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81.
The effects of F-doping concentration on geometric structure, electronic structure and optical property of β-Ga2O3 were investigated. All F-doped β-Ga2O3 with different concentrations are easy to be formed under Ga-rich conditions, the stability and lattice parameters increase with the F-doping concentration. F-doped β-Ga2O3 materials display characteristics of the n-type semiconductor, occupied states contributed from Ga 4s, Ga 4p and O 2p states in the conduction band increase with an increase in F-doping concentration. The increase of F concentration leads to the narrowing of the band gap and the broadening of the occupied states. F-doped β-Ga2O3 exhibits the sharp band edge absorption and a broad absorption band. Absorption edges are blue-shifted, and the intensity of broad band absorption has been enhanced with respect to the fluorine content. The broad band absorption is ascribed to the intra-band transitions from occupied states to empty states in the conduction band. 相似文献
82.
以TiCl4为原料,采用水解沉淀法,并在空气气氛下于不同温度煅烧2h,制备得到纳米TiO2。采用XRD、TEM及UV-Vis对样品进行表征。在卤钨灯照射下,研究了不同煅烧温度、不同pH值以及H2O2的加入等因素对TiO2光催化降解次甲基蓝的影响。结果表明:以水解沉淀法制备的纳米TiO2,随煅烧温度的提高,在600℃开始向金红石相转变,1000℃时全部转变为金红石相,并且TiO2粒子长大,吸收带边向长波方向移动。锐钛矿相与金红石相共存的纳米TiO2比纯锐钛矿相和金红石相有更优异的光催化活性,在卤钨灯下照射90min,对次甲基蓝的降解率达到97%。 相似文献
83.
设计和开发了面向对象的XML数据查询系统原型OOX(object-oriented XML).OOX系统中包括了面向对象XML数据查询系统的一些核心功能,如存储、索引、查询等.其最大的特点是:它是一个可以实现对富含面向对象XML数据进行查询的XML查询系统;支持用继承扩展的XML模式语言DTD的解析,支持用继承扩展的XML查询语言XML-RL;采用了先进的路经仓索引模式以及高效的查询处理技术,可以实现高效的查询处理. 相似文献
84.
85.
采用脉冲激光沉积(PLD)技术在Si(111)衬底上生长了Eu3+、Li+共掺杂的ZnO薄膜。分别对样品进行了X射线衍射(XRD)谱测试和光致发光(PL)谱分析,重点研究了退火处理对样品结构和发射光谱的影响。XRD谱测试表明,样品具有很好的C轴择优取向。PL谱研究表明,当用325nm光激发样品时,样品的发射光谱仅由ZnO基质的紫外发射和蓝光发射组成,并没有发现稀土Eu3+的特征发光峰;样品的蓝光发射源于电子从Zn填隙形成的浅施主能级到Zn空位形成的浅受主能级跃迁;和真空中退火的样品相比,O2中制备的样品的蓝光发射减弱,紫外发光增强。用395nm的光激发时,退火前样品分别在594nm和613nm处存在两个明显的Eu3+特征发光峰,退火后的样品仅发现Eu3+位于594nm的特征发光峰,这表明,退火处理不利于稀土离子的特征发射,但O2中退火的样品ZnO基质红绿波段发射光谱明显增强。 相似文献
86.
针对耦合波导缝隙馈电时波导内电磁场复杂且不利于工程应用的问题,提出一种耦合波导缝隙有源阻抗计算方法.根据耦合波导端口处S矩阵与端口处输入阻抗矩阵的关系建立关于耦合波导缝隙有源阻抗方程,且采用牛顿法求解此非线性高阶分式方程,得到计及缝隙间互耦的耦合波导缝隙有源阻抗值.通过提取HFSS软件中耦合缝隙馈电的裂缝天线S矩阵进行仿真计算,结果表明该计算耦合缝隙有源阻抗的方法是有效的且适合大型裂缝天线耦合裂缝设计. 相似文献
87.
《Catalysis communications》2011,14(1):101-105
Well-ordered hexagonal mesoporous silicate (HMS) materials with various contents of phosphotungstic acid (HPW) were synthesized via an original direct synthesis method. The characterization results show that the samples have regular fingerprint-like mesopores and spherical morphology. Compared with the conventional wet impregnation method, the samples obtained by the original direct synthesis method have better HPW dispersion and larger specific surface area. Finally, the catalytic performance of these samples was tested through the oxidative desulfurization (ODS) of DBT in the model oil. The results indicate that the direct synthesized samples exhibit better catalytic performance than the impregnated samples. 相似文献
88.
This paper is concerned with the leader-following consensus problem of a group of au-tonomous agents with unknown parameters and unmodeled bounded additive disturbances. Under the assumption that the topology graph has symmetric weights, distributed adaptive controllers are proposed to guarantee that each agent can follow the leader in the presence of bounded disturbances. For the dynamics without disturbances, the proposed dynamic controller ensures that the states of all agents track the leader’s state, and the errors of parameters eventually converge to the compact set which can be made as small as desired by an appropriate choice of the design parameters. 相似文献
89.
Shu Yang Sun Han Sheng Gong Kun Zhao Xiao Lin Wang Xue Wang Xi Hao Zhao Bing Yu Huan Xin Wang 《International Journal of Food Science & Technology》2013,48(9):1783-1790
This study examined the effect of co‐inoculation of yeast and lactic acid bacteria (LAB) on the chemical and sensory characteristics of cherry wines, in comparison with a traditional sequential culture. Three LABs were investigated, including two O. oeni (SG26 and Viniflora) and one L. plantarum (PL18). All co‐inoculations significantly shortened the fermentation time (average 8 days earlier) to reach a stable level of residual sugar (<2 g L?1) and L‐malic acid (<0.5 g L?1), and no inhibitory effect on the yeast proliferation was observed. For volatiles determined, co‐culture with SG26 produced the greatest amount of volatile components (138.5 mg L?1), whereas sequential inoculation with PL18 had the lowest level (119.6 mg L?1). PCA result revealed that different LABs had diverse influences on the volatile profile of cherry wines, and sensory analysis confirmed that these samples presented distinct sensory profiles, and particularly, a stronger note of fruity was perceived when co‐culture was used. 相似文献
90.