等离子体控制优化激光烧结Ni30Cr25Al15Co15Mo5Ti5Y5高熵合金涂层的显微组织与性能(英文)

提出一种激光诱导等离子体的主动抑制方法,以优化Ni₃₀Cr₂₅Al₁₅Co₁₅Mo₅Ti₅Y₅高熵合金(HEA)涂层表面激光烧结(SLS)的晶体结构和摩擦学性能,该过程采用脉冲激光和不同保护气体。结果表明,无保护气体或He气氛下的电子温度(T_e)和等离子体射流体积均高于Ar-He气氛下的。SLS过程中发生明显的相变和金属原子扩散,α-AlFe₃、α-AlNi和γ-AlFe₂Ni化合物沉淀形成冶金结合。等离子体通过逆韧致辐射(IB)吸收较低能量加强激光与HEA之间的相互作用,使涂层显微硬度增加,动态摩擦因数降低,这说明等离子体控制对激光增材制造存在重要影响。     

Formation of Bi2ZnB2O7 Nanocrystals in ZnO–Bi2O3–B2O3 Glass Induced by Femtosecond Laser

We report on the formation of Bi₂ZnB₂O₇ crystal structures with designated patterns in ZnO–Bi₂O₃–B₂O₃ glass by femtosecond laser direct writing. The crystallization mechanism in glass is investigated by crystallization kinetics analysis and simulation of the three‐dimensional temperature field distribution. The crystallized regions show larger third‐order optical nonlinearity than the unirradiated region in glass by Z‐scan technique. This finding is of great potential in application of nonlinear optical integrated devices and development of new nonlinear materials.     

Crystal growth and characterization of Tm doped mixed rare-earth aluminum perovskite

In this work, we present results of structural characterization and optical properties including radio luminescence of (Lu_xGd_yY_0.99?x?yTm_0.01)AP single crystal scintillators for (x, y) = (0.30, 0.19), (0, 0.19) and (0, 0) grown by the micro-pulling-down (μ-PD) method. The grown crystals were single phase materials with perovskite structure (Pbnm) as confirmed by XRD and had a good crystallinity. The distribution of the crystal constituents in growth direction was evaluated, and significant segregation of Lu and Gd was detected in (Lu_0.30Gd_0.19Y_0.50Tm_0.01)AP sample. The crystals demonstrated 70% transmittance in visible wavelength range and some absorption bands due to Tm³⁺, Gd³⁺ and color centers were exhibited in 190–900 nm. The radioluminescence measurement under X-ray irradiation demonstrated several emission peaks ascribed to 4f–4f transitions of Tm³⁺ and Gd³⁺. The ratio of emission intensity in longer wavelength range was increased when Y was replaced by Lu or Gd.     

Synthesis,crystal structure and properties of a new lead fluoride borate,Pb3OBO3F

A new compound, Pb₃OBO₃F, has been grown by the high temperature solution method from the PbO–PbF₂–B₂O₃ system. It crystallizes in the orthorhombic system, space group Pbcm with unit-cell parameters a = 7.6313(14) Å, b = 6.5229(12) Å, c = 11.906(2) Å, Z = 4, volume = 592.66(19) Å³. The structure of the compound is solved by the direct methods and refined to R₁ = 0.0528 and wR₂ = 0.1400. Pb₃OBO₃F consists of Pb(1)O₃F tetrahedra, Pb(2)O₄ tetrahedra and BO₃ triangles which build up the symmetrical chains extended along the c-axis. The powder X-ray diffraction pattern of the Pb₃OBO₃F has been measured. Functional groups presented in the sample were identified by Fourier transform infrared spectrum.     

载波包络相位稳定的6 fs超快强激光脉冲及其在高次谐波产生中的应用

脉冲宽度40 fs,功率1.1 W的载波包络相位(CEP)稳定的飞秒激光脉冲在充氩气的空芯光纤内由于自相位调制频谱展宽,通过啁啾镜和斜劈补偿色散,最终可获得脉冲宽度为6 fs的载波包络相位稳定的强激光脉冲.将之应用到高次谐波实验中得到了脉冲宽度为500 as的单个阿秒脉冲.     

Least squares and genetic algorithms for parameter identification of induction motors

This paper deals with off-line parameter identification of induction motors by means of least square (LS) techniques and genetic algorithms (GA), using stator voltages, stator currents and velocity as input–output data. For analytical identification by LS algorithms, filtering of experimental data is performed by means of anticausal filters. Two models useful for identification are derived in which the products of acceleration and rotor fluxes, usually neglected, are taken into account. The GA-based identification method consists of the determination of the best parameters which match input–output behaviour of the motor. Both methods are investigated and compared by means of experiments carried out on a 1-kW induction motor.     

双色场相位平缓对远场前向太赫兹的增强

太赫兹辐射极性和幅度依赖于双色场相位。由于等离子体光丝中色散和Gouy相移，导致双色场的相对相位随着激光的传播发生改变。当相位的改变量大于时，丝中的太赫兹电场极性发生反转，使得远场太赫兹辐射在离轴相位匹配角方向相干增强，而光轴前向相消减弱。通过对基频和倍频聚焦条件的调整和传输非线性色散的作用对双色场相对相位进行了调制，提出了可以使相对相位平缓的方法。模型计算证明了等离子体形成和Gouy相移调制是使双色场相移变平缓的原因。随后利用相位变平缓的条件得到了太赫兹发生极性反转的失相长度延长，最大长度近三倍于空气介质中的失相长度。在满足相位变平的条件下，远场太赫兹辐射在光轴前向的分布得到增强。     

Tm:YAP激光晶体的生长及激光性能的研究

采用提拉法生长了高质量的4%(原子分数)Tm∶YAP晶体。X射线粉末衍射分析确定生长的晶体为Tm∶YAP晶体。吸收光谱分析表明Tm∶YAP晶体在688和794nm有较强的吸收峰。采用793nm激光二极管泵浦Tm∶YAP晶体,实现了2.01μm激光输出,最大输出功率5.1W,光转换效率为37%,斜率效率高达43.5%,连续可调范围从1894～2066nm,在2010nm得到最大的输出功率值为1.84W。     

Nanostructural modification of an Al–C–Ti coating on alloy AZ91D under the multipulse action of Nd:YAG and Ng-glass lasers

Experimental results on the nanostructural modification of an Al–C–Ti coating on magnesium alloy AZ91D under the multipulse action of Nd:YAG lasers (λ = 1064 nm, τ = 20 ns, and E = 200 mJ) and Nd-glass lasers (λ = 1060 nm, τ = 85 ns, and E = 2 J) are given. It is shown that the formation of the found nanocrystalline coating structure with a grain size of 35 to 400 nm involves the process of background deposition of ablated particles and condensed clusters formed in the plasma plume.     

飞秒激光作用下透明介质材料的反射率演化

利用800 nm抽运和400 nm探针技术,测量了CaF2和MgO的时间分辨反射率,研究了材料的电子激发和弛豫超快动力学过程。采用耦合动力学模型,探讨了飞秒激光对透明介质材料的激发,以及材料的激发对抽运激光在材料中的传输、分布和反射特性的影响。根据这个理论模型计算了时间分辨反射率的演化,计算结果和实验结果相吻合。研究表明,多光子电离(MPI)和碰撞电离(II)在介质材料的导带电子激发中起着重要的作用。