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41.
《Journal of the European Ceramic Society》2005,25(2-3):129-135
A poly(aminoborazine), precursor for hexagonal boron nitride (h-BN) obtained by reaction of borazine B3N3H6 with ammonia, and its pyrolysis derivatives have been extensively characterised by 15N and 11B MAS NMR. The various B and N sites have been identified according to their first neighbouring atoms, as well as to the second ones in the case of 15N, and have also been quantified. This study demonstrates that a suitable choice of NMR techniques together with the use of isotopic enrichment can lead to a large improvement in spectral resolution, which allows a better understanding of such complex BN preceramic polymer structures and permits to follow the polymer-to-ceramic transformation. 相似文献
42.
《International Communications in Heat and Mass Transfer》2005,32(1-2):214-223
The present paper analyses the entropy generation of the fully developed laminar convection in a helical coil with constant wall heat flux and presents the optimal design based on the minimum entropy generation principal. The important design parameters, including Reynolds number (Re), coil-to-tube radius ratio (δ) and nondimensional coil pitch (λ) are varied to investigate their influences on the entropy generation. The results presented in this paper cover Re range of 100–10,000, δ and λ range from 0.01 to 0.3. Compared with Re and δ, the coil pitch λ is found to have minor influence on the entropy generation. For a demonstrated case, the minimum entropy generation occurs in the range bounded by Re from 2271 to 4277 and δ from 0.17 to 0.3, within which the irreversibility of the system is lowest and the system performance would be optimum. The details show that there is an optimal Re for a helical coil with a fixed δ; meanwhile for a helical coil flow with a specified Re, the smaller δ should be selected when the Re is larger than 5000, and the larger δ should be selected when the Re is less than 5000. These results provide worthwhile information for heat exchanger designers to find the optimal helical coil design from the viewpoint of the thermodynamic second law. 相似文献
43.
《Cement and Concrete Composites》2006,28(9):790-799
This paper presents the results of an investigation of the properties of mortar in which a calcined clay was employed as a pozzolan. Mortars were prepared using either heat treated clay or ground waste clay bricks (from the same clay subjected to 1000 °C calcining) as a pozzolanic partial replacement for cement at replacement levels of 10%, 20% and 30%. The compressive strengths of the mortars were monitored up to 90 days and the resistance to sodium sulphate solution and synthetic seawater was monitored up to 300 days. The specimens were also monitored for weight changes. Partially replacing cement by ground brick or heat-treated brick clay gives early strengths that are lower than that of the control. At 90 days, however, the strengths are the same as or are greater than that of the control. Heat-treated clay is effective in reducing expansion during exposure of the mortar to sulphate solution and synthetic seawater. The rapidly cooled clay gives better performance, in terms of strength development and resistance to harmful solutions, than the slow cooled clay. 相似文献
44.
45.
《Journal of the European Ceramic Society》2005,25(9):1629-1636
Ultimate tensile strength of five different continuous fiber-reinforced ceramic matrix composites (CMCs), including SiCf/BSAS (two dimensional (2D), 2 types), SiCf/MAS (2D), SiCf/SiC (2D), and Cf/SiC (2D, 2 types), was determined as a function of test rate at 1100–1200 °C in air. All five CMCs exhibited a significant dependency of ultimate tensile strength on test rate such that the ultimate tensile strength decreased with decreasing test rate. The dependency of ultimate tensile strength on test rate, the applicability of preload technique, and the predictability of life from one loading configuration (constant stress-rate loading) to another (constant stress loading) all suggested that the overall, phenomenological delayed failure of the CMCs would be governed by a power-law type of slow crack growth. 相似文献
46.
Repetitive processes are a distinct class of 2D systems (i.e. information propagation in two independent directions) of both systems theoretic and applications interest. They cannot be controlled by direct extension of existing techniques from either standard (termed 1D here) or 2D systems theory. In this paper, we exploit their unique physical structure to show how two term, i.e. proportional plus integral (or PI) action, can be used to control these processes to produce desired behavior (as opposed to just stability). 相似文献
47.
48.
《Energy Policy》2005,33(2):133-150
In order to forecast the technological development and cost of wind turbines and the production costs of wind electricity, frequent use is made of the so-called experience curve concept. Experience curves of wind turbines are generally based on data describing the development of national markets, which cause a number of problems when applied for global assessments. To analyze global wind energy price development more adequately, we compose a global experience curve. First, underlying factors for past and potential future price reductions of wind turbines are analyzed. Also possible implications and pitfalls when applying the experience curve methodology are assessed. Second, we present and discuss a new approach of establishing a global experience curve and thus a global progress ratio for the investment cost of wind farms. Results show that global progress ratios for wind farms may lie between 77% and 85% (with an average of 81%), which is significantly more optimistic than progress ratios applied in most current scenario studies and integrated assessment models. While the findings are based on a limited amount of data, they may indicate faster price reduction opportunities than so far assumed. With this global experience curve we aim to improve the reliability of describing the speed with which global costs of wind power may decline. 相似文献
49.
《International Journal of Hydrogen Energy》2005,30(10):1053-1062
Photocatalytic activity of mesoporous titania supported nickel oxide photocatalyst synthesized by single-step sol–gel (SSSG) process combined with surfactant-assisted template method was investigated for hydrogen evolution from an aqueous methanol solution, in comparison with one prepared by conventional incipient wetness impregnation (IWI) method. In single-step sol–gel process, nickel precursor was introduced into the titania sol prepared with the aid of a surfactant template behaving as pore-controlling agent to attain meso-scaled pore. The single-step sol–gel photocatalyst was experimentally found to enhance the photocatalytic evolution of hydrogen rather than the impregnated one. The optimum level of nickel loading in photocatalytic activity test for single-step sol–gel method was slightly higher than that for incipient wetness impregnation method. Characterization results demonstrated the significant modification of physical characteristics of the single-step sol–gel photocatalyst, anticipated to relating to the observation of higher photocatalytic hydrogen evolution activity. 相似文献
50.
《International Journal of Heat and Mass Transfer》2007,50(15-16):3250-3263