全文获取类型
收费全文 | 25223篇 |
免费 | 2262篇 |
国内免费 | 1298篇 |
专业分类
电工技术 | 1677篇 |
综合类 | 2796篇 |
化学工业 | 2104篇 |
金属工艺 | 2362篇 |
机械仪表 | 4352篇 |
建筑科学 | 3312篇 |
矿业工程 | 1080篇 |
能源动力 | 557篇 |
轻工业 | 905篇 |
水利工程 | 786篇 |
石油天然气 | 878篇 |
武器工业 | 351篇 |
无线电 | 1308篇 |
一般工业技术 | 3101篇 |
冶金工业 | 970篇 |
原子能技术 | 210篇 |
自动化技术 | 2034篇 |
出版年
2024年 | 99篇 |
2023年 | 273篇 |
2022年 | 531篇 |
2021年 | 660篇 |
2020年 | 713篇 |
2019年 | 627篇 |
2018年 | 609篇 |
2017年 | 845篇 |
2016年 | 942篇 |
2015年 | 1025篇 |
2014年 | 1444篇 |
2013年 | 1483篇 |
2012年 | 1745篇 |
2011年 | 1876篇 |
2010年 | 1397篇 |
2009年 | 1457篇 |
2008年 | 1393篇 |
2007年 | 1784篇 |
2006年 | 1646篇 |
2005年 | 1324篇 |
2004年 | 1111篇 |
2003年 | 1025篇 |
2002年 | 807篇 |
2001年 | 707篇 |
2000年 | 636篇 |
1999年 | 573篇 |
1998年 | 360篇 |
1997年 | 384篇 |
1996年 | 296篇 |
1995年 | 250篇 |
1994年 | 190篇 |
1993年 | 121篇 |
1992年 | 97篇 |
1991年 | 77篇 |
1990年 | 62篇 |
1989年 | 63篇 |
1988年 | 58篇 |
1987年 | 30篇 |
1986年 | 11篇 |
1985年 | 4篇 |
1984年 | 6篇 |
1983年 | 5篇 |
1982年 | 4篇 |
1981年 | 2篇 |
1980年 | 5篇 |
1979年 | 11篇 |
1959年 | 2篇 |
1958年 | 2篇 |
1957年 | 3篇 |
1951年 | 1篇 |
排序方式: 共有10000条查询结果,搜索用时 31 毫秒
101.
Organic‐acid‐catalyzed sol–gel route for preparing poly(methyl methacrylate)–silica hybrid materials
Jui‐Ming Yeh Kuan‐Yeh Huang Chung‐Feng Dai B. G. Chand Chang‐Jian Weng 《应用聚合物科学杂志》2008,110(4):2108-2114
In this study, a series of organic–inorganic hybrid sol–gel materials consisting of a poly(methyl methacrylate) (PMMA) matrix and dispersed silica (SiO2) particles were successfully prepared through an organic‐acid‐catalyzed sol–gel route with N‐methyl‐2‐pyrrolidone as the mixing solvent. The as‐synthesized PMMA–SiO2 nanocomposites were subsequently characterized with Fourier transform infrared spectroscopy and transmission electron microscopy. The solid phase of organic camphor sulfonic acid was employed to catalyze the hydrolysis and condensation (i.e., sol–gel reactions) of tetraethyl orthosilicate in the PMMA matrix. The formation of the hybrid membranes was beneficial for the physical properties at low SiO2 loadings, especially for enhanced mechanical strength and gas barrier properties, in comparison with the neat PMMA. The effects of material composition on the thermal stability, thermal conductivity, mechanical strength, molecular permeability, optical clarity, and surface morphology of the as‐prepared hybrid PMMA–SiO2 nanocomposites in the form of membranes were investigated with thermogravimetric analysis, differential scanning calorimetry, dynamic mechanical analysis, gas permeability analysis, ultraviolet–visible transmission spectroscopy, and atomic force microscopy, respectively. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献
102.
Emilio Marengo Valentina Longo Elisa Robotti Marco Bobba Fabio Gosetti Orfeo Zerbinati Silvana Di Martino 《应用聚合物科学杂志》2008,109(6):3975-3982
Principal component regression (PCR), partial least squares (PLS), StepWise ordinary least squares regression (OLS), and back‐propagation artificial neural network (BP‐ANN) are applied here for the determination of the propylene concentration of a set of 83 production samples of ethylene–propylene copolymers from their infrared spectra. The set of available samples was split into (a) a training set, for models calculation; (b) a test set, for selecting the correct number of latent variables in PCR and PLS and the end point of the training phase of BP‐ANN; (c) a production set, for evaluating the predictive ability of the models. The predictive ability of the models is thus evaluated by genuine predictions. The model obtained by StepWise OLS turned out to be the best one, both in fitting and prediction. The study of the breakdown number of samples to be included in the training set showed that at least 52 experiments are necessary to build a reliable and predictive calibration model. It can be concluded that FTIR spectroscopy and OLS can be properly employed for monitoring the synthesis or the final product of ethylene–propylene copolymers, by predicting the concentration of propylene directly along the process line. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献
103.
