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991.
992.
Key experiments were carried out on the three Al–R–Mg (R=Gd,Dy,Ho) systems and the results obtained used for the thermodynamic optimisation reported in a separate paper in this issue [Caccasmani G, De Negri S, Saccone A, Ferro R. Intermetallics this issue.]. The samples were characterized by differential thermal analysis (DTA), X-ray powder diffraction (XRD), light optical microscopy (LOM), scanning electron microscopy (SEM) and quantitative electron probe microanalysis (EPMA). The isothermal sections at 400 °C are all characterized by extended homogeneity regions at a constant rare earth content. The extension of the (Mg,Al)R solid solution, cP2-CsCl type, varies with the R atomic number. Ternary compounds (τ) of Al2(R,Mg) stoichiometry (hexagonal Laves phases with MgNi2-type structure) have been found to exist at 400 °C in all the systems. Their temperatures of formation were detected by DTA measurements. 相似文献
993.
Anish Kumar Baldev Raj P. Kalyanasundaram T. Jayakumar M. Thavasimuthu 《NDT & E International》2002,35(4)
The impact echo technique is based on the use of transient stress waves for non-destructive detection of flaws in concrete structures. Impact-echo testing has been carried out for assessment of the structural integrity of the ring beam of a pressurised heavy water nuclear reactor. In order to develop the test procedure for carrying out impact echo testing, mock up calibration blocks were made. The detectability of the impact echo system has also been established in terms of the depth and the lateral dimension of the detectable flaw for the ring beam under consideration. Based on the optimised test parameters identified with the help of the studies carried out on the mock up blocks, impact echo testing was carried out on the ring beam of the reactor containment structure, for assessing its structural integrity. 相似文献
994.
995.
Surface modification of spherical LiNi1/3Co 1/3 Mn1/3O2 with Al2O3 using heterogeneous nucleation process 总被引:1,自引:0,他引:1
To improve the cycle stability at high voltage and high charge/discharge rate, spherical LiNi1/3Co1/3Mn1/3O2 was coated with Al2O3 by using heterogeneous nucleation process, and the physical and electrochemical properties were studied. The SEM images show that there is a uniform coating on the modified spherical LiNi1/3Co1/3Mn1/3O2. The electrochemical tests indicate that the properties of LiNi1/3Co1/3Mn1/3O2 coated with 0.5% aluminum oxide are the best. The initial capacities are 150 and 173 mA.h/g at the rate of I C in the voltage range of 2.7-4.3 V and 2.7-4.6 V, respectively, and the discharge capacities maintain about 99% and 85% after 30 cycles, respectively. While those of the bare LiNi1/3Co1/3Mn1/3O2 are only 90% and 75%, respectively. The CV tests of LiNi1/3Co1/3Mn1/3O2 show that Al203-coating can restrain the oxide-reduction peak currents fading during the charge/discharge course. 相似文献
996.
Microstructure and formation mechanism of titanium matrix composites coating on Ti-6Al-4V by laser cladding 总被引:2,自引:1,他引:2
CAI Lifang ZHANG Yongzhong SHI Likai 《稀有金属(英文版)》2007,26(4):342-346
Laser cladding experiments were done on a 5-kW continuous wave CO2 laser to synthesize TiC and TiB rein- fowed titanium matrix composite coatings on Ti-6AI-4V alloy with a mixture of Ti and B4C precursor powder. The ther- modynamics of the reactions were calculated and analyzed. The microstructure and phase evolution of TiB and TiC com- posites were investigated. The results showed that the chemical reaction between Ti and B4C would release much heat, and these compounds, TiC, TiB, and small amount of TiB2, can be formed on the surface of Ti-6AI-4V alloy if the supplied en- ergy is sufficient to excite the reaction among the initial products. A good metallurgical bond between the coating and the substrate can be achieved. The microhardness of coating was irregular and the maximum value was approximately HV600. 相似文献
997.
The extended X-ray absorption fine structure (EXAFS) method and transmission electron microscopy (TEM) have been used for characterizing the local structure and morphology of ferric oxyhydroxides, α-FeOOH and γ-FeOOH, with and without chromium. These ferric oxyhydroxide powders were prepared from aqueous solutions containing iron and chromium ions. Radial structural functions for iron obtained by Fe K edge EXAFS spectra showed that the linkage of structural units formed by FeO6 octahedra in γ-FeOOH is distorted by chromium addition, while such distortion in α-FeOOH is not clearly detected. On the other hand, Cr K edge EXAFS spectra showed that the local structure around chromium does not necessarily correspond to the local structure around of iron, which is observed by Fe K edge EXAFS spectra. This suggests that the structural units containing iron and chromium are heterogeneously distributed in these ferric oxyhydroxides. The local structural information was discussed coupled with morphological features of these ferric oxyhydroxides observed by TEM. 相似文献
998.
The thiospinel (Cr, Al)3S4 has been identified in the internal sulfidation zone of Al-diffusion coatings by electron diffraction in a transmission electron microscope. The Al/Cr ratio of this phase can vary over a rather broad range, obviously dependent on the Al/Cr ratio in the surrounding metallic matrix. The spinel can dissolve significant amounts of Ni and Mo, some Co but only traces of Ti. Increasing Al-content extents its stability to higher temperatures. 相似文献
999.
Al2O3对CaO-Al2O3-SiO2-Na2O系微晶玻璃结构与性能的影响 总被引:1,自引:0,他引:1
利用烧结法工艺制备CaO—Al2O3-SiO2-Na2O系微晶玻璃,通过DTA、XRD、IR和SEM等分析手段,系统研究Al2O3对CaO-Al2O3-SiO2-Na2O系微晶玻璃的结晶温度、晶体结构以及性能的影响。研究表明:随着Al2O3质量分数升高,初始析晶温度升高,晶体尺寸增大、析晶率升高,微晶玻璃的表观体积密度、显微硬度和抗折强度呈先增加后降低的趋势。在本实验条件下,最佳的Al2O3质量分数为11.77%。 相似文献
1000.
高级计划与排程是一种基于约束理论面向供应链的生产计划与排程工具,APS软件系统从ERP系统获取基础数据进行生产排程,再将排程结果送到ERP和生产系统中执行。本文在分析MTO型企业生产计划制定实施关键流程的基础上,对APS在企业生产排程中的应用方法进行了深入研究,同时探讨了系统集成的体系架构和关键实现技术。 相似文献