计及PMU的混合非线性状态估计新方法

提出一种将同步相量测量单元（PMU）的直接电压相量量测变换为间接支路电流量测，并与监控与数据采集（SCADA）量测量一起进行混合迭代的非线性状态估计方法。对构造等效电流修正量而带来的间接量测误差进行了详细和定量的分析，并对该混合估计算法的精度进行了定性分析和定量计算。理论分析和算例表明，该方法可以获得较高的估计精度，在收敛次数和滤波效果上也有所改进。     

不同类型在役抽油机机架受力分析

通过现场测试和检查,对油田特定区域内经过优化后的各种不同类型抽油机在额定载荷下的支架以及连杆受力情况进行了分析和评价。为在油田范围内进行机采设备的选型和推广提供一些参考。     

Gasification of charcoal using supercritical CO2 at high pressures

A novel one-shell high temperature and high pressure semi-continuous reactor has been developed for the study of the Boudouard reaction at temperatures up to 820 °C and pressures up to 32.5 MPa. Semicontinuous gasification of charcoal using supercritical CO₂ has been achieved at conversions up to 90.8% (w/w) at LSHV between 20 and 30 h⁻¹ after 5–9 h. A gasification model is proposed and validated. Effective rates of gasification (1.32 ± 0.12) × 10⁻⁶ to (6.10 ± 2.03) × 10⁻⁵ s⁻¹ were obtained. The results indicated that this method is technically feasible for the on-line production of high pressures streams of CO/CO₂ in the lab for carrying out further chemistries, avoiding the use of CO high pressure bottles.     

Development,construction, and use of pneumometric tubes for measurement of steam flow in the steam lines of PVG-1000 at NPP

A system for the direct measurement of steam flow in steam lines after a steam generator, which utilizes a special design of pneumometric tubes and a computing unit that accounts for variation in steam pressure, has been developed to improve the quality of water-level regulation in the steam generators of VVéR-1000 power-generating units in the stationary and transitional modes. The advantage of the pneumometric tubes consists in their structural simplicity, high erosion resistance, and absence of irrevocable losses during measurement of steam flow. A similar measurement system is used at foreign NPP. The measurement system in question has been placed in experimental service at the No. 3 unit of the Balakovo NPP, and has demonstrated its worthiness. This measurement system can also be used to determine steam flow in the steam lines of NPP units with VVéR-1000 and VVéR-440 reactors, and PBMK-1000 power-generating units. __________ Translated from élektricheskie Stantsii, No. 3, March 2007, pp. 23–26.     

火电机组运行优化系统的现状与展望

简单回顾了国内外在火电机组运行优化领域的研究历程，列举了目前国内外市场上针对火电机组的各种主流运行优化产品的功能特点和应用情况，分析了国外引进产品和国内自主研发产品在中国当前市场环境下各自的优势和劣势。介绍了当前运行优化系统在国内电站机组的应用现状，阐述了国内外运行优化系统在实际应用中存在的问题，并提出了相应的改进意见。对机组运行优化系统的未来发展进行了展望，指出机组运行优化系统将利用先进技术设备和信息平台，与电站管理紧密结合，在日益规范的市场中不断发展完善，为提高电站经济性发挥更大的作用。     

On-line H NMR spectroscopic investigation of hydrogen bonding in supercritical and near critical CO2–methanol up to 35 MPa and 403 K

On-line NMR spectroscopy can beneficially be applied to studies of supercritical and near-critical fluids as an alternative to optical spectroscopy. Up to now high pressure NMR experiments are predominantly accomplished using custom made NMR batch reactors. The authors present a novel high pressure cell with displacement plunger for on-line NMR experiments on compressible fluids which can be used in conjunction with commercially available SCF NMR flow probes. The on-line technique offers advantages compared to stopped flow techniques such as enhanced control of mixture composition and reaction parameters as well as the facility of engagement into the reaction. The new apparatus is used for NMR studies on hydrogen bonding of methanol in near critical and supercritical carbon dioxide up to 403 K and 35 MPa for which data on the chemical shift of the hydroxyl group and methyl group are reported and interpreted.     

Hydrothermal synthesis and in situ surface modification of boehmite nanoparticles in supercritical water

In situ surface modification of boehmite (AlOOH) nanoparticles during hydrothermal synthesis in supercritical water was examined by adding CH₃(CH₂)₄CHO and CH₃(CH₂)₅NH₂ as modifier reagents to the reactants. Changes in surface properties of the nanoparticles by surface modification was observed by FTIR, dispersion in solvents and TEM analyses, which demonstrated that reagents chemically binded onto the surface of the AlOOH nanoparticles. The results of SEM and TEM pictures show that the surface modification affects crystal growth and reduces the particle size and changes the morphology of the particles.     

带疏水泵加热器出口主凝结水焓的计算方法

以火电厂热力系统热力单元矩阵分析法为基础，提出了一种更为科学有效的带疏水泵加热器出口主凝结水焓分析计算的新方法，应用表明，其结论与常规算法完全一致，图2表1参3。     

流动单元研究在油田开发中的应用

流动单元研究提供了精细解剖砂体，表征砂体内部非均质性的方法。应用流动单元研究的模式及不同层次流动单元的研究方法，对油田开发后期以结构要素为基本单位的剩余油研究和井网高速思路等方面进行了探讨。以东部某油田E1f1层为研究对象，对其储层流动单元分布进行了划分。应用途径包括：指导油水井部署，对高产部位进行预测，定量分析储量动用状况等。     

重油催化裂化装置再生器的改造

上海石化股份公司重油催化裂化装置为反应沉降器与再生器并列布置 ,两个再生器同轴布置。通过处理能力由 0 .8Mt/a提高至 1.0Mt/a的局部改造后 ,该装置产生了外取热器无法正常投用 ,两个再生器烧焦比例不易合理分配、第一再生器 (一再 )烧焦强度较低、剂油比偏低及催化剂单耗偏高等问题。因此 ,又对再生器进行了改造 :将一再船形待生催化剂分布器改为Y形分布器、在一再密相床上部增设格栅、外取热器催化剂返回分布器增设软密封、待生催化剂输送线路由斜管 立管 斜管的形式改为斜管形式等 ,改造效果好。