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991.
992.
Acid Green 25, which is a diazoic dye bearing two sulfonic groups, is efficiently sorbed on chitosan. The protonation of chitosan may explain the electrostatic attraction of this anionic dye and that its optimum pH is close to 3. Preliminary protonation of amine groups (obtained by contact with a sulfuric acid solution) reduced the variation of solution pH following sorbent addition but significantly reduced sorption performance: the maximum sorption capacity of raw chitosan, 525 mg dye/g (0.84 mmol dye/g), was halved by acidic preconditioning. The acidic conditioning also reduced the kinetic rate—the time necessary to reach equilibrium increased up to threefold depending on the experimental conditions. The size of sorbent particles influenced sorption kinetics and equilibrium because of resistance to intraparticle diffusion, but the sorption appeared to occur not only at the surface of the sorbent but also in the intraparticle network of the polymer. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 90: 1073–1080, 2003 相似文献
993.
G. G. Martin 《Journal of Failure Analysis and Prevention》2004,4(1):37-39
Piston failures are not a common occurrence, but they do occur, and failure is usually associated with fatigue crack growth.
Most failures initiate at the gudgeon pin hole or in the skirt of the piston. Occasionally they fail elsewhere. In the example
covered in this paper, failure initiated in the crown and progressed down to the gudgeon pin before final failure occurred.
This paper outlines the cause and mode of failure and shows that small metallurgical discontinuities can contribute to these
failures under the right circumstances. 相似文献
994.
This study examines the links between antecedents and consequences of Gabonese teachers' (N= 152) work motivation. The theoretical underpinnings are based on the Motivational Model of Job Burnout (MMJB) which is grounded in Self-Determination Theory (SDT) and states that the more supervisors satisfy an employee's need for self-determination, competence, and relatedness, the more self-determined is the latter's work motivation. The level of self-determined motivation has an impact on job satisfaction, which in turn determines life satisfaction. Higher levels of self-determined motivation also buffer emotional exhaustion and psychological distress. The model was confirmed via structural equation modeling and provides support for the validity and generalizability of the MMJB and SDT. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
995.
程行毛 《石油化工安全环保技术》2003,(2)
分析了NaSCN装置脱色釜爆燃的原因,找出了引起爆燃的主要因素,提出了脱色生产安全防范措施。 相似文献
996.
997.
曾范华 《石油化工安全环保技术》2003,19(6):46-48
聚合反应器是无法检修设备,不允许打开,所以聚合反应器的制造质量必须严格控制,在设备制造过程中,严格按照设计图纸、技术要求及国家现行标准,进行控制设备制造、检验和验收,使制造质量达到规定要求。 相似文献
998.
999.
M. R. JOYCE K. K. LEE S. SYNGELLAKIS P. A. S. REED 《Fatigue & Fracture of Engineering Materials & Structures》2004,27(11):1025-1036
Complex multi‐phase Al–Sn–Si alloys are commonly employed in the manufacture of small automotive plain bearings. The fundamental fatigue initiation behaviour of this class of alloys is currently not well understood. A range of analytical techniques were applied to investigate preferential initiation site location and to attempt to identify critical microstructural features. It was apparent from experimental studies that points of fatigue crack initiation are associated with the Si secondary phase. Using tessellation approaches and subsequently both adaptive numerical modelling and micro‐scale finite element modelling allowed the identification of features affecting the probability that a given Si phase would initiate a fatigue crack. 相似文献
1000.
多排数翅片管空冷器风阻特性的数值模拟 总被引:1,自引:0,他引:1
本文对多排数翅片管空冷器空气侧的风阻特性进行了数值模拟.利用商用软件Fluent进行数值计算,结合经验公式和已有的实验数据,分析了不同入口风速下,阻力的变化规律以及流动阻力和温度变化对模拟计算的影响. 相似文献