磁粉检验用标准试块的研制

介绍磁粉检验用B型和E型标准试块的设计、结构、研制、试验和应用。结果表明，两种标准试块都达到了国外同类标准试块的先进水平。     

Behavior of residual carbon in Sm(Co, Fe, Cu, Zr)z permanent magnets

When sintered Sm(Co, Fe, Cu, Zr)_z permanent magnets are prepared by metal injection molding, some organic binders are added in alloy powder, which leads to much residual carbon in the magnets. The residual carbon decreases magnetic properties and destroys the microstructure of the magnets. In this paper, the behavior of carbon in Sm(Co, Fe, Cu, Zr)_z permanent magnets has been studied. The results indicate that Sm(Co, Fe, Cu, Zr)_z magnets can keep excellent magnetic properties when the carbon content is below 0.1 wt.%: Br ≥ 10 kGs, H_cj ≥ 22 kOe, BH_max ≥ 25 MGOe. When the carbon content is above 0.1 wt.%, Br, H_cj and BH_max decrease with increasing carbon content evidently. Carbon consumes Zr content and forms ZrC, which reduces the volume fraction of the lamella and Sm(Co, Cu)₅ phases. Thus, the cell size increases and the cellular microstructure deteriorates. When the carbon content reaches 0.43 wt.%, there is not enough Sm(Co, Cu)₅ phase to form a uniform cellular microstructure. Br, H_cj and BH_max are approximate to zero. Since carbon has little influence on the content of Sm₂(Co, Fe)₁₇ phase, Ms can keep a high value (≥100 emu/g). ZrC has high melting point (3420 °C) and acts as dispersion particle in the magnets, which prevents the grains of SEM structure growing and reduces the liquid content of green compacts during sintering. Therefore, the density of the magnets decreases.     

钢管漏磁探伤中孔洞缺陷的漏磁场分析

针对钢管孔洞缺陷进行了分析。分别从数学模型和仿真软件建模等方面对孔洞缺陷进行了漏磁场分析，并且将采集的漏磁信号进行处理，得出孔洞半径与漏磁信号之间的关系，为孔洞缺陷信号的识别提供了一定的参考依据。     

Hysteresis minor loop analysis of plastically deformed low-carbon steel

This work investigates applicability of magnetic hysteresis method for non-destructive testing of plastically deformed low-carbon steel. Recently introduced Magnetic Adaptive Testing procedure was used for evaluation of hysteresis minor loop data-sets to find the most sensitive parameter/s for indication of the material degradation stage. Inductive measurements were carried out on two identically degraded series of samples: magnetically closed window-shaped specimens, equipped with the magnetizing and the induction coils, and magnetically open strips, measured by an attached magnetizing yoke. The aim was to compare the results between these sample series in order to determine applicability and limitations of the single-yoke measurement technique. As a result, new magnetic parameters with the best sensitivity–stability ratio in a wide deformation range were introduced and proposed for utilization. Good qualitative coincidence between the measurement results on the closed and the open sample series was obtained in all range of magnetization. Several quantitative distinctions were explained and analyzed in order to improve the single-yoke technique.     

Visualization of vortex core polarity in NiFe nanodots by tilted Fresnel images

We illustrate an approach which allows determining the out-of-plane component of the vortex core (polarity) in NiFe nanodots using Fresnel imaging in Lorentz electron microscopy. Using tilted Fresnel images, contribution of the polarity is introduced into the Fresnel image. However, this contribution is relatively small and a difference image from two symmetrically tilted Fresnel images must be used to eliminate the strong contribution from the in-plane curling magnetization and non-magnetic contrast. The sense of the polarity appears as a bipolar white-black contrast in the difference image on the tilt axis. A vortex core with a diameter of 16.5±2.5 nm is experimentally measured. Image tilting, displacement and geometrical distortion may disturb the difference image, and hence subtraction of the difference image must be aligned by cross-correlation. The method is also justified by a study of the observed contrast characteristic due to misalignment. The method is confirmed to be superior to similar approach with direct interpretation of information and more information subtracted.     

