40Cr钢复合热处理强韧化

用光学及电子显微镜(SEM.TEM)观察不同热处理的40Cr 钢的冲击及断裂韧性断口、及金相组织,阐明其间相互关系;断口结构可反映断裂特征,组织情况;细化晶粒提高强度、塑性和冲击韧性,但却减少脆断的特性距离 l 因而降低 K_(1c)模;减少碳(杂质)偏聚而使其呈较均匀地分布,从而减少可诱发塑坑的较粗大的碳(杂质)化合物的析出,即增加塑坑的间距 di 以及增加塑断组成物。从而都可增加断裂临界应变 ef,都可以提高 K_(1c)40Cr 复合热处理既靠先超高温淬、回火以减少碳(杂质)偏聚,改善其分布,以反增加位错马氏体从而提高 K_(1c),也靠后淬、回火细化晶粒而提高强度、塑性和冲击韧性,各自发挥长处达到强韧化。     

Synthesis and activation of Pt nanoparticles with controlled size for fuel cell electrocatalysts

Well-dispersed Pt nanoparticles with controlled size and narrow size distribution were prepared by polyalcohol reduction of platinum acetylacetonate, using oleylamine as a capping agent. The particle size was varied from 3.5 nm to 11.5 nm by decreasing the amount of oleylamine added in the synthesis. Size selection of the as-prepared particles by solvent fractionation yielded nearly monodispersed Pt particles. The as-prepared particles were loaded on a carbon support by physical deposition, but showed no electrocatalytic activity due to the oleylamine bound to the particle surface. The particles were activated for electrocatalysis after heating the particles in air at 185 °C for 5 h, conditions that gave no particle-sintering and no oxidation. Cyclic voltammetry showed that the particles after the heat treatment in air were electrocatalytically active for methanol oxidation. The smaller 3.5 nm and 4.0 nm Pt particles had a higher intrinsic activity for methanol oxidation, but a lower tolerance to CO poisoning, compared with 6.0 nm, 9.5 nm and 11.5 nm particles. CO-stripping results suggest that CO is more easily oxidized on larger Pt particles.     

酶法提取树莓汁的研究

本试验以澳洲红、早红、美国22三个品种树莓为原料，通过不同的酶处理方法来制原果汁，优选适于制汁的品种和酶处理方法。     

超高相对分子质量聚乙烯纤维研究进展

介绍了超高分子质量聚乙烯纤维的制备、表面改性及应用的研究进展 ,指出了今后超高分子质量聚乙烯纤维的研究及应用的发展方向     

Electrical and optical studies of ZnO:Ga thin films fabricated via the sol–gel technique

The effects of dopant (Ga) concentration, post-heat treatment temperatures, and different heat treatment environments on the morphology, electrical and optical properties of ZnO films were studied. ZnO films doped with Ga are derived from non-alkoxide zinc acetate via the alcoholic route by a sol–gel dip-coating technique. Introduction of Ga, as a dopant, can reduce crystallite size, which is attributed to the increased number of nucleation centers. Grain growth was also observed at high post-heat treatment temperature. It was discovered that different post-heat treatment environments (air or reduced atmosphere) did not change the structure orientation, microstructure shapes and size. It was found that the sheet resistance, R_s could be reduced by an order of magnitude, using post-heat treatment in reduced atmosphere (4%H₂–96%N₂).     

含氨废水处理方法的探讨

对催化剂厂含氨废水的处理，提出了多种方法，着重分析了A/O生物法、膜分离法和汽提法，比较后确定采用汽提法处理该废水，建成投产达到预期效果。     

体积-表面淬火中加热温度的自动控制

根据表面-体积淬火奥氏体规范的要求，分析了感应加热过程中温度控制的特点和方式，并介绍了采用红外线光导纤维测温和微机控温技术成功用于体积-表面淬火中透热温度的自动控制。     

真空热处理工艺参数的选取

通过多种材料、多种工件、多批次的加工，对常见真空热处理工艺参数的确定，摸索出一些经验公式，并在实际生产中取得很好效果。     

我国水利水电混凝土防渗墙的发展

４０年来，我国水利水电混凝土防渗技术，从无到有逐渐发展至今，已能够在各种特殊地层中修建各种用途的混凝土防渗墙。通过大量实践，积累了丰富经验。在科学研究、勘测设计和施工技术及现代化管理方面也获得很大进展，解决了在复杂地质条件下建坝所遇到的规模较大的常规地基处理技术，也掌握了特殊地基处理的某些关键技术。     

天荒坪电站500 kV开关站开挖与边坡整治施工——兼论开挖爆破对高边坡稳定的影响及对策

在大型水利水电施工中，经常遇到岩质高边坡稳定问题，天荒坪抽水蓄能电站５００ｋＶ开关站所处的地形地质条件非常复杂，本文着重介绍在边坡开挖和支护过程中，根据不同的地形地质情况所采取的控制爆破和支护措施。