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91.
Zan-guo?Peng Kus?Hidajat Mohammad?ShahabuddinEmail author 《Korean Journal of Chemical Engineering》2003,20(5):896-901
A colloidal suspension of magnetic particles coated with double layer surfactant molecules was prepared, characterized and
used for separation of some chemicals. The aqueous magnetic fluid was prepared by chemical precipitation method and characterized
by total organic carbon analyzer (TOC), thermogravimetric analysis (TGA) and transmission electron microscopy (TEM). The TOC
and TGA measurements indicate that the prepared magnetic particles are coated with surfactant molecules in double layers.
The outer surfactant layer has free polar heads. TEM measurement results show that magnetic particles are nanosized. A mixture
of 2-hydroxyphenol (strong polar) and 2-nitrophenol (weak polar) was chosen as the target system. Results show that the magnetic
fluid can selectively adsorb 2-hydroxyphenol from the mixture, whereas the adsorption of 2-nitrophenol is insignificant. For
2-hydroxyphenol, the adsorption equilibrium can be described well by Langmuir isotherm, and the adsorption kinetic can be
fitted well by a linear driving force mass transfer model. 相似文献
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The synthesis of magnetite nanoparticles coated with a well-defined graft polymer is reported. The magnetite nanoparticles with an initiator group for copper-mediated atom transfer radical polymerization (ATRP), 2-(4-chlorosulfonylphenyl) ethyltrichlorosilane (CTCS) chemically bound on their surfaces were prepared by the self-assembled monolayer-deposition method. The surface-initiated ATRP of methyl methacrylate (MMA) was carried out with the CTCS-coated magnetite nanoparticles in the presence of free (sacrificing) initiator, p-toluenesulfonyl chloride. Polymerization proceeded in a living fashion, exhibiting first-order kinetics of monomer consumption and a proportional relationship between molecular weight of the graft polymer and monomer conversion, thus providing well-defined, low-polydispersity graft polymers with an approximate graft density of 0.7 chains/nm2. The molecular weight and polydispersity of the graft polymer were nearly equal to those of the free polymer produced in the solution, meaning that the free polymer is a good measure of the characteristics of the graft polymer. The graft polymer possessed exceptionally high stability and remarkably improved dispersibility of the magnetite nanoparticles in organic solvent. 相似文献
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A numerical study is presented for magnetohydrodynamic free convection of an electrically conducting fluid in a shallow cavity heated from below and cooled from above. The side walls are maintained adiabatic. A uniform magnetic field, inclined with an angle 0 with respect to the horizontal plane, is externally imposed. The investigation covers the range of the Rayleigh number, Ra, from 1.8 × 103 to 3 x 104the Hartmann number, Ha, from 0 to 35, the Prandtl number, Pr, from 0.005 to 1 and aspect ratio of the cavity, A = 6. The effect of the magnetic field on the flow structure is presented. For supercritical convection it is found that, upon increasing Ha, the number of roll cells in the cavity increases when it is perpendicular to it. The imposition of an inclined magnetic field gives rise to new flow patterns with tilted lateral cell walls. The effect of both strength and orientation of the magnetic field on the overall heat transfer is found to be significant. 相似文献
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250m/s超高速磨床主轴磁浮轴承设计 总被引:3,自引:0,他引:3
本文介绍了磁浮轴承的优点,并针对一台250m/s超高速磨床主轴系统,首次进行了磁浮轴承设计,其结果对我国发展高速主轴技术有一定意义。 相似文献
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