金属材料性能试验数据的统计处理

详细阐述了试验数据的表示方法以及数据统计的方法，分析了测量数据的不确定性产生的原因及其确定和测量误差产生的原因及其传递。     

Existence, uniqueness and stability of the equilibrium points of a SHARON bioreactor model

This paper addresses the dynamics of a SHARON reactor, a promising technology for ammonium removal from concentrated wastewater streams. The contraction mapping theorem is used to determine which operating conditions of a SHARON reactor with pH-control result in a unique equilibrium state. However, this approach only identifies the case of very large dilution rates, in practice corresponding with complete biomass wash-out, i.e. with complete loss of biological activity. Practical operation of a SHARON reactor aims at reaching ammonium conversion to nitrite. To identify such interesting operating points, the equilibrium points are subsequently calculated directly in terms of input variables for a simplified SHARON reactor model. The stability of the obtained equilibrium points is assessed and the corresponding phase portraits are analyzed. The influence of slightly varying parameter and input values is investigated as well.     

Age-related response of male melon fliesDacus cucurbitae (Diptera: Tephritidae) to cue-lure

Laboratory-reared and wild adults of the melon fly,Dacus cucurbitae Coquillett, were tested for response to cue-lure at various ages. Virgin laboratory (4, 6, 8, 10, 12, and 14 days old) and wild (10, 12, 14, 16, 18, 20, and 22 days old) flies were released into outdoor field cages and trapped from 0800 until 1600 hr. Response of males to cue-lure increased with age and corresponded with sexual maturity for each strain. Females of both strains were relatively nonresponsive to cue-lure. Failure to eradicate in past male annihilation programs againstD. cucurbitae may be explained in part by the fact that only older males, which may have already mated with gravid females, respond to cue-lure.     

Effects of irradiation in combination with waxing on the essential oils in orange peel

The study evaluated the effects of waxing, irradiation dose and post‐irradiation storage time on the essential oils in orange peel. Mature oranges (Maroc late) waxed or unwaxed were treated with 1 or 2 kGy radiation and stored for 9 weeks at 20 °C and 40–50% RH. Essential oils from the peel were extracted and analysed by GC. Results showed that D ‐limonene was significantly lower in waxed oranges; levels in samples treated with 2 kGy were higher than those in non‐irradiated or treated with 1 kGy. Linalool, methyl anthranilate and 3,7‐dimethyl‐2,6‐octadienal decreased as the dose increased. Levels of linalool increased with storage time but D ‐limonene was unaffected. These results may aid in guaranteeing the quality of orange essential oils during storage time. Copyright © 2004 Society of Chemical Industry     

Tearing, folding and deformation of a carbon-carbon sp-bonded network

A monolayer and a few layers of carbon sp²-bonded networks were torn and folded by the tip of an atomic force microscope at the steps on newly cleaved highly oriented pyrolytic graphite. It was found that the preferential breaking directions and folding axes are along the symmetry directions of the graphite hexagonal structure. Depending on the force exerted by the tip, breaking may occur along other directions. The torn part of the graphene sheet can even be stretched and deformed, and does not resume its original shape after release from the tip.     

Surface characteristics of fluorine-modified PAN-based carbon fibers

Different fluorination methods were applied to modify the surface properties of carbon fibers. The relationship between the degree of fluorination and the physicochemical properties of carbon fibers was studied using a combination of mechanical tests, elemental analysis (EA), X-ray photoelectron spectrometry (XPS), and X-ray diffraction (XRD). EA and XPS analyses of fluorinated carbon fibers showed that treatment with mixtures of F₂/O₂ introduced a much higher fluorine concentration than that with F₂ only. However, XRD analysis showed that there was no increase in the interlayer distance, due to the mild fluorination condition applied. Consequently, the oxyfluorination was one of the more effective methods to increase surface polarity of carbon fibers, which probably played an important role in improving the tensile properties of the fibers in the epoxy resin system.     

A Micellar Route to Ordered Arrays of Magnetic Nanoparticles: From Size‐Selected Pure Cobalt Dots to Cobalt–Cobalt Oxide Core–Shell Systems

Starting with Co‐salt‐loaded inverse micelles, which form if the diblock copolymer polystyrene‐block‐poly(2‐vinylpyridine) is dissolved in a selective solvent like toluene and CoCl₂ is added to the solution, monomicellar arrays of such micelles exhibiting a significant hexagonal order can be prepared on top of various substrates with tailored intermicellar distances and structure heights. In order to remove the polymer matrix and to finally obtain arrays of pure Co nanoparticles, the micelles are first exposed to an oxygen plasma, followed by a treatment in a hydrogen plasma. Applying in‐situ X‐ray photoelectron spectroscopy, it is demonstrated that: 1) The oxygen plasma completely removes the polymer, though conserving the original order of the micellar array. Furthermore, the resulting nanoparticles are entirely oxidized with a chemical shift of the Co 2p_3/2 line pointing to the formation of Co₃O₄. 2) By the subsequent hydrogen plasma treatment the nanoparticles are fully reduced to metallic Co. 3) By exposing the pure Co nanoparticles for 100 s to various oxygen partial pressures pequation/tex2gif-inf-5.gif, a stepwise oxidation is observed with a still metallic Co core surrounded by an oxide shell. The data allow the extraction of the thickness of the oxide shell as a function of the total exposure to oxygen (pequation/tex2gif-inf-7.gif × time), thus giving the opportunity to control the ferromagnetic–antiferromagnetic composition of an exchange‐biased magnetic system.     

大型压力容器现场热处理技术

以大连石化350万t/a催化裂化装置再生器为例,研究开发大型炼油化工设备现场新型热处理工艺。通过设置必要的热气流导向装置,采用微正压内燃工艺,配备新型大功率燃油喷嘴、用DCS集散控制系统调节油风比例和烟囱热量排放张合度,对超厚壁板适当增加电加热辅助热处理,解决了大容积、变截面、不等壁厚、超重设备施工现场热处理温度调整难度大、不均衡等技术问题。实践证明,应用该技术进行热处理,具有工期短、效果好、经济效益明显等特点。     

泥炭土地基钻孔漏浆的处理

以云南鸡石一级公路青鱼湾大桥为例，介绍了在软弱地层中施工桥梁钻孔灌注桩遇孔壁开裂漏浆时的处理方法，经试验证明，取得了较好的技术经济效果。     

阳泉市常用地基处理方法探讨

对阳泉市常用地基处理方法进行了分析，从适用范围、设计要点、施工与检验等方面进行了论述，着重提出了阳泉市常用地基处理方法的特点与适用性。