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64.
S. Zh. Davrenbekov E. S. Mustafin B. K. Kasenov S. T. Edil'baeva Sh. B. Kasenova E. K. Zhumadilov Zh. I. Sagintaeva 《Inorganic Materials》2004,40(9):976-978
NdMCr2O5 (M = Na, K, Cs) and NdMgCr2O5.5 are prepared by solid-state reactions between appropriate oxides and carbonates and are shown to have a tetragonal structure. The heat capacity of these chromites, measured from 298.15 to 673 K, exhibits sharp changes attributable to second-order phase transitions. The C
p
0(T) data are represented by quadratic best fit equations. The electrical resistivity of the chromites is measured between 303 and 493 K. The results attest to semiconducting behavior of the materials in certain temperature ranges. 相似文献
65.
《Fuel Processing Technology》2005,86(7):809-830
The effect of weathering (natural oxidation) on the technological properties of cokes obtained at three different scales (laboratory, pilot plant and semi-industrial), from two medium volatile bituminous coals stored at INCAR open stockyard for several months, has been studied in this work. The results show that the procedure developed at laboratory scale is useful for studying the evolution of coke quality because the trends of the main quality indexes (mechanical strength and reactivity to CO2) are in agreement with those of the cokes produced at larger scales. Furthermore, it was found that the total porosity and the micropores specific surface area of the cokes vary with the scale of carbonization, and that they increase as follows: semi-industrial<pilot plant<<laboratory. All of which are related to the evolution of the mechanical strength and reactivity to the CO2. 相似文献
66.
Influence of coal forced oxidation on technological properties of cokes produced at laboratory scale
《Fuel Processing Technology》2005,87(1):1-10
The effect of coal oxidation in air at 140 °C on the technological properties of cokes obtained at laboratory scale from two medium volatile bituminous coals has been studied. The proximate and ultimate analyses do not show important changes with coal oxidation time. However oxidation clearly has a strong effect on the plastic properties of the coals in view of the fact that the Gieseler fluidity eventually disappears. From this point variations in plastic properties can still be detected by FSI. Other changes, such as a shortening of the length of the saturated fragments of the aliphatic chains, a decrease in the aliphatic hydrogen content and an increase in the oxygen-containing groups are detected by PA-FTIR. It was also found that the main coke quality indices (mechanical strength and reactivity to CO2) of both coke series are impaired with coal oxidation. A close relationship between reactivity to CO2 and the micropore specific surface area of the cokes has been corroborated. 相似文献
67.
《Fuel Processing Technology》2005,87(1):71-76
Oil agglomeration of Sivas–Divriği (S–D) Uluçayır lignite fines was carried out using kerosene and kerosene–extract oil (which was obtained from lignite treated with microwave energy) mixture as a bridging oil. The effects of parameters such as the amount and type of bridging oil, microwave time and particle size on the agglomeration performance were investigated. The amount of kerosene was varied from 5 to 30 wt.% of the initial lignite loading. The values of the grade and recovery increased with an increase in the amount of kerosene added. Extract oil fraction of the lignite extract at various ratios in kerosene increased the agglomeration recovery from 95.88% to 98.55%. The effect of microwave time was investigated and it was found that the grade was also increased with increasing microwave time (4, 8 and 10 min). The grade of char (microwave time: 8 min) was increased in comparison with the original lignite while decreasing its recovery. Dense medium separations of the lignite were conducted and the results of their grade recovery performances were compared with those of agglomeration of the particles. During the inspection of particle size effect on the dense medium separation, the recovery was increased remarkably (from 12.07% to 89.50%) with increasing particle size, while decreasing the grade (from 0.732 to 0.697). In the oil agglomeration of lignite the recovery values were increased with increasing particle size. 相似文献
68.
Xiaojun Xie Yonghong Cheng Hong Wang Qian Wang Xiaolin Chen Caixin Sun 《Ceramics International》2008,34(4):689-693
In the ideal A2B2O6O′ pyrochlore structure, the x-value of O atom position is a variable parameter. In Bi1.5ZnNb1.5−xTaxO7 (BZNT) cubic pyrochlores, the x-values alter with the different compositions of Nb/Ta. In this work, a series of initial models for BZNT were established by analyzing X-ray diffraction data. Then three structure modifying methods, including Rietveld refinement, Rietveld refinement with energy and geometry optimization based on quantum mechanics, were employed to obtain the precise models using Materials Studio. Moreover, the reflectivities of BZNT were computed by quantum mechanical simulation based on the refined models. Comparing the simulation results from different modifying models with the experimental results, it is found that Rietveld refinement with energy optimization is the most accurate method for BZNT pyrochlores. According to the simulation results, the different reflectivities correspond well with various x-values of O atom positions in BZNT pyrochlores. 相似文献
69.
《International Journal of Machine Tools and Manufacture》2007,47(3-4):462-470
In literature, five different sets of work material constants used in the Johnson–Cook's (J–C) constitutive equation are implemented in a numerical model to describe the behaviour of AISI 316L steel. The aim of this research is to study the effects of five different sets of material constants of the J–C constitutive equation in finite-element modelling of orthogonal cutting of AISI 316L on the experimental and predicted cutting forces, chip morphology, temperature distributions and residual stresses. Several experimental equipments were used to estimate the experimental results, such as piezoelectric dynamometer for cutting forces measurements, thermal imaging system for temperature measurements and X-ray diffraction technique for residual stresses determination on the machined surfaces; while an elastic–viscoplastic FEM formulation was implemented to predict the local and global variables involved in this research. It has been observed that all the considered process output and, in particular the residual stresses are very sensitive to the J–C's material constants. 相似文献
70.
《Energy Conversion and Management》2005,46(13-14):2173-2184
It is indicated that modified carbon is a practical sorbent for removal of NO and SO2 from waste gases by the adsorption method. The ideal compositions for the prepared sorbent were 4.0 wt.% and 2.5 wt.% Na2CO3 and KOH at the experimental conditions, respectively, shortened as ACNaK2.5. Experimental investigation showed that the sorbent had a comparatively high breakthrough adsorption capacity of NO and SO2, about 5.8 g (NO + SO2)/100 g sorbent. It is indicated that a relatively high adsorption temperature would benefit the sorbent adsorption capacities on NO and SO2 at a certain space velocity and pressure. Further study revealed that the ACNaK2.5 sorbent had good regenerability at the experimental conditions, which implied that the ACNaK2.5 sorbent would be a useful sorbent for simultaneous removal of NO and SO2 from waste gases by adsorption. 相似文献