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91.
硫化铜矿中提取铜的新方法研究   总被引:3,自引:0,他引:3  
对从硫化铜矿中提取铜的溶剂进行了详细研究,提出了“过硫酸铵-氨水-Ag ̄+”催化、氧化、络合的提取法。  相似文献   
92.
α,ω-Methacrylate-terminated poly(1,3-dioxolane)s (polyDXL) were synthesized by cationic ring-opening polymerization of DXL in the presence of methylene-bis(oxyethylmethacrylate) as transfer agent. If the initiator concentration is small compared with the transfer agent concentration, the molecular weights of the polymers are governed by the ratio of the reacted monomer to the reacted transfer agent. The α,ω-methacrylate-terminated polyDXLs obtained undergo free radical polymerization with formation of polyacetal networks. The properties of the networks as function of the molecular weight of the corresponding prepolymers are reported.  相似文献   
93.
A CEC-funded project has been performed to tackle the problem of producing an advanced Life Monitoring System (LMS) which would calculate the creep and fatigue damage experienced by high temperature pipework components. Four areas were identified where existing Life Monitoring System technology could be improved:
1. 1. the inclusion of creep relaxation
2. 2. the inclusion of external loads on components
3. 3. a more accurate method of calculating thermal stresses due to temperature transients
4. 4. the inclusion of high cycle fatigue terms.

The creep relaxation problem was solved using stress reduction factors in an analytical in-elastic stress calculation. The stress reduction factors were produced for a number of common geometries and materials by means of non-linear finite element analysis. External loads were catered for by producing influence coefficients from in-elastic analysis of the particular piping system and using them to calculate bending moments at critical positions on the pipework from load and displacement measurements made at the convenient points at the pipework. The thermal stress problem was solved by producing a completely new solution based on Green's Function and Fast Fourier transforms. This allowed the thermal stress in a complex component to be calculated from simple non-intrusive thermocouple measurements made on the outside of the component. The high-cycle fatigue problem was dealt with precalculating the fatigue damage associated with standard transients and adding this damage to cumulative total when a transient occurred.

The site testing provided good practical experience and showed up problems which would not otherwise have been detected.  相似文献   

94.
简要介绍了采用慢应变速率试验,U型弯曲和C形环试验等技术,分别对800合金,304和316及316Ti不锈钢A533B压力容器用多在模拟核反应堆环境中的应力腐蚀破裂敏感性性进行的试验研究的一些主要结果;并结合电化学测试和表面膜俄歇电子能谱分析结果进行了讨论。  相似文献   
95.
Si3N4powders coated with 6 wt% Y2O3and 4 wt% Al2O3were prepared by coprecipitation. The resulting powders were dispersed in water at different pH values and with addition of various amounts of ammonium polyacrylate (NH4PA) to produce 32 vol% slips. The influence of the amount of NH4PA solution added and pH on the rheological properties of 32 vol% coated Si3N4slips were studied. In addition, the sintered density of cast samples was determined and related to the degree of slip dispersion. The adsorption of the NH4PA on the coated particle surface was rather high and the surface became saturated near 0.86 mg/m2at pH 9.2. High NH4PA concentrations (1.7–3 wt%) were necessary to obtain well dispersed 32 vol% coated Si3N4slips at pH 9.2. The best stabilization was obtained with the addition of 2.3 wt% NH4PA; in this condition, the viscosity reached a minimum value of 35 mPa.s at 100 s–1. The slip viscosity increased with increasing pH from 9.2 to 10.2. Slips with low viscosities gave a more dense packing of cast samples and consequently higher sintered density values.  相似文献   
96.
随着油田开发时间的延长,油水井井下套管的损坏将越来越严重,套管故障井将越来越多,为了恢复套损井生产,将套管损坏所造成的损失降到最低,在配套波纹管补贴,水动力补贴,爆炸补贴等专门修套技术的基础上,通过认真调查研究,又配套了操作方便简单,适用套管损坏类型广的自动力套管补贴加固技术,使各种套管变形,套管断错(错开没有位移或位移量不大时)、套管破裂,误射孔井段封堵,已射开水层封堵等修井作业的难度进一步降低,从而进一步提高了修复井综合开发经济效益。  相似文献   
97.
晋城市煤炭加工利用现状、存在问题及发展建议   总被引:1,自引:0,他引:1  
张茂林 《煤化工》2002,30(1):6-8
阐述了晋城市煤加工利用的现状 ,分析了煤炭加工利用存在的问题 ,提出了今后的发展建议  相似文献   
98.
Incorporation of silicon species from an alloy substrate into anodic titania is shown to stabilise the structure of the film, facilitating investigation of the ionic transport processes in amorphous titania grown at high efficiency. Thus, an amorphous anodic film developed on a sputtering-deposited Ti-6 at.%Si alloy formed to 100 V in phosphoric acid electrolyte in contrast to a partially crystalline film developed on relatively pure titanium at <20 V. Silicon species, which are immobile and act as marker species in the growing film, are present in the inner 58% of the film thickness. Evidently, the film material forms simultaneously at the film/electrolyte and alloy/film interfaces by co-operative transport of cations and anions, as is usual in amorphous anodic oxides. The phosphate anions incorporated from the electrolyte migrate inward at 0.34 times the rate of O2− ions and hence are present in the outer 62% of the film thickness.  相似文献   
99.
该控制工程主要效益是改变鄱阳湖“夏水冬陆”的现状,成为祖国名符其实的第一大淡水湖,水面与避署胜地庐山和历史名城南昌、景德镇等相连,改善沿湖环境,发展航运,增加水产,开发利用丰富的水资源和旅游资源使之与杭州西湖、瑞士日内瓦湖等并列为世界名湖。  相似文献   
100.
介绍了质量流量计的工作原理有应用效果。这种新型质量流量计精度高,稳定性好,示值计量简便,可直接显示质量、流量、介质温度、密度等,维护量低,但必须正确安装、使用,才能发挥其应有的作用。  相似文献   
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