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11.
Poly(ethylene aspartate) [PEA] was synthesized by the melt condensation of D,L-aspartic acid and ethylene glycol. PEA containing pendent amino and carbonyl groups in its repeating chain was used as the polymeric ligand for complexation with transition metal ions, viz. Co(II), Ni(II), Cu(II), Mn(II), Zn(II), Cd(II), Ca(II), Mg(II), Pb(II) and Hg(II). Complexation was found to be most effective in DMSO. The resulting polyester-metal complexes were solid coloured materials which have been characterized by IR spectroscopy, elemental analysis and magnetic susceptibility measurements. The thermal stability of the polyester-metal complexes was investigated by thermogravimetric analysis (TGA). On the basis of the physico-chemical studies, an oxygen and nitrogen coordinated structure for the polyester-metal complexes is proposed. 相似文献
12.
Melt index is considered an important quality variable determining product specifications. Reliable prediction of melt index (MI) is crucial in quality control of practical propylene polymerization processes. In this paper a least squares support vector machines (LS‐SVM) soft‐sensor model of propylene polymerization process is developed to infer the MI of polypropylene from other process variables. Considering the use of a SSE cost function without regularization might lead to less robust estimates; the weighted least squares support vector machines (weighted LS‐SVM) approach of propylene polymerization process is further proposed to obtain a robust estimation of melt index. The performance of standard SVM model is taken as a basis of comparison. A detailed comparison research among the standard SVM, LS‐SVM, and weighted LS‐SVM models is carried out. The research results confirm the effectiveness of the presented methods. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 101: 285–289, 2006 相似文献
13.
总结了开发生产低熔融指数聚丙烯的试验过程与结果,通过优选催化剂、优化操作过程、控制加氢量,生产出质量稳定可靠的熔融指数在0.2~0.5g/l0min之间的低熔融指数聚丙烯. 相似文献
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钨在铂电极上成核动力学研究 总被引:3,自引:0,他引:3
采用循环伏安法和计时电流法研究了钨在KF-B2O3-K2WO4(62-37-1m/o)熔体中(T=795℃)铂电极上成核动力学过程。实验结果表明:该过程符合扩散步骤控制的半球形三维晶核连续成核长大的动力学规律。 相似文献
16.
提出了一种新的铝液夹杂物快速检测方法。导出了该法的检测原理方程。分析并试验研究了影响检测重复性和分辨率的因素。试验选择了较好的检测参数,并获得了较好的检测结果。 相似文献
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The homopolyester of 4-(4′-hydroxyphenoxy)benzoic acid (poly(4-HPBA)), was prepared under two different reaction conditions and compared with a sample provided by another research group. Depending on the synthetic route, different melting points, d.s.c. traces and crystal lattices were found. However, after repeated heating and cooling, one thermodynamically stable modification with a melting point of 370–375°C can be obtained. Copolyesters of 4-hydroxybenzoic acid and 4-(4′-hydroxyphenoxy)benzoic acid were prepared with various molar ratios either in the melt (condensation in bulk) or in solution. These copolyesters were characterized by elemental analyses, 1H n.m.r. spectroscopy, d.s.c. measurements, wide-angle X-ray scattering measurements at various temperatures, and optical microscopy. Whereas copolyesters prepared in solution do not melt below 500°C, those prepared by polycondensation in bulk show melting points down to approximately 260°C and form a nematic melt. 相似文献
19.
单螺杆挤出机—熔体泵串联挤出系统的性能与应用 总被引:3,自引:0,他引:3
从原理与应用方面,分析、探讨了单螺杆挤出机-熔体泵串联挤出系统的优异性能以及在塑料挤出成型领域的高效应用。 相似文献
20.
Effect of Traveling Magnetic Field on Mould-Filling Length of the A357 Melt during Casting THin Walled Plate 总被引:1,自引:0,他引:1
In order to improver the mould filling ability ,the method for production of thin-walled castings in the traveling magnetic field was applied,The relationship between magnetic field density and input voltage as well as distance was investigated,and the mould filling length of A357 melt has been studied,The electromagnetic forces applied on the melt were also analyzed,The result shows that the mould-filling length of the melt increase rapidly with the increase of magnetic flux density,The mould filling lengths in gypsum upper mould and magnetic material upper mould were compared from the standpoint of application,It demonstrated that the steel upper mould is superior to gypsum mould. 相似文献