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31.
32.
Emilio Marengo Valentina Longo Elisa Robotti Marco Bobba Fabio Gosetti Orfeo Zerbinati Silvana Di Martino 《应用聚合物科学杂志》2008,109(6):3975-3982
Principal component regression (PCR), partial least squares (PLS), StepWise ordinary least squares regression (OLS), and back‐propagation artificial neural network (BP‐ANN) are applied here for the determination of the propylene concentration of a set of 83 production samples of ethylene–propylene copolymers from their infrared spectra. The set of available samples was split into (a) a training set, for models calculation; (b) a test set, for selecting the correct number of latent variables in PCR and PLS and the end point of the training phase of BP‐ANN; (c) a production set, for evaluating the predictive ability of the models. The predictive ability of the models is thus evaluated by genuine predictions. The model obtained by StepWise OLS turned out to be the best one, both in fitting and prediction. The study of the breakdown number of samples to be included in the training set showed that at least 52 experiments are necessary to build a reliable and predictive calibration model. It can be concluded that FTIR spectroscopy and OLS can be properly employed for monitoring the synthesis or the final product of ethylene–propylene copolymers, by predicting the concentration of propylene directly along the process line. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献
33.
Crystal phase transition between the low- and high-temperature phases has been investigated for ethylene (E)-tetrafluoroethylene (TFE) alternating copolymer (ETFE) containing the third monomeric species by the temperature dependent measurements of wide-angle X-ray diffraction (WAXD) and small-angle X-ray scattering (SAXS) and differential scanning calorimetry. Nonafluoro-1-hexene (NFH) and hexafluoropropylene (HFP) were chosen as the third monomers, where they are different in the side-branch length, -(CF2)3CF3 and -CF3, respectively. In the case of E/TFE/NFH copolymer (ET-C4F9), the crystal phase transition temperature of the original ETFE two-components copolymer was not very much affected by the existence of NFH in the range of NFH content from 0.7 to 3 mol%. Contrarily, the crystal phase transition temperature of E/TFE/HFP copolymer (ET-CF3) was found to decrease drastically with increasing HFP content. The melting temperature and the higher-order structure were also affected sensitively depending on the HFP content. This difference in phase transition behavior between ET-C4F9 and ET-CF3 copolymers is reasonably interpreted as follows: the short side groups (-CF3) of HFP monomeric unit are included in the crystal lattice of E/TFE chains and the unit cell is expanded gradually with an increment of the HFP content, resulting in the decrease in phase transition point because of easier thermal motion of the chains. On the other hand, the long side groups [-(CF2)3CF3] of NFH monomeric units are excluded out of the crystal lattice and located on the lamellar surfaces or in the amorphous region and do not affect very much the phase transition temperature even when the NFH content is increased. In association with such a change in crystal structure, the long period of stacked lamellar structure was found to decrease remarkably in the case of NFH, whereas it does not change very much for HFP, consistent with the interpretation of the above-mentioned WAXD data. 相似文献
34.
介绍光电被动感应控制开关模块工作原理,研究开发了一种基于被动感应控制原理的自动冲水控制装置,总结比较了主动感应控制与被动感应控制的优缺点及其应用特点。 相似文献
35.
陈伯夫 《石油化工设备技术》2003,24(3):10-13
熔体过滤器为聚酯装置关键设备,其国产化问题一直未能解决。该文通过对天津分公司200kt/a聚酯装置熔体过滤器改造方案的介绍,探讨了其国产化条件,分析了国产熔体过滤器的结构特点,并与进口过滤器进行了对比,提出了一些看法。 相似文献
36.
结构安全性综合评估方法的研究 总被引:1,自引:0,他引:1
已有结构的安全性的评估是关系到社会经济、安全的重大问题。本文作者从临界结构入手,以构件失效影响面积为参考,得到了计算构件重要性系数的简便方法,结合构件的可靠度提出了定性与定量结合的结构安全性综合评估方法。从工程实例来看,本文提出的方法简单实用,与现行的鉴定标准符合得比较好。 相似文献
37.
Farnaz Agahian Seyed Ali Amirshahi Seyed Hossein Amirshahi 《Color research and application》2008,33(5):360-371
The weighted principal component analysis technique is employed for reconstruction of reflectance spectra of surface colors from the related tristimulus values. A dynamic eigenvector subspace based on applying certain weights to reflectance data of Munsell color chips has been formed for each particular sample and the color difference value between the target, and Munsell dataset is chosen as a criterion for determination of weighting factors. Implementation of this method enables one to increase the influence of samples which are closer to target on extracted principal eigenvectors and subsequently diminish the effect of those samples which benefit from higher amount of color difference. The performance of the suggested method is evaluated in spectral reflectance reconstruction of three different collections of colored samples by the use of the first three Munsell bases. The resulting spectra show considerable improvements in terms of root mean square error between the actual and reconstructed reflectance curves as well as CIELAB color difference under illuminant A in comparison to those obtained from the standard PCA method. © 2008 Wiley Periodicals, Inc. Col Res Appl, 33, 360–371, 2008 相似文献
38.
分析比较了进口锡与国产锡的成分和性能。设计出了新型的引线热浸镀锡合金,它具有较低的工作温度、优良的抗氧化性、流动性和可焊性。 相似文献
39.
无源软开关电路拓扑的研究 总被引:1,自引:0,他引:1
提出一个研究无源软开关电路的新技术方法;其特征是对基本的单管隔离型PWM DC/DC变换器进行类比分析,由此直接导出可行的缓冲能量再生复位电路.该新方法能使DC/DC PWM硬开关变换器转变为软开关变换器.以新型Boost无源软开关变换器为例,进行了电路理论分析与中功率样机的实验测试;结果表明此新变换器具有较宽的软开关工作范围、较低的电应力、较小的缓冲元件量值等特点.由此认为,这种研究方法推导简单、物理意义清晰,还能深入地研究无源软开关的新电路拓扑. 相似文献
40.
An algorithmic approach was used to select recoveries for non-sharp sequence designs. Simple distillation columns were employed. The non-key component distribution was modeled using the Fenske equation. The combination of producing impure products and allowing non-key component distribution, results in a large search space. With this large search space size and software limitations, five problems were solved (see summary table in the Design Examples sub-section). The optimal non-key component distribution was found to be significant but not necessarily maximal. Parallel processing was selected as optimal in contrast to the more traditional sequential processing. 相似文献