Thermally induced microstructural changes in cotton fibers: A free‐volume study

I measured positron lifetime in natural polymer–cotton fibers as a function of isochronal annealing temperature in the range 27–290°C. The variations in the positron results indicated structural changes occurring in the cotton fibers and determined the glass‐transition temperature as 80°C. Activation energies were measured separately for the crystalline and amorphous regions, indicating the versatility of the technique. These values were close to the O? H bond dissociation energy, suggesting O? H bond dissociation, the most probable process occurring under thermal treatment. As an extension of the positron results, the molecular weight of the cotton fibers was determined to be 1,200,000 based on free volume, which was within the range suggested for cotton. There seemed to be an indication that crosslinking changed the spiral structure of cotton fibers to the network type. However, this needs to be validated by other measurements. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 86: 3336–3345, 2002     

滩海油罐CAD/CAG

根据滩海油田地区环境条件的特殊性,认为取50年一遇的3秒钟瞬时风速作为计算依据更切合实际,给出了相应的抗风设计方法和设计公式,根据最新储油罐抗震理论编制了验算程序.将计算机辅助设计与辅助绘图集成一体,形成了一套完整的储油罐CAD/CAG系统.该系统省去了过去人工计算需要查取数据的麻烦,可以自动检索,并完成各项分析计算和全套施工图的绘制工作.速度快、准确性高,直接输出透明图,整洁规范.该系统正用于实际设计生产.     

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本文应用灰色关联分析方法,对70种不同类型和组成的钻井液,进行了两参数流变模式优选及评价。与现行方法比较的结果表明此方法与现行结果的吻合度高,并有新颖、数据要求量少、结论易于比较等优点。     

Preparation of fatty acid methyl esters for gas-chromatographic analysis of lipids in biological materials

Theoretically, preparation of fatty acid methyl esters (FAMEs) deals with reversible chemical reactions in a complex system. Methodologically, there are numerous ways, generally characterized by the type of catalysts used and steps involved. Although there are more than a half dozen common catalysts, the majority fall into either acidic (HCl, H₂SO₄ and BF₃) or alkaline types (NaOCH₃, KOH and NaOH), with each having its own catalytic capability and application limitations. In terms of steps, many conventional methods, including those officially recognized, consist of drying, digestion, extraction, purification, alkaline hydrolysis, transmethylation/methylation and postreaction work-up. Although these methods are capable of providing reliable estimates if some precautions are taken, they are cumbersome, time-consuming and cost-inefficient. A new approach has been to transmethylate lipidsin situ. Due to its simplicity, high sensitivity, comparable reliability and capability to determine total fatty acids, the method of direct transmethylation is finding a unique place in lipid determination. Regardless of which method is used, quantitative methylation requires chemists to take precautions at every step involved, particularly during FAME formation and subsequent recovery steps. Evidently, there is an urgent need for more systematic studies, guided by the chemical principle of reactions involved and physicochemical properties of regents and end products, into factors affecting these steps. Hopefully, this will lead to an improved method, which measures lipid composition in biological materials not only with high accuracy but also with high efficiency and minimum costs.     

脉冲功率器件直流和动态热特性探测

介绍了针对影响微波脉冲功率器件可靠性的热性能问题，应用红外热分析技术。对比探测微波脉冲功率器件在动态和直流状态下的温度分布，峰值结温，热阻及其变化规律。     

Properties of ligno‐cellulose fiber Hildegardia

Studies on some properties such as the density, the degradation temperatures, the morphology and the spectral features of the ligno‐cellulose fiber Hildegardia were carried out in both untreated and alkali treated form. The fibers are found to have good morphology and moderate initial and final degradation temperatures. On alkali treatment, the lignin was found to be eliminated. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 84: 2216–2221, 2002     

Open‐cycle OTEC systems with freshwater product: Effects of noncondensable gases on performance of condenser

An open‐cycle ocean thermal energy conversion (OC‐OTEC) system is one of the energy conversion methods used to generate electricity from ocean thermal energy. For the OC‐OTEC system, steam evaporated from the surface seawater due to flash evaporation drives the turbine. At that time, dissolved gas such as air is introduced into the low‐pressure system (OC‐OTEC system) as the noncondensable gas, which degrades the performance of condensation heat transfer. In this paper, a small‐scale OC‐OTEC experimental unit experimentally investigates the effect of noncondensable gas on the heat transfer performance in a condenser. The experimental results are discussed in comparison with theoretical estimation by the Sparrow–in method. It is shown that the condensation is occupied by heat and mass transfer near a condensation surface and that the condensation efficiency is affected by exhaust quantity of noncondensable gas at a relatively high concentration ratio of condensable gas. © 2005 Wiley Periodicals, Inc. Electr Eng Jpn, 154(1): 29–35, 2006; Published online in Wiley InterScience ( www.interscience.wiley.com ). DOI 10.1002/eej.20179     

太阳能热风发电技术研究进展

介绍了太阳能热风发电的产生背景、技术原理和特点。太阳能热风发电能够实现由太阳能到空气动能,最终到电能的转变,具有环保无污染、运行维护简单、缓解常规能源消耗等特点。简要介绍世界上第1座试验性质的太阳能热风发电站。对太阳能热风发电技术相关研究历程从试验研究和理论研究2个方面做了综述,重点介绍了澳大利亚电站的建设进展及最新相关学术研究进展,包括过渡段理论及试验研究、系统数值模拟和太阳能热风发电技术在高山地区的应用等。介绍我国太阳能资源情况,指出我国太阳能资源丰富,适合建造大型太阳能热风发电站。     

TRT入口方管道爆裂原因剖析

介绍了鞍钢7#高炉TRT装置入口方管道爆裂事故经过,进行了原因分析,并提出了解决措施。