Despite the common use of tapping-mode atomic force microscopy to image composites or polymer blends, very few studies have focused on the measurement of the interdiffusion at an interface between two polymers in contact. In this study, we show how to assess the interphase between two polymers with two methods. First, stable and robust tapping conditions are established, and the problem of the phase contrast is discussed. Second, a contact-resonance method is presented: the tip in contact with the sample is electrostatically excited at its resonance frequency by a self-controlled oscillator. The gain and frequency images allow us to measure the interdiffusion width. Both methods (using high and weak mechanical solicitation) give the same assessment of the interdiffusion width. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献
104.
Masashi Kashiwagi 《Journal of Engineering Mathematics》2007,58(1-4):51-66
Based on the momentum and energy conservation principles, a compact calculation formula is analytically derived for the wave-drift
force on a 2-D body floating in a two-layer fluid of finite depth. In a two-layer fluid, two different wave modes (the surface-wave
mode with longer wavelength and the internal-wave mode with shorter wavelength) exist not only in the incident wave but also
in the body-scattered wave, and these wave characteristics are properly incorporated in the obtained formula. It is noted
that, unlike the single-layer case, the wave-drift force can be negative in the incident wave of surface-wave mode, if the
transmitted wave with internal-wave mode is large. Numerical computations are implemented for a Lewis-form body by means of
the boundary-integral-equation method with Green’s function for the two-layer fluid problem. The effects of density ratio,
interface position, and body motions on the wave-drift force are studied, and some important features are found for two-layer
fluids. 相似文献
105.
本文通过运用“生产函数法”、“增长速度方程”来定量分析技术进步在长城铝业公司水泥厂产出增长中的作用,从中找出该水泥厂生产经营过程中存在的问题及未来发展方向。 相似文献
106.
荣鼎华 《重庆理工大学学报(自然科学版)》2003,17(2):29-30
指出根据《金属切削手册》给出的切削用量范围确定切削用量,有可能不适当,特别是在三爪卡盘装夹硬度低的半径小的工件时容易发生这种情况,提出根据工件硬度、夹持长度、三爪的夹持半径等诸因素确定切削用量的方法。 相似文献
107.
利用磁力显微镜(MFM)对TbFe磁性薄膜进行了不同抬举距离(分别为60~780nm)的磁力成像研究.在实验中,比较了低抬举距离(100nm以下)磁力像中样品-针尖的互相干扰;同时发现在高抬举距离磁力像中,随着抬举距离的增大,出现了与高凸起形貌对应的图像衬度特征,并随抬举距离的变化也改变着位置与强度,一直到抬举距离为仪器的极限值780nm时,形貌干扰仍未消失,对其形成机制进行了分析. 相似文献
108.
A. A. Korobkin 《Journal of Engineering Mathematics》2007,58(1-4):121-139
The paper deals with the two-dimensional unsteady problem of the impact of a liquid parabola onto a rigid flat plate at a
constant velocity. The liquid is assumed ideal and incompressible and its flow potential. The initial stage of the impact
is the main concern in this study. The non-dimensional half-width of the contact region between the impacting liquid and the
plate plays the role of a small parameter in this problem. The flow region is subdivided into four parts: (i) the main flow
region, the dimension of which is of the order of the contact-region width, (ii) the jet-root region, where the curvature
of the free surface is very high and the flow is strongly nonlinear, (iii) the jet region, where the flow is approximately
one-dimensional, (iv) the far-field region, where the flow is approximately uniform at the initial stage of impact. A second-order
solution in the main flow region has been derived and matched to the first-order inner solution in the jet-root region. The
matching conditions provide an estimate of the dimension of the contact region for small time. Pressure distributions in both
the main flow region and the inner region are derived. The accuracy of the obtained asymptotic formulae is estimated. The
second-order hydrodynamic force acting on the plate is obtained and compared with available experimental data. A fairly good
agreement is reported. 相似文献
109.
S. Zaefferer 《Advanced Engineering Materials》2003,5(8):607-613
In recent years the investigation of local texture and microstructure by analysis of electron backscatter diffraction patterns (EBSP) in the SEM has become a very powerful and popular method. With the introduction of SEM with field emission guns (FEG) the spatial resolution of EBSP measurements could be enhanced from 500 nm with a tungsten emitter to better than 50 nm. This evolution of SEM techniques raises the question whether transmission electron microscopy (TEM) still has fields of application in texture research. The present article answers this question with a clear “yes” and presents three examples of investigations where TEM is indispensable. The three examples comprise the investigation of the correlation between dislocation structure and deformation texture, a study on nucleation mechanisms of recrystallization in highly deformed metals and the investigation of microtexture and microstructure in nanocrystalline materials. Together with the presentation of these cases some of the necessary measurement techniques are described briefly. It is shown that TEM has to be applied when highest spatial resolution of orientation determination and imaging and high accuracy of orientation determination are to be reached, when the three‐dimensional and quantitative characterization of lattice defects is required or when materials with a high density of lattice defects are to be investigated. 相似文献
110.