电磁搅拌技术在莱钢六号合金钢连铸机上的设计与应用

介绍结晶器电磁搅拌在矩形坯连铸机上的应用。采用内置式结晶器电磁搅拌后,连铸坯低倍组织大为改善,质量明显提高。     

适用于鱼肉中氯霉素检测的抗体包被金磁纳米微粒修饰安培免疫传感器研究

研制了基于氯霉素抗体包被Fe3O4/Au金磁纳米微粒(GMP)和三乙撑四胺铜(II)(CuL)共固定修饰平面热解石墨电极的安培免疫传感器(PRG|CuL / anti CAP-GMP),用于测定鱼肉中CAP含量.该免疫传感器是利用外加磁场,将anti CAP-GMP吸引到CuL修饰的PRG电极(PRG|CuL)表面制备而成.CuL对H2O2还原具有良好的电催化能力,当该传感器在含CAP样品液中温育后,CAP与电极表面的anti CAP的免疫结合物导致CuL对H2O2的催化还原电流(I)降低,电流下降值(△I)和CAP浓度成正比,可用于CAP定量测定.在25℃的pH=6.5磷酸盐缓冲液(PBS)中温育30 min,该传感器对CAP的检测线性范围为0.6~110 ng/mL,检出下限为0.092 ng/mL(3σ法).应用于鱼肉中CAP检测并与传统的液相色谱法(HPLC)比较,结果一致,其添加回收率在97%~104%之间.该免疫传感器集分离、富集为一体,电极表面可更新,检测灵敏快速,对于水产品中痕量氯霉素分析提供了一种新颖的方法.     

3维空间线与体对象间的拓扑关系完备性研究

线与体是3维空间中两类重要的空间对象,对其之间的拓扑关系进行研究在地矿开采、交通运输等很多领域都有非常重要的应用价值。为了准确高效地对3维空间线与体,特别是复杂对象间的拓扑关系进行分析,首先定义了一类基本空间对象,同时用9交模型来表达空间对象之间的拓扑关系;然后利用线与体之间的9条否定规则推导出基本线与体之间可能存在的11种拓扑关系,再利用复合推导的方法来得到复合线对象与体之间的19种拓扑关系;最后得出了用于推导分析复杂线与体之间拓扑关系的算法。经过详细分析与讨论,证明了这些拓扑关系具有完备性。实践表明,利用完备拓扑关系,不仅可以保证推导分析算法的正确性,也能极大简化复杂线对象与体对象间拓扑关系的分析。     

冲击载荷下磁流变阻尼器结构优化设计

应用于火炮反后坐装置中的磁流变阻尼器工作在高冲击、高速环境下,对磁流变阻尼器的设计指标和性能提出了更高的要求.针对冲击试验中,磁流变阻尼器表现出的阻尼力可调动态范闱的不足,利用Herschel-Bulkley的磁流变液非线性结构特性的平行平板恒流模型,采用多目标规划方法,提出了火炮反后坐装置应用中的磁流变阻尼器优化设计方法.最后分析了磁流变阻尼器磁路设计准则,结合优化设计尺寸,对阻尼器活塞磁场进行了有限元分析.结果表明,磁流变阻尼器阻尼通道处能产生足够大的磁场强度且分布均匀.     

Identification of parameters in a dynamic problem of elasticity for a body with an inclusion

Explicit expressions for gradients of residual functionals are obtained for the identification of the parameters of elastic dynamic deformation of multicomponent bodies by gradient methods. The technique is based on the solutions of conjugate problems found using the theory of optimal control over states of multicomponent distributed systems that is developed by the authors. Translated from Kibernetika i Sistemnyi Analiz, No. 3, pp. 75–97, May–June 2OO9.