真空熔炼高压气体雾化制粉技术及设备

介绍了气体雾化粉的品种、用途及工业化生产。还介绍了真空熔炼-高压气体雾化制粉所需的设备。     

新型双旋流平焰烧嘴的研制与应用

介绍了一种新型双族流平焰烧嘴的设计思路、结构参数及工业试验结果。其结构特点是每个部件都易装易卸，其煤气旋流器的位置可根据煤气压力变化进行调节，无需稳焰器就可保证煤气压力在较大范围波动时，都可形成稳定的平展火焰。     

储层识别模式的研究

用数学方法建立气测井油气储层识别模式,以解决录井中实时软件在判别依据少的条件下,及时识别油气显示假异常的难题。该判别式经实用,正到率达90％。     

采用混合物作工质的J—T节流制冷机

报告了国内外采用混合物作工质的Ｊ一Ｔ节流制冷机的实验研究情况。理论计算的两个重要参数（等温节流效应和正常沸点）与这些实验的结果作了对比。另外，给出了工作在不同压力下的一种混合工质及纯氮的焓温图。从理论计算和实验的结果可以看出混合工质Ｊ一Ｔ节流制冷机比单纯工质的Ｊ一Ｔ节流制冷机有更大的制冷量和更高的热效率。     

烟用香料配制的气相色谱法质量控制研究

采用气相色谱法对香料房卷烟用料液中的溶剂及水分进行检测,分析测定其中的水分、乙醇、丙二醇、山梨醇等的含量,通过对香料房每批配制料液的抽检,可以跟踪料液配制的准确性,保证卷烟产品质量,该方法操作简单、准确性高、重现性好。     

莺歌海盆地CO2成因及运聚特征的初步研究

在已获天然气地地化资料的基础上，重点论述了ＣＯ２天然气地化特征及成因类型，追踪和判识ＣＯ２气烃类气的气源，初步了ＯＣ２气的分布特征及控制因素，指出本区ＣＯ２气属壳源型岩石化学的成因，气源主要来自莺黄组中、下部含钙海相泥岩，与深部火山慢源的ＣＯ２气无关，谱不具深源的特征。     

SISAK快速化学分离装置的建立

SISAK(Short-lived Isotopes Studies by the AKUFVE technique)技术是目前使用最广泛的快速化学分离方法之一,主要应用在短寿命核素的分离和鉴别、超重元素的人工合成以及化学性质研究等方面的工作中.本文简单地叙述了SISAK技术的流程、原理和发展现状,介绍了自行建立的国内第一套基于SISAK技术的快速化学分离装置,并通过从裂变产物中分离短寿命核素这一实例验证了SISAK技术在快速化学分离中的优越性.     

GC/MS characterization of mate tea leaves extracts obtained from high-pressure CO2 extraction

This work presents a study concerning the chemical characteristics and analytical separation process of the essential oil obtained from high-pressure carbon dioxide extraction of Ilex paraguariensis. The experiments were performed in a laboratory-scale unit in the temperature range of 20–40 °C, from 100 to 250 bar. A blend of the I. paraguariensis extracts was percolated through a preparative chromatographic column, containing silica gel, and successively eluted with 150 mL of each of the following solvents: hexane, toluene, dichloromethane, ethyl acetate, acetone and methanol. The raw extract and its fractions were analyzed by gas chromatography coupled to mass spectrometry detection (GC/MS). The fractionation procedure showed to be a good clean up technique due to the isolation of different classes of compounds in each fraction. Chromatographic analyses allowed the identification of caffeine, fatty acids and esters, phytol, squalene, Vitamin E, stigmasterol derivatives and saturated hydrocarbons.     

β放射性气体浓度计的新分度方法

本文介绍β放射性气体浓度计的一种新的分度方法——泄漏元件排气法。其特点是一只元件可分度放射性气体浓度计的许多读出数(甚至是几个量程),操作方便。     

MASS TRANSFER IN GAS-SPARGED POROUS ELECTRODES

The electrochemical limiting current method was used to measure mass transfer coefficients with cocurrent upward gas-liquid flow in packed bed electrodes. Liquid-solid and overall gas-solid coefficients were determined from limiting current data in the presence of inert or reactive gas flows with the use of a plug flow model. The presence of inert gas flow increased mass transfer coefficients over those in single-phase flow by a factor of up to 1.7. As a result of boundary layer penetration by gas bubbles, sparging with reactive gas increased mass transfer rates by a factor of up to 3.5.