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11.
12.
Veysel T. Yilmaz Evrim Senel Canan Kazak 《Journal of Inorganic and Organometallic Polymers and Materials》2008,18(3):407-413
The reaction of [Cu(sac)2(H2O)4] · 2H2O with 2-methylpyrazine (mpyz) leads two complexes, concomitant crystallization of a mononuclear complex [Cu(sac)2(mpyz)(H2O)2] (1) and a polymeric complex [Cu(sac)2(μ-mpyz)]n (2). Both complexes have been characterized by elemental analyses, magnetic measurements, FT-IR and ESR, TG-DTA and single-crystal
X-ray diffraction analyses. Single-crystal X-ray analyses show that complex 1 consists of discrete molecules in which the copper(II) ions exhibits a square-pyramidal coordination geometry. The individual
molecules of 1 are connected into a hydrogen-bonded chain structure, which is further assembled to form a three-dimensional network by π–π stacking interactions.
Complex 2 is an 1D coordination polymer in which copper(II) centers are bridged by the mpyz ligand. The chains are further assembled
to form two-dimensional frameworks by π–π and C–H···π stacking interactions. 相似文献
13.
Hironori Oda 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》1995,63(3):223-228
Fluorans are given considerable attention as functional dyes for heat-and/or pressure-sensitive recording media. Numerous potential metal complexes were synthesised to prolong the life of coloured species. The protecting effect of these compounds against the photofading was examined on cellulose. It was found that the zinc or nickel salts of 3,5-dihydroxy-2-naphthoic acid and its derivatives can be applied as effective stabilisers against the fading of fluoran dyes. 相似文献
14.
Construction of the La Grande Complex in Eastern Canada called for complete or partial diversion of six rivers, the mean annual discharge of which varied from 60 to 1600 m3 s?1, and the transfer of water from two adjoining watersheds (1586m3 s?1) into La Grande Rivière. Three of these rivers with reduced flow, Eastmain (from 700 to 95m3 s?1), Opinaca (from 260 to 35m3 s?1), and Caniapiscau (from 1708 to 960m3 s?1) and the waterways with increased flows, Boyd-Sakami (from 1 to 811m3 s?1) and La Grande Rivière (from 1760 to 3400m3 s?1) were intensively monitored from 1978 to 1988, while the others were surveyed sporadically. Very few modifications were observed, compared to previous conditions, in banks stability, water quality, and aquatic fauna of the affected rivers: those which appeared can be explained by the water level fluctuations, the water quality of the tributaries of the residual drainage basin, and/or by the direct influence of the reservoirs. In James Bay, the areal extent of the Eastmain River and La Grand Rivière plumes varied with discharge in an exponential relation, mostly under ice cover; resources from the coastal environment had not yet undergone any major changes. Because of the very small population dwelling in the area, less than 3000 inhabitants, modifications in the hydrological regime of these rivers did cause relatively few impacts, the main being greater banks instability in specific locations, reduction of the thickness and ice cover on La Grande Rivière, enhancement of navigation constraints on Eastmain River, and higher mercury levels in fish related to operation of the reservoirs. 相似文献
15.
两种具有电双稳态的全有机络合物 总被引:9,自引:0,他引:9
首次发现两种在室温下即具有电双稳态的全有机(有机-有机)络合物,分别称为MCA+TCNQ和BBDN+TCNQ。它们可在真空中制备成薄膜,在数伏电压的作用下,从高电阻至低电阻的跃迁时间小于100ns,因此可作为一次写入的存储器材料。根据我国目前最小刻线宽度的水平,可望在1.6cm2的SiO2平面上做出64Mb的存储器。 相似文献
16.
用面向对象编程实现问题求解自动化 总被引:2,自引:0,他引:2
本文从面向对象方法基本原理和面向对象编程的技术特征出发,阐明所建应用软件系统中的对象,类及相应类层次结构和类组合结构,使系统具有很强的表现真空世界复杂系统结构的能力,系统通过消息传递在程序执行中实现对操作的调用机制,使之在面向用户问题选择和执行求解策略方面有很强的适应性,这一点对于强调人-机交互和解题协作的智能决策支持系统设计至关重要,文章给出了用C++实现的模型对象系统及消息传递机制。 相似文献
17.
Meimei Xia Zeshui Xu 《Information Fusion》2012,13(1):31-47
We study the group decision making problem under intuitionistic fuzzy environment. Based on entropy and cross entropy, we give two methods to determine the optimal weights of attributes, and develop two pairs of entropy and cross entropy measures for intuitionistic fuzzy values. Then, we discuss the properties of these measures and the relations between them and the existing ones. Furthermore, we introduce three new aggregation operators, which treat the membership and non-membership information fairly, to aggregate intuitionistic fuzzy information. Finally, several practical examples are presented to illustrate the developed methods. 相似文献
18.
In recent years several approaches have been proposed to overcome the multiple-minima problem associated with nonlinear optimization techniques used in the analysis of molecular conformations. One such technique based on a parallel Monte Carlo search algorithm is analyzed. Experiments on the Intel iPSC/2 confirm that the attainable parallelism is limited by the underlying acceptance rate in the Monte Carlo search. It is proposed that optimal performance can be achieved in combination with vector processing. Tests on both the IBM 3090 and Intel iPSC/2-VX indicate that vector performance is related to molecule size and vector pipeline latency. 相似文献
19.
Maria Buuales Maria Cristina Ballesteros-Briones Manuela Gonzalez-Aparicio Sandra Hervas-Stubbs Eva Martisova Uxua Mancheo Ana Ricobaraza Sara Lumbreras Cristian Smerdou Ruben Hernandez-Alcoceba 《International journal of molecular sciences》2021,22(8)
Immune checkpoint inhibitors (ICIs) have demonstrated remarkable efficacy in a growing number of malignancies. However, overcoming primary or secondary resistances is difficult due to pharmacokinetics issues and side effects associated with high systemic exposure. Local or regional expression of monoclonal antibodies (mAbs) using gene therapy vectors can alleviate this problem. In this work, we describe a high-capacity adenoviral vector (HCA-EFZP-aPDL1) equipped with a mifepristone-inducible system for the controlled expression of an anti-programmed death ligand 1 (PD-L1) blocking antibody. The vector was tested in an immune-competent mouse model of colorectal cancer based on implantation of MC38 cells. A single local administration of HCA-EFZP-aPDL1 in subcutaneous lesions led to a significant reduction in tumor growth with minimal release of the antibody in the circulation. When the vector was tested in a more stringent setting (rapidly progressing peritoneal carcinomatosis), the antitumor effect was marginal even in combination with other immune-stimulatory agents such as polyinosinic-polycytidylic acid (pI:C), blocking mAbs for T cell immunoglobulin, mucin-domain containing-3 (TIM-3) or agonistic mAbs for 4-1BB (CD137). In contrast, macrophage depletion by clodronate liposomes enhanced the efficacy of HCA-EFZP-aPDL1. These results highlight the importance of addressing macrophage-associated immunoregulatory mechanisms to overcome resistance to ICIs in the context of colorectal cancer. 相似文献
20.
合成4种标题配合物,用元素分析、红外和紫外光谱、摩尔电导、核磁共振氢谱、荧光光谱及X射线粉末衍射物相分析研究了它们的组成和性质及其结构。按结构将配合物分为两类,一是含氢键的离子缔合物;一是含金属—氧键的螯环型配合物。 相似文献