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981.
Giuseppe G. G. Manzardo Sandra Kürsteiner-Laube und Daniel Perrin 《Zeitschrift für Lebensmitteluntersuchung und -Forschung A》1996,203(6):501-506
In diethyl ether extracts from celeriac (Apium graveolens L. var.rapaceum) all four stereoisomers of (3a–7a)-cis-3-butylhexahydrophthalide were found to be present. The analyses were carried out by means of GC, enantioselective GC and GC-MS. The assignment of the relative configuration of the diastereomers3 and4 was accomplished by NOE difference spectroscopy. 相似文献
982.
The pyrolysis of tertiarybutylphosphine (TBP) has been studied in the low pressure conditions used for chemical beam epitaxy
(CBE). The pyrolysis studies were carried out in low pressure reactors of two different configurations, one of which is a
cracker cell designed for use in a CBE system. The reaction products were studied using a quadrupole mass spectrometer. The
products observed are accounted for by a reaction mechanism involving homolysis of the parent TBP molecule to produce PH2 and C4H9 radicals. These undergo subsequent reactions to form the stable products C4H8, PH3 and H2, with smaller amounts of P and P2 being produced. The production of the sub-hydride PH2 using this cracker cell design indicates that the use of partially cracked TBP may be a promising technique for reducing
the amount of carbon incorporated into the growing epitaxial layer. 相似文献
983.
研究了Al2O3、Al2o3/TiB2和Al2O3/TiB2/SiCW三处陶瓷材料在不同条件下的擦靡损特性。结果表明:三种陶瓷材料与硬质合金摩擦副的摩擦系数随温度温度的增加有不同的变化规律,摩擦表面的X射线衍射分析表明,摩擦系数的变化与陶瓷物膜的和结构有关,在高温下Al2O3/TiB2陶瓷材料摩擦表面形成了具有优良的高温润性的TiO2氧化膜,因而TiB2的加入明显改善了Al2O3陶瓷材料 摩擦磨损 相似文献
984.
H. Perez-Blanco 《International Journal of Refrigeration》1993,16(6):429-433
The search for high-efficiency, gas-fired cooling cycles has led to the development of dual-loop absorption machines with cooling coefficients of performance (COPs) in the 1.2 to 1.7 range. This increased performance may call for high generator temperatures, new working fluids or new materials of construction. In most cases, two different sets of working fluids are required. The conceptual design presented here is aimed at obtaining high efficiencies with relatively low temperatures, employing only one set of fluids. The concept consists of two loops coupled in a configuration aimed at minimizing the loss of thermodynamic availability incurred when transferring refrigerant between the loops. The working fluid pair is a solution of lithium bromide-water. The calculated COPs are of the order of 1.8. The cycle relies on an elaborate evaporator-absorber combination. The paper presents the conceptual design, the critical assumptions, and the performance calculations for the concept. 相似文献
985.
TORGILS FOSSEN ØYVIND M. ANDERSEN DAG OLAV ØVSTEDAL ATLE T. PEDERSEN ÅSE RAKNES 《Journal of food science》1996,61(4):703-706
Three red onion (Allium cepa) cultivars, top onion (A. cepa var. vivi-parum), A. altaicum and chive (A. schoenoprasum) contained several or all of the following anthocyanins: 3-(6′-malonyl-3′-glucosylglucoside), 3-(3′,6′-dimalonylglucoside), 3-(6′-malonylglucoside), 3-(3′-malonyl-glucoside), 3-(3′-glucosylglucoside) and 3-glucoside of cyanidin. Trace amounts of two pelargonidin derivatives and the 3,5-diglucosides of cyanidin and peonidin were for the first time reported in red onion. Carbon NMR data showed that the sugars of the 3-(6′-malonyl-3′-glu-cosylglucoside), 3-(6′-malonylglucoside) and 3-glucoside of cyanidin were pyranoses. Substitution either by sugar or acid in the sugar 3-position of an anthocyanin has never been reported outside the genus Allium. 相似文献
986.
Claes-Gran Johansson 《Journal of the Institute of Brewing》1996,102(4):249-250
A combustion method, relying on the Dumas principle, for the determination of total nitrogen in barley and malt, has been collaboratively tested by the Analysis Committee of the European Brewery Convention. Repeatability, r95, and reproducibility, R95, values were 0.063 and 0.116% of dry matter, respectively, for samples with nitrogen contents in the range 1.23 to 1.86% N of dry matter. There was no significant difference between these values for barley and malt. The Analysis Committee approved the adoption of the combustion method for inclusion in Analytica EBC as an alternative method. 相似文献
987.
续竞存 《固体电子学研究与进展》1996,16(3):254-258
用电荷控制及热电子弹道运动模型计算InAs/InP0.7Sb0.3热电子晶体管的截止频率fT及最高振荡频率fmax。结果表明,fT、fmax分别达到280GHz及600GHz。并指出,通过生长GaSb中间层,InAs/InP0.7Sb0.3HET可在GaAs衬底上实现单片集成。 相似文献
988.
It is possible to optimize the performance of the inorganic-organic composites dispersing the inorganic component in the organic matrix on a nanomiter length scale. If dry the inorganic phase cannot be intimately dispersed during the incorporation in the matrix. When the particle surface is organically modified, and the incorporation is made starting from a liquid dispersion (particles in polymer solution), the resulting composites exhibit an excellent homogeneity. Here, monolithic [poly(methyl methacrylate)/monodisperse silica particles] nanocomposites have been prepared and characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), dynamic light scattering (DLS), micro-hardness, and differential scanning calorimetry (DSC). 相似文献
989.
990.
Determination of assimilable organic carbon (aoc) in ozonated water with acinetobacter calcoaceticus
The effect of ozone application in drinking water on the production of assimilable organic carbon (AOC) was evaluated. The typical procedure to determine AOC is suggested by van der Kooij, which is the method of bacterial growth measurement by colony‐forming units using the strain P17 and/or NOX. The bacterial indicator species used for this study is Acinetobacter calcoaceticus which was isolated and identified while ozonating Nakdong river water. This strain could never be isolated from the raw water, but this strain was the predominant isolate in the ozonated water. Within a short incubation time, this organism was found to replicate well on acetate and oxalate as the sole carbon sources. The yield coefficients of this organism for acetate and oxalate are the same order of magnitude as the value of P17 and NOX. With full‐scale experiments, A. calcoaceticus concentration was found to increase after ozonation, but did not decrease upon chlorination. In laboratory‐scale experiments with Yongsan river water, aldehyes were found to be produced in proportion to the ozone dose. The raw water contains low concentrations of aldehydes, but has a high AOC concentration. A correlation between aldehyde production and AOC production was observed in the tested water with ozonation. 相似文献