N_2O—C_2H_2火焰原子吸收分光光度法测定钨制品中的钇

本文研究了N_2O—C_2H_2火焰原子吸收分光光度法测定钨制品中钇的条件,拟定了分析方法.方法相对标准偏差1. 2%～3%,回收率95%以上.     

Effect of Y content on microstructure and mechanical properties of 2519 aluminum alloy

The effects of yttrium（Y） content on precipitation hardening, elevated temperature mechanical properties and morphologies of 2519 aluminum alloy were investigated by means of microhardness test, tensile test, optical microscopy（OM）, transmission electron microscopy（TEM） and scanning electron microscopy（SEM）. The results show that the tensile strength increases from 485 MPa to 490 MPa by increasing Y content from 0 to 0.10%（mass fraction） at room temperature, and from 155 MPa to 205 MPa by increasing Y content from 0 to 0.20% at 300 ~C. The high strength of 2519 aluminum alloy is attributed to the high density of fine 0＇ precipitates and intermetallic compound AICuY with high thermal stability. Addition of Y above 0.20% in 2519 aluminum alloy may induce the decrease in the tensile strength both at room temperature （20 ℃） and 300℃.     

钇离子注入锆的动电位极化曲线研究

通过对锆表面进行不同剂量的钇离子注入及对电位极化曲线的测量，分析了钇离子注入对锆电化学行为的影响。结果表明：钇离子注入能明显地提高锆在酸性、中性及碱性环境中的耐腐蚀性能。用X光电子能谱(XPS)分析了离子注入样品表层的成分与价态，进而探讨了钇离子注入表面改性的机理。     

钕离子掺杂钇铝石榴石(Nd3+:Y3Al5O12)透明陶瓷研究进展

回顾了新一代激光工作物质Nd3 :Y3Al5O12透明陶瓷的发展历史,并与激光晶体进行了比较介绍了其技术优势,同时简述了Nd3 :Y3Al5O12透明陶瓷的2种常用工艺。     

Properties of plasma sprayed NiCrAlY ＋ ZrO2 coating on TiAl alloy surface

The NiCrAIY＋ZrO2 thermal barrier coating was prepared on the surface of TiAI alloy by plasma spraying technique. The microstructure and phase structure were analyzed using scanning electron microscopy （SEM） and X-ray diffractometry （XRD）. The high temperature oxidation resistance of the plasma sprayed samples at 850℃ was investigated. The results show that the bonding between thermal barrier coating and substrate is very good. Surface hardness of TiAI alloy is improved too, The microhardness of the coating surface is about HV 900 after the oxidation test at 850 ℃. The oxidation resistance of the samples is improved remarkably.     

La2O3-Gd2O3-Mo secondary emission material

A new kind of materials La2O3-Gd2O3-Mo has been produced by powder metallurgy method.The composition and microstructure of the material were studied by XRD and SEM.It shows that no chemical reaction takes place among La2O3,Gd2O3,Mo and the rare earth oxides exist along molybdenum grain boundaries and in the pores.The emission property measurement results of this material show that adding rare earth oxide into molybdenum can improve the secondary emission coefficient of the emitter,and the emission property depends on the activation temperature.After La2O3-Gd2O3-Mo was activated at 1360℃,the maximum secondary emission coefficient can be high to 2.62,which has exceeded that for practical uses(2.0).     

EFFECTS OF CARBON AND YTTRIUM ON 500℃ AGING EMBRITTLEMENT OF ALLOY Fe-15Cr-4Al

测定了Ｆｅ－１５Ｃｒ－４Ａｌ合金在５００℃的时效脆化动力学，利用内耗，ＴＥＭ，ＥＰＭＡ和ＳＥＭ等手段研究了合金在时效后的组织变化和断裂行为。结果表明，时效脆化第一阶段（０－１００ｈ）主要是碳化物在α相晶界析出的作用，它损害界面结合，降低断裂应力，使塑性在时效０．２５ｈ后消失；第二阶段（１００－１０００ｈ）主要是富Ｃｒ－α＇相均匀析出的作用，它通过强化基体引起二次脆化。含０．２和０．４％的Ｆｅ－１５     

钇离子注入AZ31镁合金的氧化行为

研究了AZ31镁合金在钇离子剂量为5×10^16，1×10^17及5×10^17ions／cm^2注入条件下的氧化性能。纯氧气氛、500℃下的氧化实验结果表明，钇离子注入能提高AZ31镁合金的抗氧化性能，而且随着注入剂量的增大，合金表面抗氧化性能提高越大。俄歇电子能谱（AES）和X光电子能谱（XPS）分析表明：钇离子注入以后，在镁合金表面形成了具有双层结构的氧化层，外层主要由MgO组成，而内层主要由Y2O3，MgO构成。这一新形成的氧化层有利于提高AZ31镁合金的抗氧化性能。     

YIG带阻滤波器的研究进展

随着通信与雷达系统在高频、宽带和小型化方面的高速发展,钇铁石榴石（YIG）带阻滤波器是其发展道路中不可缺少的磁调谐器件。该文针对YIG带阻滤波器阐述了YIG带阻滤波器设计原理,介绍了近年来几种典型谐振器结构的发展状况,并分析了这几种结构的优缺点。     

Al-Si合金的等离子电解氧化及膜层组织性能研究

为提高铝合金材料在高温下的使用性能,采用等离子电解法在锆盐体系和锆盐-钇盐复合体系中于铝硅合金表面制备了陶瓷层.分析了电解液浓度及成分对起弧电压、膜层厚度、组织及隔热温度的影响.研究结果表明:两种电解液体系中随电解液浓度的增大,起弧电压降低,陶瓷层厚度和隔热温度先增大后减小.与锆盐体系相比,锆盐-钇盐体系中起弧电压显著降低,膜层厚度与隔热温度提高.锆盐体系陶瓷层中生成了常温下稳定的t-ZrO2,锆盐-钇盐体系涂层中则生成了立方相的c-Y0.15Zr0.85O1.93.制备的两种陶瓷膜层与传统的硅酸盐膜层相比,其表面孔洞较少,锆盐-钇盐体系相对于锆盐体系其陶瓷层更加均匀、致密.