SGZ730/110型前、后部刮板输送机的研制

详细地介绍了用于短壁综采放顶煤工作面的SGZ730/110型前、后部刮板输送机的主要技术参数、结构特点、制造及井下试验情况。     

半固态模锻变形机制研究

通过帽形件的半固态模锻成形,阐述了半固态浆料变形的物理模型,研究了半固态浆料变形过程及变形机制。实验表明:半固态浆料模锻成形的变形方式是不同的,不同的固相率下其固液两相的塑性流动机制也是不同的;而且制件不同部位的微观组织形貌也有差异。     

液相浸渍C/C复合材料反应生成TaC的形貌及其形成机制

采用Ta有机溶剂浸渍C/C复合材料,经固化、热处理制备C/C-TaC复合材料.研究发现:在2MPa浸渍压力下,Ta有机溶剂易于浸渍C/C复合材料和固化;1500℃热处理后,Ta有机溶剂全部转变为TaC,其尺寸细小,结晶度高,呈颗粒状或聚集成团簇均匀分布在热解炭层面上;1800和2000℃热处理后的TaC形貌与1500℃热处理后的相似,Tac颗粒无明显长大现象.Ta有机溶剂转化生成Tac的机理研究表明:热处理过程中,Ta有机溶剂先生成中间相的氧氟化钽,转变为Ta₂O₅后,再与C还原-化合生成TaC.     

Precise and fast phase wraps reduction in fringe projection profilometry

Phase wraps in a 2D wrapped phase map can be completely eliminated or greatly reduced by frequency shifting. But it usually cannot be optimally reduced using conventional fast Fourier transform (FFT) because the spectrum can be shifted only by a integer number in the frequency domain. In order to achieve a significant phase wrap reduction, we propose a fast and precise two-step method for phase wraps reduction in this paper, which is based on the iterative local discrete Fourier transform (DFT). Firstly, initial estimate of the frequency peak is obtained by FFT. Then sub-pixel spectral peak with high resolution is determined by iteratively upsampling the local DFT around the initial peak location. Finally, frequency shifting algorithm that operates in the spatial domain is used to eliminate phase wraps. Simulations and experiments are conducted to demonstrate the superb computing efficiency and overall performance of the proposed method.     

用热化学反应法制备金属陶瓷涂层工艺的研究

研究用热化学反应法在金属表面制备陶瓷涂层的工艺，并对涂层的相结构及显微组织进行分析。结果表明，采用该工艺可以在金属表面获得连续、致密且与基体结合良好的陶瓷涂层。腐蚀试验证明，采用本工艺在４５号钢表面涂覆陶瓷后可使其抗蚀性显著提高。     

碳酸钙对热致相分离制备聚偏氟乙烯多孔膜结构的影响

通过熔融共混聚偏氟乙烯(PVDF)/CaCO3/复合稀释剂拟三元体系,采用热致相分离法(TIPS)制备了PVDF多孔膜。研究了复合稀释剂含量、CaCO3含量、粒径以及后期酸处理对膜结构的影响。结果表明:CaCO3含量和粒径对膜结构有明显的影响。在采用复合稀释剂的基础上,通过控制CaCO3粒子添加量,改变粒径,可以实现对膜结构的优化,并且经酸处理提高了PVDF膜孔隙率。     

退火温度对纳米TiO2薄膜结构和亲水性的影响

采用射频磁控溅射方法制备出纳米二氧化钛(TiO2)薄膜,研究了不同退火温度对薄膜微观结构和超亲水性的影响.结果表明:退火温度升高,晶粒长大,孔隙率减小;常温制备300 ℃以下退火的TiO2薄膜为无定形结构,亲水性差;400 ℃～650 ℃退火的薄膜为锐钛矿结构,表现出超亲水性;800 ℃退火薄膜为金红石结构,亲水性有所下降.     

低价钒－锯氧化物系的相关系和电导率

研究了Ｓｒ－Ｖ－Ｏ系统内低价钒氧化物存在时的相关系．用Ｘ光衍射分析鉴定了相组成，并用标准直流四探针法测定了１００～１０００Ｋ温度范围内的组成相的电阻率．结果表明在该系统内，在还原气氛下形成的低价钒化合物有六方的Ｓｒ８Ｖ８Ｏ（２５），立方的Ｓｒ２Ｖ２Ｏ５和Ｖ２Ｏ３，三者在１５０Ｋ以上均具有１０ｏ～１０１Ω·ｃｍ的电阻率．Ｖ２Ｏ３相在低于１５０Ｋ附近电阻率有一个约１０４数量级的跃升，显示了在降温时由导电性向绝缘性的突变．     

Liquid Letters

Using the interfacial jamming of cellulose nanocrystal (CNC) surfactants, a new concept, termed all‐liquid molding, is introduced to produce all‐liquid objects that retain the shape and details of the mold with high fidelity, yet remain all liquid and are responsive to external stimuli. This simple process, where the viscosity of the CNC dispersion can range from that of water to a crosslinked gel, opens tremendous opportunities for encapsulation, delivery systems, and unique microfluidic devices. The process described is generally applicable to any functionalized nanoparticles dispersed in one liquid and polymer ligands having complementary functionality dissolved in a second immiscible liquid. Such sculpted liquids retain all the characteristics of the liquids but retain shape indefinitely, very much like a solid, and provide a new platform for next‐generation soft materials.     

电子束蒸镀纳米TiO_2薄膜结构、相组成及亲水性研究

利用电子束蒸镀技术在石英玻璃和单晶Si〈100〉上制备了纳米TiO2薄膜,研究了衬底温度和退火温度对其结构、相组成和亲水性能的影响。结果表明,衬底温度为40~240℃时,石英玻璃上制备的薄膜为无定型TiO2,单晶Si〈100〉上制备的薄膜为弱结晶性的金红石TiO2,两类薄膜的亲水性均很差。退火温度显著影响薄膜的相组成及亲水性能。石英玻璃上不同衬底温度制备的TiO2薄膜经550,650℃退火后均转变为锐钛矿TiO2,具有很好的亲水性能。单晶Si〈100〉上不同衬底温度制备的TiO2薄膜经550~950℃退火后,均由金红石和锐钛矿TiO2混晶组成,且随退火温度升高,薄膜中锐钛矿TiO2含量逐渐增加;随退火温度升高,衬底温度为40℃时制备的TiO2薄膜的亲水性能逐渐降低,而衬底温度为240℃时制备的TiO2薄膜的亲水性能逐渐增强。