molecules to sulphur atoms in the coke. Gasification, which increases the surface area of the coke and removes the sulphur preferentially, is discussed in terms of reactivity.     

A generalized hybrid transfinite element computational approach for nonlinear/linear unified thermal-structural analysis

The paper describes the development of a new hybrid computational approach for nonlinear/linear thermal-structural analysis. The proposed transfinite element approach is a hybrid scheme as it combines the modeling versatility of contemporary finite elements with transform methods and the classical Bubnov-Galerkin schemes. Application of the proposed formulations for nonlinear analysis is also developed. Several test cases are presented to include nonlinear/linear unified thermal-stress and thermal-stress wave propagations. Comparative results validate the fundamental capabilities of the proposed hybrid transfmite element methodology.     

污染土壤/底泥电动修复研究进展

修复污染土壤/底泥对改善生态环境质量极为重要,通过对污染土壤/底泥施加电场,可使污染物定向迁移、富集并去除.综述了电动修复的发展历程,比较了重金属、有机污染物及复合污染物的电动修复机理及其限制因素,分析了土壤预处理(加入酸、氧化剂、共溶剂、表面活性剂,搅拌,升温等)、电极优化(交换电极、阳极逼近、电极矩阵等)、多技术(...     

3种杀虫剂亚致死浓度胁迫对桃蚜扩散行为的影响

[目的]明确氟吡呋喃酮、氟啶虫胺腈和环氧虫啶亚致死浓度作用下桃蚜的扩散行为.[方法]实验室条件下测定3种杀虫剂对桃蚜的相对生物活性,并开展各药剂亚致死浓度对桃蚜扩散能力影响研究.[结果]"杀虫剂种类"和"作用时间"是影响桃蚜扩散行为的主要因素;氟吡呋喃酮LC10和LC30处理桃蚜2 h,其扩散率分别为12.38％和36...