热解气催化活化促进石河子烟煤热解的研究

采用等体积浸渍法制备了Fe/MgO,Co/MgO和Ni/MgO催化剂,利用固定床反应器对石河子烟煤在热解气气氛下的催化热解行为进行了研究,考察热解气在催化剂作用下对煤热解焦油产率、半焦产率、轻重油比例以及焦油族组成的影响,并与相同条件下N2气氛和热解气气氛热解特性进行了对比分析.结果表明,三种催化剂对煤在热解气中的热解都有促进作用,其中Ni/MgO催化剂对提高焦油产率最明显.在气体流量为400mL/min,热解温度为550℃,Ni/MgO为催化剂的条件下,焦油产率为7.33%,与相同条件下在N2气氛和热解气气氛下热解相比,焦油产率分别提高了78%和42%.而Co/MgO催化剂对提高轻油的作用较明显.这表明热解气催化活化对煤热解有较好的促进作用,可抑制缩聚反应,提高焦油的产率和改善焦油的品质.     

Analysis and simulation of QSP beamformer

The real Direction Of Arrival (DOA) varies with time in mobile communication system. In such situation, the performance of conventional beamformers will be degraded obviously. Quantum Signal Processing (QSP) beamformer is insensitive to DOA errors, thus it can achieve stable output performance in such circumstance. This letter verified the effectiveness and feasibility of the QSP beamformer by simulation results.     

新疆马铃薯种薯综合保鲜技术的研究

对新疆马铃薯种薯进行了贮藏研究,确定了最佳贮藏条件,并对贮藏过程中的干物质、淀粉、还原糖、蛋白质和Vc含量变化进行了分析.结果表明:最佳贮藏条件是低温3～5 ℃ 套袋处理,在此条件下贮藏的马铃薯失重率、腐烂率和发芽率均最低.贮藏过程中还原糖含量的变化始终遵循着淀粉-还原糖-淀粉的可逆动态平衡;随着贮藏时间的延长,马铃薯Vc含量逐渐降低;蛋白质、干物质含量变化不明显;淀粉含量呈先下降,到了末期有所回升的趋势.     

超声法提取中药制剂中醇溶性成分的研究

以超声时间、提取温度、乙醇浓度和固液比为因素,每因素进行3水平的正交实验,用紫外分光光度法测定中药制剂——促生长散中厚朴酚的含量和以其作为综合评价指标。结果发现提取实验中影响因素最大的是乙醇浓度,最佳提取条件为:超声时间60(20,20,20)min,超声温度35℃,乙醇浓度65%,固液比1:10。     

A numerical study of natural convection heat transfer in a vertically eccentric spherical annulus

The results of a numerical investigation of the natural convection process between isothermal vertically eccentric spheres with hotter inner core, are being presented. The Grashof and the Prandtl numbers have been kept constant at 4×10⁴ and 10 respectively. Eccentricities varying from −0.75 to +0.75 have been studied. From the numerical solution, it is possible to explain the average results obtained previously for the regime where the steady crescent flow pattern exists. Negative eccentricities have been found to enhance convection while positive eccentricities have the reverse effect. Results also show that heat transfer actually increases slightly for very high positive eccentricities where conduction plays an important role.     

淀粉接枝共聚高吸水树脂的研究进展及应用

介绍了淀粉系高吸水性树脂的制备引发方式,阐述了利用化学引发法合成的淀粉接枝丙烯腈类、丙烯酸类和丙烯酸酯或丙烯酰胺类3个系列吸水树脂的研究进展,并且介绍了淀粉接枝共聚高吸水树脂在个人卫生、医药、农业园林等方面的应用。简要指出了高吸水树脂的研究及发展方向。     

超临界CO_2萃取与浸渍法提取白刺果油化学成分的分析与比较

为了促进白刺属植物在医药和精细化工等领域中的应用,该研究采用超临界CO2萃取法和溶剂浸渍法提取唐古特白刺果油,并用气相色谱-质谱联用技术对其化学成分进行了分析,从超临界CO2萃取出的白刺果油中分离鉴定出51种化学成分;从浸渍法提取出的白刺果油中鉴定出22种成分;两种方法提取的果油共有14种相同化学成分,含量较高的主要有:二十九烷、二十七烷、亚油酸乙酯、γ-生育酚、VE(α-生育酚)、γ-谷甾醇、菜油甾醇、等。该研究工作的新颖性,已为新疆维吾尔自治区科委石河子大学图书馆2007年1月15日出具的第20070000000005号《科技查新报告》所证实。     

The Microstructure and thermal diffusivity of carbon nanostructures/Si3N4 composites processed using spark plasma sintering

Graphene nanoribbons (GNRs) were obtained by unzipping multiwall carbon nanotubes (MWCNTs). Three different silicon nitride-carbon nanostructures were prepared by spark plasma sintering (SPS): ceramic composites that contained 1 wt% carbon nanofibers (CNFs), 1 wt% MWCNTs and 1 wt% GNRs respectively. The α to β-Si₃N₄ transformation ratio and thermal diffusivity of GNR/Si₃N₄ composites were higher than both CNF/Si₃N₄ composites and MWCNT/Si₃N₄ composites. Furthermore, the higher thermal diffusivities of GNR/Si₃N₄ composites can primarily be attributed to the higher number of elongate β-Si₃N₄ grains.     

A study of job shop standard setup time quota

For the multi-item and small lot size production mode and single machine job shop scheduling sequence independent setup time, many setup times are difficult to estimate accurately, which influences the ability to achieve accurate production cycles and costs of products. The survey shows that the length of the setup time depends on the level of employee’s knowledge. Therefore, a method for determining the standard setup time quota based on the level of employees’ knowledge is proposed. First, an evaluation index system for the level of employee’s knowledge is built; the level of employee’s knowledge is estimated by the masses and experts fuzzy comprehension evaluation and entropy method. Second, the range and definition of the level of employees’ knowledge index are developed. Third, the relational model of the employee’s knowledge level and the level of employees’ knowledge index is constructed through the least squares method. Finally, an example application is presented to verify the feasibility and effectiveness of the proposed model.     

微波合成对-香豆酸的工艺研究

采用微波辐射法,利用正交设计,以对-羟基苯甲醛和丙二酸为原料,甲苯、吡啶作为溶剂,苯胺作催化剂合成了对-香豆酸.最佳反应条件:在微波辐射下,反应物摩尔比为1:2(0.015mol:0.03mol),催化剂苯胺用量0.54g,辐射时间50min,产率达到72.76%.与传统法比较,微波辐射具有反应速度快、产率高的优点.